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Application of high energy X-ray diffraction and Rietveld refinement in layered lithium transition metal oxide cathode materials
Layered lithium transition metal oxide (LTMO) cathode materials have attracted much attention for lithium-ion batteries and are shining in the...
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Influences of nano-3Y-TZP reinforcement on phase transformation and crystallite size modification of zirconia-toughened alumina and Rietveld refinement of crystallographic data
The effects of varying amount of nano-3 mol% yttria-stabilized zirconia addition on the crystal structures, mechanical, and microstructural...
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Rietveld refinement and magnetic characterization of nanospheric CoFe2O4 prepared under the effect of ethylene glycol and H2O
Cobalt ferrite nanoparticles (CF NPs) have received appreciable interest recently due to their impressive chemical stability, high coercivity, and...
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Rietveld refinement combined with first-principles study of Zn and Al–Zn doped CdO thin films and their structural, optical and electrical characterisations
Un-doped, Zn-doped, and Al–Zn co-doped CdO thin films were deposited onto glass substrates at 350 °C by spray pyrolysis. X-ray diffraction (XRD)...
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Synthesis, microstructural, rietveld refinement and optical characterizations of sol–gel grown cerium oxide ceramics
The cerium oxide (CeO 2 ) ceramics have been synthesized in the current study by employing the sol–gel technique. Synthesized CeO 2 ceramics were eyed...
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MAUD Rietveld Refinement Software for Neutron Diffraction Texture Studies of Single- and Dual-Phase Materials
This work presents a detailed instructional demonstration using the Rietveld refinement software MAUD for evaluating the crystallographic texture of...
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Rietveld refinement, luminescence and catalytic study of as-synthesized and Dy3+-doped cubic Y2O3 nanopowder prepared by citrate mediated sol–gel technique
This paper reports on synthesis of undoped and Dy 3+ -doped cubic Y 2 O 3 nanopowder via a neoteric and conducive citrate sol–gel technique. The size and...
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Growth, rietveld refinement, Raman spectrum and dislocation of Ca2+/Mg2+/Zr4+-substituted GGG: a potential substrate and laser host material
The Ca 2+ /Mg 2+ /Zr 4+ -substituted Gd 3 Ga 5 O 12 (SGGG) crystal is widely used as magneto-optical substrate, such as preparation of YIG series thin films by...
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Dynamic electric, dielectric, impedance, and modulus spectroscopy study with Rietveld refinement of Al-substituted NiCuZn bulk ceramics
Ni 0.27 Cu 0.10 Zn 0.63 Al x Fe 2− x O 4 ( x = 0.0–0.16 with step 0.02) bulk ceramics were prepared from sol–gel-synthesized nanocrystalline powders and sintered...
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Dynamic response of electrical, dielectric and magnetic properties of La-substituted Ni-Cu-Cd bulk ceramics with structural rietveld refinement
Bulk dense ceramics are needed in many electronic applications instead of powder with grain in the nanometric range that is the prime objectives of...
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Co-relation between Rietveld analysis, dielectric studies and impedance spectroscopy of the Ba1−xSrxTiO3 ceramics
Barium strontium titanate (BST), with varying Sr do** levels ( x = 0, 0.05, 0.075, 0.1, 0.15, 0.3), was successfully synthesized using the...
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Magnetic-Controlled Short Process Preparation Technique for Phosphor Bronze Based on Structure Refinement
The conventional preparation process for Phosphor bronze typically involves high-temperature long-duration solid solution treatment to address the...
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Rietveld refinement, optical, dielectric and ac conductivity studies of Ba-doped SrSnO3
The samples SrSnO 3 (SBS0) and Sr 0.98 Ba 0.02 SnO 3 (SBS2) were synthesized using sol–gel route, followed by calcination at 1073 K. Rietveld refinement...
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Superstructure reflections in 40% Sn(II)-substituted BaZr0.5Ti0.5O3 perovskite modeled with a Bayesian method for crystallographic refinement
Tin(II) perovskite oxides are promising for lead-free ferroelectric applications because Sn(II) is isoelectronic to Pb(II) and is predicted to...
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Rietveld-Based Quantitative Phase Analysis of Sherardizing Coatings
The zinc coatings obtained by sherardizing consist of three zinc-rich Fe–Zn phases ( γ , δ and ζ ) and the properties of coatings are influenced by the...
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Rietveld refinement structure, electric, dielectric and ferroelectric properties of lead-free Ba0.985Sr0.015Zr0.10Ti0.90O3 ceramics
Ba 0.985 Sr 0.015 Zr 0.10 Ti 0.90 O 3 (BSZT) compound is prepared using the standard solid-state reaction technique to explore for energy storage...
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Rietveld refined structural and sintering temperature dependent electromagnetic properties of Al3+ substituted Ni–Co ferrites prepared through sol–gel auto combustion method for high-frequency and microwave devices
This research focuses on the formation and assessment of sol–gel auto-combustion-produced nanocrystalline Co 0.40 Ni 0.6 Al x Fe 2−x O 4 (x = 0.00, 0.05, 0.1,...
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Phase Equilibrium in Solid Solutions of BaTiO3 Doped with Eu3+ and Gd3+
Barium titanate is an ABO3 type perovskitePerovskite of great interest due to its magnetic, dielectric, piezoelectric, and thermal properties, among... -
Dynamic electric, modulus and impedance study of Ni0.5Cu0.2Cd0.3Fe2-zAlzO4 nanoparticles with magnetization and Rietveld analysis
The ferrite nanoparticles of Ni 0.5 Cu 0.2 Cd 0.3 Fe 2-z Al z O 4 (0.00 ≤ z ≤ 0.075 with step 0.015) were synthesized with popular sol–gel method and their...