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Article
Synthesis and characterization of BaSn(OH)6 and BaSnO3 acicular particles
The synthesis of BaSn(OH)6 acicular crystals by precipitation at 100 °C from aqueous solutions and their transformation in the perovskitelike compound BaSnO3 was investigated. Single acicular crystals 100–200 μm ...
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Article
Effect of Isovalent Ba-Site Substitutions on the Properties of (Ba1 – x – y M y Y x )TiO3(M = Ca, Sr, Pb) PTCR Ceramics
An approach is proposed for fabricating fine-grained, low-resistivity BaTiO3-based PTCR ceramics via partial isovalent substitutions on the Ba site. The grain size of the ceramics thus prepared is shown to decrea...
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Article
Formation and decomposition of the rutile-type compound FeSbO4
The reaction between Fe2O3 (hematite) and Sb2O3 leading to the formation of the rutile-type compound FeSbO4 was analysed by means of DTA and TG, performed under various O2 partial pressures up to 1673 K. The reac...
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Article
Synthesis, sintering and expansion of Al0.8Mg0.6Ti1.6O5: a low-thermal-expansion material resistant to thermal decomposition
A low-thermal-expansion ceramic with the composition Al0.8Mg0.6Ti1.6O5 that is isostructural to aluminium titanate Al2TiO5, was prepared by solid-state reaction of a mixture of α-Al2O3, MgO and TiO2-rutile. Th...
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Article
Decomposition of Al2TiO5-MgTi2O5 solid solutions: a thermodynamic approach
The decomposition of Al1−xMgxTi1+xO5 solid solutions with x=0.0, 0.1, 0.2, 0.4, 0.5 and 0.6 was studied in the temperature range 900–1175 °C using a 250 h annealing test. As x increases from 0–0.2 there is a stro...
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Article
Low-temperature aqueous synthesis (LTAS) of ceramic powders with perovskite structure
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Article
The effect of MgAl2O4 on the formation kinetics of Al2TiO5 from Al2O3 and TiO2 fine powders
The formation of Al2(1−x)MgxTi(1+x)O5 solid solutions from Al2O3-TiO2-MgAl2O4 powder mixtures of ≈1 μm particle size and moderate purity has been studied at 1300°C for different final composition values: x=0 (“pu...