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Article
Synthesis and characterization of BaSn(OH)6 and BaSnO3 acicular particles
The synthesis of BaSn(OH)6 acicular crystals by precipitation at 100 °C from aqueous solutions and their transformation in the perovskitelike compound BaSnO3 was investigated. Single acicular crystals 100–200 μm ...
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Article
The preparation of porous perovskite membranes using BaTiO3 nanopowders
The aim of this study was to develop a simple and reliable procedure in order to prepare composite membranes through the deposition of thin porous layers of perovskite-like oxides onto ceramic porous supports....
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Article
Synthesis, sintering and expansion of Al0.8Mg0.6Ti1.6O5: a low-thermal-expansion material resistant to thermal decomposition
A low-thermal-expansion ceramic with the composition Al0.8Mg0.6Ti1.6O5 that is isostructural to aluminium titanate Al2TiO5, was prepared by solid-state reaction of a mixture of α-Al2O3, MgO and TiO2-rutile. Th...
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Article
Decomposition of Al2TiO5-MgTi2O5 solid solutions: a thermodynamic approach
The decomposition of Al1−xMgxTi1+xO5 solid solutions with x=0.0, 0.1, 0.2, 0.4, 0.5 and 0.6 was studied in the temperature range 900–1175 °C using a 250 h annealing test. As x increases from 0–0.2 there is a stro...
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Article
Low-temperature aqueous synthesis (LTAS) of ceramic powders with perovskite structure
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Article
The effect of MgAl2O4 on the formation kinetics of Al2TiO5 from Al2O3 and TiO2 fine powders
The formation of Al2(1−x)MgxTi(1+x)O5 solid solutions from Al2O3-TiO2-MgAl2O4 powder mixtures of ≈1 μm particle size and moderate purity has been studied at 1300°C for different final composition values: x=0 (“pu...
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Article
Erratum: The transition from internal oxidation to continuous film formation during oxidation of dilute Ni-Si alloys
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Article
The transition from internal oxidation to continuous-film formation during oxidation of dilute Ni-Si alloys
The oxidation of Ni-2.05Si and Ni-4.45Si was studied in oxygen over the range of 600°–1000°C for 18 hr. The oxidation kinetics did not follow a parabolic rate law, bur rather a power law of the form (Δw)n=kt was ...
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Article
The corrosion of nickel in 1 atm of pure SO2 at 600–1000°C and the mechanism of formation of the two-layered scales
The reaction of pure nickel with 1 atm SO2 at 600–1000°C follows an irregular type of kinetics, tending to become parabolic at the highest temperature. The reaction rate tends to decrease with an increase of temp...
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Article
Oxidation of two-phase Co-54.86 wt.% Cu alloy at 700–1000°C
The oxidation in 1 atm of pure oxygen of a binary two-phase Co-Cu alloy has been studied as a simple example of the oxidation behavior of a multiphase alloy. The two-phase alloy oxidizes according to a parabol...
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Article
High-temperature oxidation of copper-manganese alloys
The oxidation behavior of copper-manganese alloys (2–35 wt. % Mn) in pure oxygen at 760 Torr was investigated at 100° intervals between 550 and 850°C. Gravimetric measurements of the oxidation kinetics have be.....