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  1. No Access

    Article

    Influence of Chemically Active Additives on the Nature of the Evaporation of Highly Volatile Impurities during Their Determination in Aluminum and Its Oxide by Arc Atomic Emission Spectrometry

    The effect of chemically active fluorine-containing additives AlF3, AgF, and ZnF2 on the nature of the evaporation of non-volatile elements, B, Be, Cr, Hf, Mo, Si, Ti, and V from aluminum oxide in a direct curren...

    N. I. Zolotareva, S. S. Grazhulene in Journal of Analytical Chemistry (2024)

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    Article

    Nanocomposites Based on Multi-Walled Carbon Nanotubes, Magnetite Nanoparticles, and Core–Shell Molecularly Imprinted Polymers in Piezoelectric Sensors for the Determination of Macrolide Antibiotics

    A piezoelectric sensor with a recognition layer based on magnetic carbon nanocomposites, including multi-walled carbon nanotubes, magnetic Fe3O4 nanoparticles, and polymer nanospheres with molecular imprints of e...

    E. V. Bizina, A. V. Efrosinina, O. V. Farafonova in Journal of Analytical Chemistry (2023)

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    Article

    Use of Magnetic Carbon Nanocomposites in the Formation of a Recognition Layer of a Piezoelectric Immunosensor for the Determination of Penicillin G

    Conditions for the formation of a recognition layer of a piezoelectric immunosensor based on magnetic carbon nanocomposites (MCNCs) under the action of an external magnetic field are studied. The effects of th...

    E. V. Bizina, O. V. Farafonova, N. I. Zolotareva in Journal of Analytical Chemistry (2023)

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    Article

    Behavior and Fractionation of Low-Volatile Impurities in a DC Arc in the Analysis of Zirconium by Atomic Emission Spectrometry

    We studied the effect of chemically active fluorine-containing additives AlF3, BaF2, and ZnF2 on the character of evaporation of some low-volatile elements from a refractory matrix in the crater of a DC arc elect...

    N. I. Zolotareva, S. S. Grazhulene in Journal of Analytical Chemistry (2023)

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    Article

    Adsorption Potential of a Magnetic Composite Based on Modified Carbon Nanotubes Synthesized Using Various Catalysts

    Using an example of the adsorption of Ag(I), Au(III), and Pd(II) ions from aqueous solutions, we studied the dependence of the adsorption capabilities of MNP@CNT magnetic adsorbents on the ratio of their compo...

    S. S. Grazhulene, N. I. Zolotareva, A. N. Redkin in Journal of Analytical Chemistry (2022)

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    Article

    A Piezoelectric Immunosensor Based on Magnetic Carbon Nanocomposites for the Determination of Ciprofloxacin

    A piezoelectric immunosensor with a recognition layer based on magnetic carbon nanocomposites is developed for the determination of ciprofloxacin. The receptor coating of the sensor is formed by the action of ...

    E. V. Bizina, O. V. Farafonova, N. I. Zolotareva in Journal of Analytical Chemistry (2022)

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    Article

    Using Chemically Active Additives for the Arc Atomic Emission Determination of Boron in Graphite

    We studied the effect of chemically reactive additives of AlF3, ZnF2, and SrF2 on the character of boron evaporation from a crater in a DC arc electrode in the analysis of graphite. The introduction of fluorinati...

    N. I. Zolotareva, S. S. Grazhulene in Journal of Analytical Chemistry (2021)

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    Article

    Sorption Properties of a Magnetic Composite Based on Modified Carbon Nanotubes: Influence of the Synthesis Conditions

    The performance of a magnetic composite sorbent consisting of magnetic nanoparticles and carbon nanotubes (CNTs) in sorption of toxic metal ions [Be(II), Bi(III), Cd(II), Cr(III)] was studied in relation to th...

    S. S. Grazhulene, N. I. Zolotareva, A. N. Red’kin in Russian Journal of Applied Chemistry (2020)

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    Article

    Magnetic Sorbent Based on Magnetite and Modified Carbon Nanotubes for Extraction of Some Toxic Elements

    Magnetic sorbent MNP@CNT was synthesized on the basis of magnetic nanoparticles of magnetite (MNPs) and carbon nanotubes (CNTs). The sorbent was studied in extraction of toxic elements from aqueous media and i...

    S. S. Grazhulene, N. I. Zolotareva, A. N. Red’kin in Russian Journal of Applied Chemistry (2018)

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    Article

    Microstructural investigations of sorption layers in mass-sensitive sensors for the detection of nitrogen-containing compounds

    The influence of the nature of sorption phases on the microweighing parameters of volatile organic compounds sorbed from gases and vapors is investigated using microstructural methods. The mechanism of interac...

    T. A. Kuchmenko, R. U. Umarkhanov in Journal of Surface Investigation. X-ray, S… (2014)

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    Article

    Study of correlations between the physicochemical properties of carbon nanotubes and the type of catalyst used for their synthesis

    It is found that carbon nanotubes (CNTs) obtained by the catalytic pyrolysis of ethanol vapor with Ni-, Co-, and Fe catalysts vary in their ability to oxidative modification and, finally, in adsorption capacity, ...

    S. S. Grazhulene, A. N. Red’kin, G. F. Telegin in Journal of Analytical Chemistry (2012)

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    Article

    Quartz crystal microbalance determination of vapors of volatile organic compounds on carbon nanotubes under batch conditions

    Specific features of the sorption of vapors of monoatomic aliphatic alcohols and aromatic compounds on coatings formed from carbon nanotubes of various genesis studied by the method of piezoelectric micro weig...

    Yu. Kh. Shogenov, T. A. Kuchmenko, S. S. Grazhulene in Journal of Analytical Chemistry (2012)

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    Article

    Broadening of linear dynamic range of photoelectric registration of emission spectra

    A method for broadening the linear dynamic range of measurements (LDRM) for a developed photoelectron system of registering emission spectra using series of charge-coupled devices (CCDs) was suggested. The met...

    Zh. P. Burmii, N. I. Zolotareva, V. A. Khvostikov, S. S. Grazhulene in Inorganic Materials (2011)

  14. No Access

    Article

    Laser-induced fluorescence monitoring of the gas phase in a glow discharge during reactive sputtering of vanadium

    Processes in the gas phase of a glow discharge during diode and magnetron reactive sputtering of vanadium in an Ar–O2 atmosphere have been investigated by laser-induced fluorescence (LIF) as a function of the par...

    V. A. Khvostikov, S. S. Grazhulene, Zh. P. Burmii in Journal of Applied Spectroscopy (2011)

  15. No Access

    Article

    Adsorption properties of carbon nanotubes depending on the temperature of their synthesis and subsequent treatment

    A correlation between the temperature of the synthesis of carbon nanotubes (CNT) by method of catalytic pyrolysis from ethanol on a nickel catalyst and their ability for the modification of oxidation under variou...

    S. S. Grazhulene, A. N. Red’kin, G. F. Telegin in Journal of Analytical Chemistry (2010)

  16. No Access

    Article

    Study of carbon nanomaterials as potential sorbents to concentrate admixtures in the atomic spectroscopy analysis methods

    Carbon nanomaterials (CNM) obtained by the catalytic pyrolysis of ethanol vapors are characterized with respect to their morphology, chemical purity, and sorption capacity. The efficacy of their usage to conce...

    S. S. Grazhulene, A. N. Red’kin, G. F. Telegin, N. I. Zolotareva in Inorganic Materials (2009)

  17. No Access

    Article

    Gaseous phase monitoring during reactive sputtering of yttrium in glow discharges

    The emission and fluorescence spectra at wavelengths of 580–650 nm during sputtering of yttrium, zirconium, and their alloys are studied for the purpose of develo** spectroscopic methods for monitoring the c...

    V. A. Khvostikov, S. S. Grazhulene in Journal of Applied Spectroscopy (2009)

  18. No Access

    Article

    Analytical Russian-German-Ukrainian symposium (ARGUS): History and main results of cooperation

    S. S. Grazhulene in Journal of Analytical Chemistry (2007)

  19. No Access

    Article

    State-of-the-art in analytical characterization of high purity solid samples by different spectroscopic methods

    Facilities and some results of several spectroscopic methods which have potential applications in the field of analysis of solid high purity substances and which have been elaborated in Russia, will be discuss...

    S. S. Grazhulene in Bulletin of Materials Science (2005)

  20. No Access

    Article

    Determination of Mercury by Nondispersive Atomic Fluorescence Spectrometry

    A nondispersive atomic fluorescence spectrometer for the determination of mercury by the cold-vapor technique has been developed. The conditions for mercury vapor generation in a hydride generator (the concent...

    V. A. Khvostikov, G. F. Telegin, S. S. Grazhulene in Journal of Analytical Chemistry (2003)

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