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Article
Open AccessIn-situ aerosol nanoparticle characterization by small angle X-ray scattering at ultra-low volume fraction
State-of-the-art aerosol nanoparticle techniques all have one feature in common: for analysis they remove the nanoparticles from their original environment. Therefore, physical and chemical properties of the p...
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Article
Open AccessAuthor Correction: Salt concentration and charging velocity determine ion charge storage mechanism in nanoporous supercapacitors
The original version of this Article contained an error in the Acknowledgements, which incorrectly omitted from the end the following: ‘The research leading to these results has received funding from the Europ...
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Article
Open AccessSalt concentration and charging velocity determine ion charge storage mechanism in nanoporous supercapacitors
A fundamental understanding of ion charge storage in nanoporous electrodes is essential to improve the performance of supercapacitors or devices for capacitive desalination. Here, we employ in situ X-ray trans...
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Article
Quantification of ion confinement and desolvation in nanoporous carbon supercapacitors with modelling and in situ X-ray scattering
A detailed understanding of confinement and desolvation of ions in electrically charged carbon nanopores is the key to enable advanced electrochemical energy storage and water treatment technologies. Here, we ...
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Article
Nucleation and growth of CdS nanoparticles observed by ultrafast SAXS
Aqueous solutions containing Cd2+ and S2- ions have been brought together in a T-mixer, and the formation of CdS nanoparticles has been monitored by ultrafast X-ray small angle scattering down to 0.2 ms. While no...
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Article
Probing hemoglobin confinement inside submicron silica tubes using synchrotron SAXS and electrochemical response
The configuration of hemoglobin in solution and confined inside silica nanotubes has been studied using synchrotron small angle X-ray scattering and electrochemical activity. Confinement inside submicron tubes...
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Article
X-ray lithography and small-angle X-ray scattering: a combination of techniques merging biology and materials science
The advent of micro/nanotechnology has blurred the border between biology and materials science. Miniaturization of chemical and biological assays, performed by use of micro/nanofluidics, requires both careful...
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Article
Time-resolved structure investigation with small angle X-ray scattering using scanning techniques
Due to the availability of high-brilliance X-rays at synchrotron radiation facilities, small angle X-ray scattering (SAXS) measurements have become feasible for new sample environments, like microfluidics or a...
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Article
Reconstitution of aluminium and iron core in horse spleen apoferritin
This study investigates the uptake of iron and aluminium by apoferritin. In particular, we provide the first evidence that apoferritin is able to bind in vitro the physiological form of aluminium, Al(OH)4 ...
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Article
Role of temperature-independent lipoplex–cell membrane interactions in the efficiency boost of multicomponent lipoplexes
Multicomponent lipoplexes have recently emerged as especially promising transfection candidates, as they are from 10 to 100 times more efficient than binary complexes usually employed for gene delivery purpose...
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Article
Time-resolved in-situ X-ray diffraction study of the formation of 3D-hexagonal mesoporous silica films
Highly oriented 3D-hexagonal silica thin films have been produced on silicon substrates by dip-coating technique, using cetyltrimethylammonium (CTAB) bromide as structuring agent. For the first time, time-reso...
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Article
Counterion condensation in ionic micelles as studied by a combined use of SANS and SAXS
We report a combined use of small-angle neutron scattering (SANS) and small-angle X-ray scattering (SAXS) to the study of counterion condensation in ionic micelles. Small-angle neutron and X-ray scattering mea...
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Article
A First Insight in the Mechanisms Involved in the Self-Assembly of 2D-Hexagonal Templated SiO2 and TiO2 Mesostructured Films During Dip-Coating
Since mesoporous materials can be prepared by combining the sol-gel chemistry and the structuring effect of surfactants, they have attracted attention for application in various high technology fields. The pre...
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Article
Industrial applications of the aggregation of block copolymers in supercritical CO2: a SANS study
Industrial applications of supercritical carbon dioxide (scCO2) rely upon the rather selective and easily adjustable solvent ability of CO2. CO2 near the critical point is a poor solvent for high molecular weight...
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Article
SAXS investigation on aggregation phenomena in supercritical CO2
Synchrotron Small-Angle X-Ray scattering (SAXS) measurements on aggregate formation of a Polyvinyl acetate-b-Perfluoro octyl acrylate (PVAc-b-PFOA) block copolymer in supercritical CO2 are here reported. Experime...
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Fragmentation in Large Strain Cold Rolled Aluminium as Observed by Synchrotron X-Ray Bragg Peak Profile Analysis (SXPA), Electron Back Scatter Patterning (EBSP) and Transmission Electron Microscopy (TEM)
In the last decade investigations of plastic deformation have focussed on the large strain ranges, i.e. stage IV and V of deformation [1–5]. Although several models have been developed to explain the work hardeni...
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Article
Contributory presentations/posters
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Nature of Irreversible Structural Changes Induced By Intense Light in Thylakoids. Small Angle X-ray and Neutron Scattering of Magnetically Aligned Chloroplasts
Earlier, by measuring light induced CD changes (ΔCD) in thylakoid membranes, it was shown that granal thylakoid membranes are capable of undergoing light induced reversible changes in their macrodomains posses...
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Chapter
Reconstitution of Membranes Using Non-Bilayer Forming Lipids and Plant LHCII
At the molecular level, the structure of the thylakoid membranes is quite complex: they contain specific mixtures of different lipid molecules and a large number of membrane proteins and their aggregates. Thyl...
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Studies on the 14.5 nm Meridional X-Ray Diffraction Reflection During Length Changes of Intact Frog Muscle Fibres
The intensity of the 14.5 nm meridional reflection (M3) from activated skeletal muscle fibres was studied in both single fibres and fibre bundles during the imposition of length changes. During shortening at s...