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Solid-Phase Microextraction
Sample preparation represents a pivotal stage within the analytical workflow. This chapter delves into the latest advancements in solid-phase...
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Determination of aliphatic aldehydes C1–C5 with headspace solid phase microextraction in tap water: derivatization in-solution versus on-fiber
Short-chain aliphatic aldehydes are hazardous environmental pollutants and important biomarkers of various diseases. The development of effective...
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Determination of Biomarkers in Multifloral Honey by Vacuum-Assisted Headspace Solid-Phase Microextraction
This paper focuses on the study of volatile and semi-volatile compounds of honey, using for the first-time vacuum-assisted solid-phase...
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Measurement of Distribution Constants Between Air and Solid Substrates Using Gas Chromatography for Quantification of Hydrocarbons in Solid Substrates via Headspace-Solid Phase Microextraction
This study focused on the chromatographic measurements of the distribution constants of hydrocarbons at the air–solid interface for indirect...
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A Device for the Simultaneous Cooling of the Fiber and the Evaporated Sample in the Determination of Pesticides from Soil Samples Using Fiber Headspace Solid-Phase Microextraction
AbstractPesticides are used to control agricultural and industrial pests, and even combat diseases such as malaria, posing a serious threat to public...
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Extraction and preconcentration of residual solvents from herbal medicines by headspace-micro solid phase extraction combined with deep eutectic solvent-based dispersive liquid–liquid microextraction
In this study, a headspace-micro solid phase extraction method combined with dispersive liquid–liquid microextraction was utilized in the extraction...
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Hollow-Fibre Liquid-Phase Microextraction
This chapter discusses microextraction using liquid membranes immobilized in a porous support membrane, including two- and three-phase hollow fibre...
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Single-Drop Microextraction
Since its discovery in 1995 by Dasgupta et al., and further implementation by Jeannot et al. in 1996, single-drop microextraction (SDME) has...
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Comparison of Gas Chromatography–Mass Spectrometry and Headspace-Solid phase Microextraction Methods for the Qualitative and Semi-Quantitative Determination of Aroma Compounds in Fruit-Based Spirits (Rakija) from Serbia
AbstractThe qualitative and semi-quantitative composition of aroma compounds in plum-, pear-, and quince-based spirits from Serbia was determined and...
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Analytical factors for eight short-chain fatty acid analyses in mouse feces through headspace solid-phase microextraction–triple quadrupole gas chromatography tandem mass spectrometry
This study developed a method for quantifying eight short-chain fatty acids (SCFAs) in mouse fecal samples using solid-phase microextraction (SPME)...
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Combination of headspace solid phase extraction with lighter than water organic solvent-based dispersive liquid-liquid microextraction for the extraction of residual solvents from herbal laxative medicine prior to gas chromatography-flame ionization detection
A combined headspace solid phase extraction-dispersive liquid–liquid microextraction method was developed for the extraction of residual solvents...
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Solid-Phase Microextraction as a Promising Tool for the Determination of Volatile Organic Components in Vinegar
AbstractVinegar is a widely used acidic condiment in the world with wide varieties and different flavors. Aroma can be used as an important factor to...
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Solid-Phase Microextraction and Comprehensive Two-Dimensional Gas Chromatography for Food Analysis
In this research protocol, we present helpful guidellines that could be adopted during food analysis, specifically during the development of...
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Synthesis of SiO2@MOF-199 as a Fiber Coating for Headspace Solid-Phase Microextraction of Phthalates in Plastic Bottled Milk
In this paper, SiO 2 @MOF-199 composite with core–shell structure was prepared by in-situ growth of MOF-199 on the surface of SiO 2 microspheres, and SiO
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Zeolitic imidazole framework-67 coated stainless steel fiber for solid-phase microextraction of some alcohols in alcoholic beverage samples
By a simple and low-cost method, zeolitic imidazole framework-67 was synthesized. It was used as a solid-phase microextraction coating. The...
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Solid-Phase Microextraction for the Quantification of Acetophenone Migrated to Air and Water from Toys and School Supplies
AbstractAcetophenone is a reagent used in various consumer products, including fragrance chemicals in toys and childcare products. Contact with...
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Ethane-bridge periodic mesoporous organosilica materials as a novel fiber coating in headspace solid-phase microextraction of phthalate esters from saliva and PET container samples
The current study presents a periodic mesoporous organosilica (PMO) with a high surface area and uniform-porosity material. The PMO materials were...
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Ordered mesoporous hairbrush-like nanocarbon assembled microfibers for solid-phase microextraction of benzene series in oilfield sewage
The development of advanced functional nanomaterials for solid-phase microextraction (SPME) remains an imperative aspect of sample pretreatment....
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Covalent Organic Framework/Reduced Graphene Oxide Composite for Solid-Phase Microextraction of Polycyclic Aromatic Hydrocarbons in Honey
A covalent organic framework/reduced graphene oxide composite (COF/rGO) was fabricated by facile ultrasonic self-assembly strategy and further coated...
