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Article
Ibrutinib related bleeding complications in elderly patients with B cell malignancies
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Article
Crystal and molecular structure of tetramethylammonium picrate
The synthesis and crystal and molecular structure of the tetramethylammonium picrate [C4H12N+C6H2N3O7] is reported. It belongs to the triclinic space groupP¯1 witha=7.300(3),b=9.797(2),c=10.841(3)Å,α=64.70(2),β=8...
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Article
Di-μ-sulphido-bis[4-methyl-piperidinedithiocarbamate tin(IV)]: Synthesis, characterization, and crystal and molecular structure
The title compound, C15H26SnN2S5Cl2, was prepared, and characterized by means of X-ray and IR measurements. The crystals are monoclinic, space groupP21/n, (non standard setting ofP21/c, No. 14) witha=12.330(2),b=...
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Article
1,4-Benzodiazepines as ligands. Synthesis, characterization and crystal and molecular structure ofbis(8-chloro-6-(o-chlorophenyl)-1-methyl-4H-s-triazolo[4,3-a]1,4-benzodiazepine (triazolam)) cadmium (II) dichloride
The compound C34H24CdN8Cl6 was prepared and characterized by means of X-ray, IR, and Raman measurements. The crystals are monoclinic, space groupC2/c, (No. 14) witha=22.284(3),b=14.501(2),c=14.595(2) Åβ=129.77(1)...
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Article
Structure, IR, and NMR spectra of tetrakis(4-methyl piperidinedithiocarbamate) dimercury(II)
The compound C14H24HgN2S4 was prepared and characterized by means of X-ray, IR, and NMR measurements. The crystals are monoclinic, space group P21/c, (No. 14) witha=8.697(2),b=19.156(3),c=12.098(2) Å,β=108.14(1)°...
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Article
Structural and spectral study of 7-bromo-1,3-dihydro-5-(2-pyridyl)-2H-1,4-benzodiazepin-2-one (bromazepam) platinum(II) dichloride bisdimethylsulfoxide
The synthesis and crystal and molecular structure of the title compound are reported. It belongs to the monoclinic space groupC2/c, witha=17.889(2),b=13.511(1),c=19.912(2) Å,β=99.841(4)°, andZ=8. The structure wa...
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Article
Structural and spectral study of 7-chloro-3-hydroxy-1-methyl-5-phenyl-1,3-dihydro-2H-1,4-benzodiazepin-2-one (temazepam)mercury(II) dichloride
The synthesis and crystal and molecular structure of the title compound is reported. It belongs to the monoclinic space groupP21/a witha=29.3990 (20),b=7.1150 (6),c=8.3140 (9) Å,β=98.060 (9)° andZ=4. The structur...
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Article
Transition metal complexes with 2-methyl-, 3-methyl-, and 4-methyl-piperidine dithiocarbamate as ligands
A new series of manganese(III), cobalt(II), nickel(II), zinc(II), cadmium(II) and mercury(II) complexes with monomethylsubstituted dithiocarbamates as ligands has been synthesized and studied. Their structures...
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Article
Cyclic substituted dithiocarbamates as ligands. Vanadium(III)and oxovanadium(IV, V) complexes
New vanadium(III) and oxovanadium(VI,V) dithio-carbamato complexes formulated as V(Rdtc)3, V(Rdtc)2Cl, VO(Rdtc)2, VO(Rdtc)Cl2, VO(Rdtc)2Cl and VO(Rdtc)3 (Rdtc = piperidine-, morpholine-, thiomorpholine- orN-methy...
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Article
Magnetic and thermogravimetric studies on copper(II) heterocyclicdithiocarbamates
A series of copper(II) dithiocarbamates of the type Cu(Rdtc)2, [Rdtc=piperidine- (Pipdtc), morpholine(Morphdtc), thiomorpholine- (Timdtc), piperazine- (Pzdtc) orN-methylpiperazine-dithiocarbamate (Me-Pzdtc)] has ...
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Article
The first example of a copper(II) chloride complex with 1,3-thiazolidine-2-thione
The reaction of copper(II) chloride with 1,3-thiazolidine-2-thione in absolute ethanol yields the complex CuL2Cl2. This derivative has been studied by elemental analyses, molar conductance, magnetic moment measur...
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Article
Spectroscopic techniques in the study of the nature of metal-ligand bonding in vanadium(III) and oxovanadium(IV,V) para -and metasubstituted benzeneseleninato complexes
Vanadium(III) and oxovanadium(IV,V) paraand metasubstituted benzeneseleninato-complexes, formulated as V(XC6H4SeO2)3, VO(XC6H4SeO2)2 and V2O2(XC6H4SeO2)3Cl3 (where X = H, m-Cl, p-Cl, m-Br, p-Br, p-CH3), have been...
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Article
Synthesis and characterization ofpara- andmeta-substituted benzeneseleninato complexes of tin(II), silver(I) and iron(II)
New complexes of tin(II), silver([) and iron(II) withpara- andmeta-substituted benzeneseleninic acids are reported and studied by chemical analyses, spectroscopic methods, conductivity and magnetic measurements. ...
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Article
Metal-ligand bonding in benzeneseleninato complexes of p- and d-block metals
New complexes of lead(II) and zirconium(IV) withmeta-andpara-substituted benzeneseleninic acids are reported and characterized by chemical analyses, spectroscopic methods and conductivity and magnetic measurement...
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Article
Study of the reactivity of some square planar nickel(II) carbodithioato derivatives towards ethylenediamine
Five-coordinate bis(carbodithioato)tris(ethylenediamine)-nickel(II) complexes are obtained by reaction of piperidine-, morpholine-4-, piperazine-4-,N-methylpiperazine-4-, and thiomorpholine-4-carbodithioato nicke...
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Article
The reactivity of areneseleninato complexes. New pentacoordinate nickel(II) complexes with benzeneseleninato ions and ethylenediamine as ligands
Five-coordinate bis(Se-benzeneseleninato)tris(ethylenediamine)nickel(II) complexes are obtained by reaction of the Ni(H2O)2(XC6H4SeO2)2 complexes (X = H,p-Cl,m-Cl,m-Br orp-Me) with ethylenediamine. All the diaquo...
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Article
Syntheses and spectroscopic studies on group IIB metal 1,4-benzodiazepine complexes
The preparation and characterization of some zinc(II) and cadmium(II) halide complexes with 1,3-dihydro-7-nitro-5-phenyl-2H-1,4-benzodiazepin-2-one and 7-chloro-l-methyl-5-phenyl-3H-1,4-benzodiazepin-2-one are...
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Article
Synthesis and characterization of rhodium(III), iridium(III), ruthenium(III) and osmium(III) complexes containing sterically hindered heterocyclic ligands
Some thiazolidine-2-thione and thiomorpholin-3-one complexes of rhodium(lll), iridium(III), ruthenium(III) and osmium(III) have been prepared and characterized by chemical analysis, conductivity measurements, ...
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Article
Iridium(III) hydride complex withm-chlorobenzeneseleninic acid
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Article
Five-coordinate low-spin cobalt(II) complexes with benzeneseleninato ions and ethylenediamine as ligands
Five-coordinate bis(benzeneseleninato)tris(ethylenediamine) cobalt (II)complexes are obtained by reaction of Co(H2O)2 (XC6 H4 SeO2)2 complexes (X = H, p-Cl, m-CI, p-Br, ni-Br, p-Me,p-NO2) with ethylenediamine. Th...
