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Article
Characterization and Crystal Structure of a Novel Mononuclear Cobalt(II) Complex with Hydrazone Derived from Protocatechuic Acid
A novel complex [CoII(L)2·CH3OH] with hydrazone derived from protocatechuic acid (HL=C16H14N2O4) is designed and synthesized. The complex is characterized by single crystal X-ray diffraction, elemental analysis, ...
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Article
Structure and urease inhibitory activity of copper(II) complex with (E)-3-(2,3-dihydrobenzo[b][1,4]dioxin-6-yl)acrylic acid
A new caffeic acid derivative ((E)-3-(2,3-dihydrobenzo[b][1,4]dioxin-6-yl)acrylic acid, HL1)) is synthesized from caffeic acid, followed by the preparation of a Cu(II) complex, [Cu2(L1)4DMSO2]·2DMSO. The structur...
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Article
Supramolecular structure of tetraaquabis[1-(carboxylatomethyl)-1,3-benzimidazol-3-ium-3-acetato-κO] Cadmium(II) dehydrate
A new complex, [Cd(C11H9N2O4)2(H2O)4]·2H2O, was synthesized and studied by X-ray diffraction analysis. The central Cd(II) atom lies on a crystallographic inversion center and is coordinated by four water molecule...
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Article
Chemical constituents from the roots of Senecio scandens
The chemical constituents of the roots of Senecio scandens Buch.-Ham. grown in the Funiu mountains in China have been investigated. Four compounds were isolated and identified as β−sitosterol (1), pentacosanoic a...
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Article
A new naphthoquinone and a new neolignan from Ligularia vellerea rhizomes
In the course of phytochemical investigations of Ligularia vellerea rhizomes, a new naphthoquinone, 2,5-dihydroxy-6,7-dimethylnaphthoquinone (1), and a new neolignan, 4-[(3',4'-dihydroxycinnamoyl)-oxy]methyl cinn...
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Article
A novel azide copper complex: [[Azido{bis[2-(piperidin-1-ylmethyl)pyridine]}copper(II)]perchlorate] hydrate
Synthesis and single crystal X-ray diffraction study were carried for compound {[Cu(C11H16N4)2(N3)](ClO4)} · H2O (I). The structure is molecular, and the Cu2+ ion is in a five-coordinated compressed trigonal bipy...
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Article
Study on the effect of mechanical alloying on properties of Zn-Sb alloy
The effect of mechanical alloying on Zn-Sb alloy system is investigated with X-ray diffraction (XRD), laser grain size analysis and differential scanning calorimetry (DSC) respectively. The results of laser pa...
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Article
Synthesis and characterization of radiation sensitive TiO2/monazite photocatalyst
A TiO2/monazite photocatalyst was prepared by embedding TiO2 nanoparticles into a monazite substrate surface. TiCl4 hydrolysis/citric acid chelating procedure under acidic conditions were used to synthesize the n...
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Article
Radiation effects on gaseous iodine at very low concentrations</p> </p>
Exploratory experiments have been carried out to investigate the effects of gamma-radiation on iodine aerosols under various chemical conditions. The results indicate that iodide ions (I-) in aerosol can be readi...
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Article
Multielement Analysis of Suspended Particulates Collected with a Beta-Gauge Monitoring System by ICP Atomic Emission Spectrometry and Mass Spectrometry
This work presents a two-step HNO3+HClO4/HF(1:2:1, v/v) acid mixture microwave digestion method for determining the elemental concentrations in suspended particulates collected on glass fiber filters by a beta-ga...
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Article
Rapid determination of90Sr by Compton suppression gamma-ray spectrometry
This work presents a low-level background gamma spectrometry system capable of achieving rapid determination of90Sr without chemical separation, in a soil sample when the90Sr to γ-ray emitting nuclide concentrati...
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Article
Assessment of Closed Vessel Digestion Methods for Elemental Determination of Airborne Particulate Matter by ICP-AES
Closed vessel acid digestion methods, especially the microwave digestion, have been investigated for elemental analysis of airborne particulates collected by glass fiber filter and analyzed by ICP-AES. A two-s...
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Article
Daily dietary intake of minor and trace elements by upper social groups in Taiwan
Sixteen minor and trace element contents of diet samples from three different social population groups in Taiwan were determined. Samples were prepared using duplicate portion technique by collecting the 15 su...
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Article
Mössbauer effect in YbBe13: Mixed valence and magnetic ordering
Mössbauer effect investigations on the cubic intermetallic compound YbBe13 in the temperature range between 0.065 K and 81 K are reported. Above the magnetic ordering temperatureT Neel=1.27 K the results cannot b...