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Determination of Rhodamine B by UV–Vis spectrophotometry in cosmetics after microextraction by using heat-induced homogeneous liquid–liquid extraction method

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Abstract

An environmentally friendly microextraction method which includes determination of trace levels of rhodamine B in cosmetic and detergent samples by using UV–vis spectrophotometric determination after enrichment with has been established heat-induced homogeneous liquid–liquid microextraction method. As extraction solvent, cyclohexylamine has been used, and the rhodamine B concentration in extraction phase was determined at 550 nm by using UV–vis spectrophotometry. The major parameters influencing in the method including pH, volume of cyclohexylamine, amount of NaCl, sample volume have been assessed. The influences of the matrix components were also investigated. The limit of detection, the limit of quantitation and linear range were found as 0.014, 0.047  and 0.047–4.79 μg mL−1, respectively. The relative standard deviation was 1.03%. The extraction procedure was applied to determination of rhodamine B in the cosmetic and detergent samples.

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Acknowledgements

The authors are grateful for the financial support of the Unit of the Scientific Research Projects of Erciyes University (TDK-2018-8318). The authors also thank to Erciyes University Technology Research and Application Center (ERU-TAUM) for instrumental facilities. Dr. Mustafa Soylak thanks to Turkish Academy of Sciences for financial support.

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Authors and Affiliations

  1. Faculty of Sciences, Department of Chemistry, Erciyes University, 38039, Kayseri, Turkey

    Zeliha Erbas & Mustafa Soylak

  2. Technology Research & Application Center (TAUM), Erciyes University, 38039, Kayseri, Turkey

    Zeliha Erbas & Mustafa Soylak

  3. Science and Technology Application and Research Center, Yozgat Bozok University, 66200, Yozgat, Turkey

    Zeliha Erbas

  4. Turkish Academy of Sciences (TUBA), 06670, Ankara, Cankaya, Turkey

    Mustafa Soylak

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  1. Zeliha Erbas
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  2. Mustafa Soylak
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Correspondence to Mustafa Soylak.

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This study is a part of PhD thesis of Zeliha Erbas.

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Erbas, Z., Soylak, M. Determination of Rhodamine B by UV–Vis spectrophotometry in cosmetics after microextraction by using heat-induced homogeneous liquid–liquid extraction method. J IRAN CHEM SOC 19, 3935–3942 (2022). https://doi.org/10.1007/s13738-022-02579-8

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  • DOI: https://doi.org/10.1007/s13738-022-02579-8

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