SpringerLink
Log in

Ultrasound-assisted deep eutectic solvent microextraction procedure for traces Ponceau 4R in water and cosmetic samples

  • Original Paper
  • Published:
International Journal of Environmental Science and Technology Aims and scope Submit manuscript

Abstract

A rapid, cheap and environmentally friendly DES-based LPME method for the determination of Ponceau 4R dye in real samples by UV–Vis spectrophotometry has been developed. Tetra-n-butylammonium bromide (TBAB) and decanoic acid (DA) were two components of DES solution used in the presented work. TBAB and DA were used to get DES. pH, DES type and volume, THF volume, ultrasonication and centrifuge time, sample volume and interfering effects, which are effective on the yield of the method, have been optimized. Ponceau 4R dye was extracted to the DES phase at pH 3.0. Limit of detection (LOD), limit of quantification (LOQ) and preconcentration factor were found as 5.97 µg/L, 18.1 µg/L and 40, respectively. The validation of the developed method was determined by addition recovery studies to water and cosmetic samples.

This is a preview of subscription content, log in via an institution to check access.

Access this article

Log in via an institution

Subscribe and save

Springer+ Basic
EUR 32.99 /Month
  • Get 10 units per month
  • Download Article/Chapter or Ebook
  • 1 Unit = 1 Article or 1 Chapter
  • Cancel anytime
Subscribe now

Buy Now

Price excludes VAT (USA)
Tax calculation will be finalised during checkout.

Instant access to the full article PDF.

Institutional subscriptions

Fig. 1
Fig. 2
Fig. 3
Fig. 4
Fig. 5
Fig. 6

Similar content being viewed by others

References

  • Abbey J, Fields B, O’Mullane M, Tomaska LD (2013) Food additives: colorants. In: Motarjemi Y (ed) Encyclopedia of food safety, vol 2. Hazards and diseases. Academic Press, pp 459–465

  • Abdolhosseini M, Shemirani F, Yousefi SM (2020) Poly (deep eutectic solvents) as a new class of sustainable sorbents for solid phase extraction: application for preconcentration of Pb(II) from food and water samples. Microchim Acta 187:602

    Article  CAS  Google Scholar 

  • Ahmadi S, Hamed Mosavian MT, Heydari S (2018) Response surface methodology for modelling and determination of catechin in Pistachio green hull using surfactant-based dispersive liquid–liquid microextraction followed by UV–Vis spectrophotometry. J Iran Chem Soc 15:2605–2614

    Article  CAS  Google Scholar 

  • ALOthman ZA, Habila MA, Yilmaz E et al (2020) A novel deep eutectic solvent microextraction procedure for enrichment, separation and atomic absorption spectrometric determination of palladium at ultra-trace levels in environmental samples. Measurement 153:107394

    Article  Google Scholar 

  • ALOthman ZA, Yilmaz E, Habila MA et al (2019) Supramolecular Solvent Microextraction and Ultra-performance Liquid Chromatography-Tandem Mass Spectrometry for Preconcentration and Determination of Malathion in Environmental Samples. Desalin Water Treat 144:166–171

    Article  CAS  Google Scholar 

  • Altunay N, Katin KP (2020) Ultrasonic-assisted supramolecular solvent liquid-liquid microextraction for determination of manganese and zinc at trace levels in vegetables: Experimental and theoretical studies. J Mol Liq 310:113192

    Article  CAS  Google Scholar 

  • Altunay N, Elik A, Gürkan R (2020) Preparation and application of alcohol based deep eutectic solvents for extraction of curcumin in food samples prior to its spectrophotometric determination. Food Chem 310:125933

    Article  CAS  Google Scholar 

  • Asheghhosseini A, Zolgharnein J (2020) Iron terephthalate metal–organic framework (MOF-235) as an efficient adsorbent for removal of toluidine blue dye from aqueous solution using Box-Behnken design as multivariate optimization approach. J Iran Chem Soc 17:2663–2673

    Article  CAS  Google Scholar 

  • Aydin F, Çakmak R, Levent A, Soylak M (2020) Silica Gel-Immobilized 5-aminoisophthalohydrazide: A novel sorbent for solid phase extraction of Cu, Zn and Pb from natural water samples. Appl Organomet Chem 34:5481

    Article  Google Scholar 

  • Bas SD, Gurkan R (2021) Selective extraction and enrichment of 5-hydroymethylfurfural from honey, molasses, jam and vinegar samples prior to sensitive determination by micro-volume UV-vis spectrophotometry. J Food Comp Anal 95:103664

    Article  CAS  Google Scholar 

  • Beyler-cigil A (2020) Preparation, characterization and adsorption into aqueous solutions of polyethyleneimine-coated silica nanoparticles. J Turk Chem Soc Sect A 7:883–892

    Article  CAS  Google Scholar 

  • Bisgin AT, Narin I, Ucan M, Soylak M (2015) A new cloud point extraction procedure for determination of trace amount crystal violet in wastewater by UV-VIS. Spectrometry Oxid Commun 38:232–240

    CAS  Google Scholar 

  • Erulas AF, Saylan M, Topal S et al (2020) A New Microextraction Method for Trace Nickel Determination in Green Tea Samples: Solventless Dispersion based Dispersive Liquid-Liquid Microextraction Combined with Slotted Quartz Tube- Flame Atomic Absorption Spectrophotometry. J Food Compos Anal 94:103623

    Article  CAS  Google Scholar 

  • Faraji M (2019) Determination of some red dyes in food samples using a hydrophobic deep eutectic solvent-based vortex assisted dispersive liquid-liquid microextraction coupled with high performance liquid chromatography. J Chromatogr A 1591:15–23

    Article  CAS  Google Scholar 

  • Filik H, Cengel T, Apak R (2009) Selective cloud point extraction and graphite furnace atomic absorption spectrometric determination of molybdenum (VI) ion in seawater samples. J Jazard Mater 169:766–771

    Article  CAS  Google Scholar 

  • Ghaedi M, Noormohamadi H, Asfaram A, Montazerozohori M, Tashkhourian J, Soylak M (2016) Modification of Platinum Nanoparticles Loaded on Activated Carbon and Activated Carbon with a New Chelating Agent for Solid Phase Extraction of Some Metal Ions. J Mol Liq 221:748–754

    Article  CAS  Google Scholar 

  • Harikrishnan R, Sundraraj K, Hui BY et al (2020) Vortex-assisted supramolecular-based dispersive liquid phase microextraction for spectrophotometric determination of rhodamine b in chili powder. Malaysian J Anal Sci 24:197–208

    Google Scholar 

  • Hassan M, Erbas Z, Alshana U, Soylak M (2020) Ligandless reversed-phase switchable-hydrophilicity solvent liquid–liquid microextraction combined with flame-atomic absorption spectrometry for the determination of copper in oil samples. Microchem J 156:104868

    Article  CAS  Google Scholar 

  • Huang J, Zeng Q, Wang L (2016) Ultrasensitive electrochemical determination of Ponceau 4R with a novel ϵ-MnO2 microspheres/chitosan modified glassy carbon electrode. Electrochim Acta 206:176–183

    Article  CAS  Google Scholar 

  • Kanberoglu GS, Yilmaz E, Soylak M (2019) Application of deep eutectic solvent in ultrasound-assisted emulsification microextraction of quercetin from some fruits and vegetables. J Mol Liq 279:571–577

    Article  CAS  Google Scholar 

  • Karatepe A, Akalin C, Soylak M (2017) Spectrophotometric determination of carmoisine after cloud point extraction using Triton X-114. Turkish J Chem 41:256–262

    Article  CAS  Google Scholar 

  • Khan S, Soylak M, Alosmanov RM et al (2018) Development of phosphate-containing polymer-based solid phase extraction procedure for the separation, enrichment, and determination of cadmium in water and food samples by FAAS. At Spectrosc 39:158–163

    Article  CAS  Google Scholar 

  • Li H, Zhao C, Tian H et al (2019) Liquid-Liquid Microextraction Based on Acid–Base-Induced Deep Eutectic Solvents for Determination of β-Carotene and Lycopene in Fruit Juices. Food Anal Methods 12:2777–2784

    Article  Google Scholar 

  • Li R, Wang Y, Tan J et al (2020) Simultaneous determination of synthetic edible pigments in beverages by titania-based RP-HPLC. Arab J Chem 13:3875–3881

    Article  CAS  Google Scholar 

  • Ma X, **e Y, Yu Y et al (2018) Three-dimensional β-cyclodextrin functionalized graphene aerogels: An enhanced electrochemical sensing platform for quantification of Ponceau 4R. J Electroanal Chem 823:437–444

    Article  CAS  Google Scholar 

  • Mehrani Z, Karimpour Z, Ebrahimzadeh H (2020) Using PVA/CA/Au NPs electrospun nanofiber as a green nanosorbent to preconcentrate and determine Pb2+ and Cu2+ in rice samples, water sources and cosmetics. New J Chem 44:15000–15009

    Article  CAS  Google Scholar 

  • Mendil D, Uluozlu OD, Tuzen M, Soylak M (2019) Multi-element determination in some foods and beverages using silica gel modified with 1-phenylthiosemicarbazide. Food Addit Contam - Part A Chem Anal Control Expo Risk Assess 36:1667–1676

    Article  CAS  Google Scholar 

  • Movaghgharnezhad S, Mirabi A, Toosi MR, Rad AS (2020) Synthesis of cellulose nanofibers functionalized by dithiooxamide for preconcentration and determination of trace amounts of Cd(II) ions in water samples. Cellulose 27:8885–8898

    Article  Google Scholar 

  • Salahuddin NA, El-Daly HA, El Sharkawy RG, Nasr BT (2018) Synthesis and efficacy of PPy/CS/GO nanocomposites for adsorption of ponceau 4R dye. Polymer 146:291–303

    Article  CAS  Google Scholar 

  • Sarafraz-Yazdi A, Amiri A (2010) Liquid-phase microextraction. TrAC-Trends Anal Chem 29:1–14

    Article  CAS  Google Scholar 

  • Sayar S, Ozdemir Y (1997) Determination of Ponceau 4R and tartrazine in various food samples by derivative spectrophotometric methods. Turk J Chem 21:182–187

    CAS  Google Scholar 

  • Soylak M, Altin R (2013) Determination of palladium in anodic slime and waste waters by flame AAS after preconcentration separation. Fresenius Environ Bull 22:2896–2900

    CAS  Google Scholar 

  • Soylak M, Karaca M (2016) Vortex Assisted Dispersive liquid-liquid microextraction of Pb(II) as 2-Hydroxypyridine-3-carboxylic Acid Chelates from Food and Water Samples prior to Flame Atomic Absorption Spectrometric Determination. At Spectrosc 37:108–113

    Article  CAS  Google Scholar 

  • Soylak M, Uzcan F (2020) A novel ultrasonication-assisted deep eutectic solvent microextraction procedure for tartrazine at trace levels from environmental samples. J Iran Chem Soc 17:461–467

    Article  CAS  Google Scholar 

  • Soylak M, Acar D, Alothman ZA (2017) Activated Carbon Cloth (ACC) as Efficient Adsorbent for Trace Cu(II), Co(II), Cd(II), Pb(II), Mn(II), and Ni(II) as 0-0-diethylphosphorodithioic Acid Chelates for the Enrichment From Water and Soil Samples. At Spectrosc 38:65–70

    Article  CAS  Google Scholar 

  • Soylak M, Gorucu HH, Yilmaz E (2020) Micelle-based restricted access ion-pair microextraction of phosphate at trace levels in water samples for separation, preconcentration and determination. EuroBiotech J 4:89–96

    Article  Google Scholar 

  • Tang W, Ho Row K (2020) Evaluation of CO2-induced azole-based switchable ionic liquid with hydrophobic/hydrophilic reversible transition as single solvent system for coupling lipid extraction and separation from wet microalgae. Bioresour Technol 296:122309

    Article  CAS  Google Scholar 

  • Unsal YE, Tuzen M, Soylak M (2015) Separation and Preconcentration of Sudan Blue II Using Membrane Filtration Method for UV-visible Spectrophotometric Detection of its in River Water Industrial Waste Water Samples. J AOAC Int 98:213–217

    Article  CAS  Google Scholar 

  • Unsal YE, Tuzen M, Soylak M (2019) Ultrasound-assisted ionic liquid-dispersive liquid–liquid of curcumin in food samples microextraction and its spectrophotometric determination. J AOAC Int 102:217–221

    Article  CAS  Google Scholar 

  • Vas G, Vékey K (2004) Solid-phase microextraction: A powerful sample preparation tool prior to mass spectrometric analysis. J Mass Spectrom 39:233–254

    Article  CAS  Google Scholar 

  • Vichapong J, Santaladchaiyakit Y, Burakham R, Srijaranai S (2020) Mixed micelle-mediated cloud point extraction coupled to spectrophotometry for fast screening of salbutamol in wastewater, pig feed and pork samples. Chiang Mai J Sci 47:542–553

    CAS  Google Scholar 

  • Wang Z, Zhang H, Wang Z et al (2015) Trace analysis of Ponceau 4R in soft drinks using differential pulse strip** voltammetry at SWCNTs composite electrodes based on PEDOT:PSS derivatives. Food Chem 180:186–193

    Article  CAS  Google Scholar 

  • Yalcin S, Apak R, Hizal J, Afsar H (2001) Recovery of copper (II) and chromium (III, VI) from electroplating-industry wastewater by ion exchange. Sep Sci Technol 36:2181–2196

    Article  CAS  Google Scholar 

  • Yang X, Sun D, Zeng R et al (2017) Trace analysis of ponceau 4R based on the signal amplification of copper-based metal-organic framework modified electrode. J Electroanal Chem 794:229–234

    Article  CAS  Google Scholar 

  • Yayayuruk O, Yayayuruk AE, Ozmen P, Karagoz B (2020) PDMAEMA grafted microspheres as an efficient adsorbent for the removal of Sunset yellow from pharmaceutical preparations, beverages and waste water. Eur Polym J 141:110089

    Article  CAS  Google Scholar 

  • Yi J, Zeng L, Wu Q et al (2018) Sensitive Simultaneous Determination of Synthetic Food Colorants in Preserved Fruit Samples by Capillary Electrophoresis with Contactless Conductivity Detection. Food Anal Methods 11:1608–1618

    Article  Google Scholar 

  • Zhang Y, Zhang X, Lu X et al (2010) Multi-wall carbon nanotube film-based electrochemical sensor for rapid detection of Ponceau 4R and Allura Red. Food Chem 122:909–913

    Article  CAS  Google Scholar 

  • Zhang J, Wang X, Zhang S et al (2014) An Electrochemical Sensor for Simultaneous Determination of Ponceau 4R and Tartrazine Based on an Ionic Liquid Modified Expanded Graphite Paste Electrode. J Electrochem Soc 161:453–457

    Article  Google Scholar 

  • Zhang J, Zhang S, Wang X et al (2015) Simultaneous determination of Ponceau-4R and Allura Red in soft drinks based on the ionic liquid modified expanded graphite paste electrode. Int J Environ Anal Chem 95:581–591

    Article  CAS  Google Scholar 

Download references

Acknowledgements

Syed Nasrullah Shah is a thankful to the Scientific and Technological Research Council of Turkey 200 (TUBITAK) under “2221 (Postdoctoral fellow) Research Fellowship Programme for Foreign Citizens.” The authors are grateful of Erciyes University for providing facilities and good environment in the chemical laboratory.

Author information

Authors and Affiliations

  1. Department of Chemistry, Faculty of Sciences, Erciyes University, Kayseri, 38039, Turkey

    S. N. Shah, F. Uzcan & M. Soylak

  2. National Centre of Excellence in Analytical Chemistry, Universıty of Sindh, Jamshoro, 76080, Pakistan

    S. N. Shah

Authors
  1. S. N. Shah
    View author publications

    You can also search for this author in PubMed Google Scholar

  2. F. Uzcan
    View author publications

    You can also search for this author in PubMed Google Scholar

  3. M. Soylak
    View author publications

    You can also search for this author in PubMed Google Scholar

Corresponding author

Correspondence to M. Soylak.

Additional information

Editorial responsibility: Fatih ŞEN.

Rights and permissions

Reprints and permissions

About this article

Check for updates. Verify currency and authenticity via CrossMark

Cite this article

Shah, S.N., Uzcan, F. & Soylak, M. Ultrasound-assisted deep eutectic solvent microextraction procedure for traces Ponceau 4R in water and cosmetic samples. Int. J. Environ. Sci. Technol. 19, 189–196 (2022). https://doi.org/10.1007/s13762-021-03154-z

Download citation

  • Received:

  • Revised:

  • Accepted:

  • Published:

  • Issue Date:

  • DOI: https://doi.org/10.1007/s13762-021-03154-z

Keywords

Search

Navigation