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Article
Synthesis and characterization of organosoluble luminescent poly(amide-imide)s
Poly(amide-imide)s (PAIs) were synthesized from 9,9’-bis(4-aminophenyl)fluorene (APF) and different diimide-dicarboxylic acids (DIDA). The aromatic fluorene group is isolated by DIDA. The structure of the ...
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Article
Preparation of Polyimide-Silica Nanocomposites from Nanoscale Colloidal Silica
The polyamic acid (PAA) solutions were blended directly with a commercial nanoscale colloidal silica sol, and converted to polyimides (PIs)/silica nanocomposite films. Polyamic acid was prepared from the react...
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Article
Isothermal Crystallization of Poly(ethylene-co-glycidyl methacrylate)/Silica Nanocomposites
γ-Aminopropyltriethoxysilane was used to modify nano-size silica particles (A-Silica), and silanation was studied by 29Si and 13C CP MAS NMR. 3 wt % original silica (Silica) and modified silica (A-Silica) particl...
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Article
Non-isothermal Crystallization of Poly(ethylene-co-glycidyl methacrylate)/Silica Nanocomposites
Nano-sized silica particles were modified by γ-aminopropyltriethoxysilane and the modified and unmodified silica particles were then respectively compounded with poly(ethylene-co-glycidyl methacrylate) (PEGMA) in...
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Article
Unusual Thermal Degradation Behavior of PEGMA in Air at Different Heating Rates
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Article
Reactivity of Poly(amic acid) Isomers in Thermal Imidization
The reactivity of isomers of poly(amic acid) prepared from 4,4′-oxydianiline and pyromellitic dianhydride in thermal imidization was investigated both in solution and in solid state at 130°C. FT-NMR was the ma...