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  1. Article

    Promising New Salt of Oseltamivir

    A synthetic method for the promising new drug oseltamivir ethoxysuccinate is described in detail. Various conditions for obtaining the target substance are considered. Its complete physicochemical characterist...

    A. I. Kalashnikov, E. G. Sonina, D. A. Kulagina in Pharmaceutical Chemistry Journal (2021)

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    Article

    Synthesis and Analgesic Activity of 4,10-Bis((±)-5-Benzoyl-2,3-Dihydro-1hpyrrolo[1,2-a]Pyrrole-1-Carbonyl)-2,6,8,12-Tetraacetyl-2,4,6,8,10,12-Hexaazatetracyclo[5,5,03,11,05,9]Dodecane

    A method of preparing the potential analgesic substance 4,10-bis((±)-5-benzoyl-2,3-dihydro-1H-pyrrolo-[1,2-a]pyrrole-1-carbonyl)-2,6,8,12-tetraacetyl-2,4,6,8,10,12-hexaazatetracyclo[5,5,03,11,05,9]dodecane is des...

    D. A. Kulagina, S. V. Sysolyatin, A. I. Kalashnikov in Pharmaceutical Chemistry Journal (2021)

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    Article

    Nitrolysis of 2,6,8,12-tetraacetyl-4,10-dibenzyl-2,4,6,8,10,12-hexaazatetracyclo[5.5.0.03,11.05,9]dodecane

    Nitrolysis of 2,6,8,12-tetraacetyl-4,10-dibenzyl-2,4,6,8,10,12-hexaazatetracyclo-[5.5.0.03,11.05,9]dodecane results in the substitution of benzyl groups by the nitro groups with the formation of 2,4,6,8,10,12-hex...

    A. I. Kalashnikov, S. V. Sysolyatin, G. V. Sakovich in Russian Chemical Bulletin (2017)

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    Article

    Management of flight control for “ExoMars-2018” robotic interplanetary space station

    The article covers the current status of activities on development of “ExoMars-2018” robotic interplanetary space station in terms of SC Composite flight program, results of onboard systems interaction functio...

    A. E. Shirshakov, M. I. Artyukhov, Yu. V. Kazakevich in Solar System Research (2015)

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    Article

    Features of RadioAstron Mission Control

    Support means of the Spektr-R spacecraft flight and features of the Mission Control Center operation and spacecraft control are considered. Software for scheduling and preparing sessions of controlling and simula...

    V. V. Khartov, A. E. Shirshakov, M. I. Artyukhov, Yu. V. Kazakevich in Cosmic Research (2014)

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    Article

    A search for raw materials for the isolation of shikimic acid

    The content of shikimic acid in the vegetative parts of a number of plants growing in the Altai Territory has been studied. The greatest content of shikimic acid (about 1.5%) was found in the coniferous needle...

    D. V. Bochkov, S. V. Sysolyatin in Russian Journal of Bioorganic Chemistry (2013)

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    Article

    Principles of interaction of furazano-1,2,3,4-tetrazine-1,3-dioxide with organic solvents

    Physicochemical interactions of furazano-1,2,3,4-tetrazine-1,3-dioxide (F) with organic solvents are studied according to thermogravimetry and UV spectrophotometry. It is shown that the donor-acceptor interact...

    V. P. Zelenov, P. I. Kalmykov, A. I. Kalashnikov in Russian Journal of Physical Chemistry A (2013)

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    Article

    Facile method for the synthesis of oseltamivir phosphate

    A ten-step scheme for the preparation of an antiviral agent, ethyl (3R,4R,5S)-4-acetylamino-5-amino-3-(pent-3-yloxy)cyclohex-1-enecarboxylate phosphate, from (-)-shikimic acid was studied. The main parameters of ...

    A. I. Kalashnikov, S. V. Sysolyatin, G. V. Sakovich in Russian Chemical Bulletin (2013)

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    Article

    Synthesis of Betulin Derivatives: N’{N-[3-OXO-20(29)-Lupen-28-OYL]-9-Aminononanoyl}3-Amino-3-Phenylpropionic Acid

    A method for synthesizing N’-{N-[3-oxo-20(29)-lupen-28-oyl]-9-aminononanoyl}-3-amino-3-phenylpropionic acid, a compound that exhibited immunostimulating and antiviral activities, by adding the methyl ester of N-(...

    S. V. Sysolyatin, V. N. Surmachev, V. V. Malykhin in Pharmaceutical Chemistry Journal (2012)

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    Article

    Debenzylation of 2,6,8,12-tetraacetyl-4,10-dibenzyl-2,4,6,8,10,12-hexaazatetracyclo[5.5.0.03,11.05,9]dodecane

    The debenzylation of 2,6,8,12-tetraacetyl-4,10-dibenzyl-2,4,6,8,10,12-hexaazatetra-cyclo[5.5.0.03,11.05,9]dodecane by catalytic hydrogenolysis in a mixture of HCOOH with other RCOOH (R = Me, Et, Pri) is accompani...

    A. I. Kalashnikov, S. V. Sysolyatin, G. V. Sakovich in Russian Chemical Bulletin (2009)

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    Article

    Behavior of [1,2,5]oxadiazolo[3,4-e][1,2,3,4]tetrazine 4,6-dioxide in various media

    A behavior of [1,2,5]oxadiazolo[3,4-e][1,2,3,4]tetrazine 4,6-dioxide (1) in organic solvents and aqueous solutions of various acidity has been studied by UV spectrophotometry. Kinetic laws for the N,N′-dioxide 1 ...

    V. P. Zelenov, A. A. Lobanova, N. I. Lyukshenko in Russian Chemical Bulletin (2008)

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    Article

    Ferrous metallurgy in the German Democratic Republic

    M. A. Kovalevskii, A. I. Kalashnikov, I. I. Pashko, I. I. Osadchii in Metallurgist (1969)