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Article
Fabrication of c-axis oriented higher manganese silicide by a high-magnetic-field and its thermoelectric properties
We report the preparation and thermoelectric properties of oriented higher manganese silicide (HMS) with a composition of MnSi1.73 bulk. The grain alignment and densification were achieved by rotating high magnet...
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Article
Fabrication of c-axis oriented polycrystalline ZnO by using a rotating magnetic field and following sintering
We succeeded in fabricating c-axis (00l) oriented ZnO ceramics by using a rotating magnetic field and a subsequent sintering treatment. The degree of orientation in the green compact was about 0.5 along (00l) on ...
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Article
Liquid immersion technique coupled with infrared microscopy for direct observation of internal structure of ceramic powder compact, with alumina as an example
Infrared microscopy was applied to observe the internal structure of alumina powder compact, which was made transparent with an immersion liquid. It provided clear images of nonuniformity in the structure for ...
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Article
Characterization of processing pores and their relevance to the strength in alumina ceramics
Characterization of bulk defects was successfully accomplished in alumina with a transmission optical microscope. The characterization technique used is based on the fact that many ceramics are essentially tra...
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Article
Binder surface segregation during spray drying of ceramic slurry
Spray-dried granules were observed by a laser microscopy with the immersion liquid technique. The binder distribution in the granules was analyzed from light intensity profiles of the images. The results showe...
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Article
Complex beam epitaxy of metal oxide films
YBa2Cu3O7 films were prepared by the new deposition technique ”complex beam epitaxy”. In this technique, metal-EDTA complexes are evaporated by excimer laser ablation. The metal-EDTA complexes are decomposed by ...
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Article
Microstructure design of HIPed TiO2 ceramics for improved corrosion resistance
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Article
High strength, electrically conductive pore-free TiO2 ceramics made by hot isostatic pressing
A high-purity, single-phase TiO2 ceramic with high density, strength, and electrical conduction was developed as a key structural material for the production equipment of semiconductors. Green bodies were made of...
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Article
Change of internal/pore structure in alumina green body during initial sintering
A novel characterization method was applied to study the morphological changes of large pores in a ceramic green body during the early stage of densification at 1100°C for 1–64 h. Large processing pores were p...
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Article
Filter cake forming and hot isostatic pressing for TZP-dispersed hydroxyapatite composite
The combination of a filter cake forming process and hot isostatic pressing was applied to prepare hydroxyapatite composites containing dispersed tetragonal zirconia polycrystal (TZP) with high strength and to...
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Article
Effect of Applied Pressure of Hip on the Removal of Processing Void in Alumina Ceramics and the Resultant Improvement of Mechanical Property
Alumina ceramics prepared at various processing conditions were subjected to hot isostatic pressing (HIP) to remove processing-originated voids. Transmission optical microscope was used for characterizing void...
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Article
Direct Evidence on the Elimination of Pore by the Applied Pressure in Hot Isostatic Pressing of Alumina
Removal of natural pore during capsule hot isostatic pressing (HIP) and normal sintering were examined directly with the novel liquid immersion technique, which can reveal details of micro-structure and charac...
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Article
Direct observation of internal structure in spray-dried yttria-doped zirconia granule
Spray-dried yttria-doped zirconia granules were made transparent by immersion in a liquid and the internal structure was characterized using an optical microscope. This unique technique was found to be applica...
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Article
Hydrogen post-etching effect on CVD diamond film
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Article
Thermochemical etching effect on CVD diamond film in an oxygen atmosphere
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Article
Orientation of ZnO grains by pyroelectric charge-electrical field interaction
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Article
Effect of additives on the hot pressing of zinc sulphide
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Article
Synthesis of aluminium titanate-mullite composite having high thermal shock resistance
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Article
Electrical properties of high purity tin dioxide doped with antimony
The electrical conductivity of high purity tin dioxide doped with antimony was studied at temperatures of 900 to 1200° C and partial pressures of oxygen between 10−8 and 1 atm. For specimens having a dopant conce...
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Article
Electrical conductivity of yttria-stabilized zirconia single crystals
The electrical conductivities of YSZ single crystals with various compositions covering FSZ and PSZ regions were measured by a complex impedance method and a four-probe a.c. method. The conductivities changed ...