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Mechanism of the Decomposition of Hydrazine Monohydrate on Pd/Al2O3 Studied by in Situ IR Spectroscopy
AbstractPd-containing catalysts (1% Pd/Al 2 O 3 and 5% Pd/Al 2 O 3 ) supported on aluminum oxide were studied in the decomposition reaction of hydrazine...
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Applications of in-situ spectroscopic techniques towards CO2 electroreduction
In-situ experimental techniques have been widely applied to uncover the dynamic evolutions of both the structure of catalysts and the interfacial...
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Thermal behavior of natural stellerite: high-temperature X-ray powder diffraction and IR spectroscopy study
The thermal behavior of stellerite from the Savinskoye deposit (Transbaikalia, Russia), Ca 7.69 Na 0.25 K 0.06 (Si 56.24 Al 15.76 )O 144 ·53.39H 2 O, was...
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An end-to-end approach for single-cell infrared absorption spectroscopy of bacterial inclusion bodies: from AFM-IR measurement to data interpretation of large sample sets
BackgroundInclusion bodies (IBs) are well-known subcellular structures in bacteria where protein aggregates are collected. Various methods have...
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Effects of Instrumental Configuration, Sample Preparation, and Pretreatment on the IR spectra of Silicalite-1
Infrared spectroscopy (IR) is an important tool to investigate the structure of silicalite-1, but the reported spectra vary considerably depending on...
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Homogeneous nucleation in polyamide 66, a two-stage process as revealed by combined nanocalorimetry and IR spectroscopy
Nanocalorimetry and Fourier transform infrared (FTIR) spectroscopy are combined to measure the calorimetric properties and molecular spectra of the...
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Rapid and in-situ determination of epoxy equivalent weight of bisphenol-based epoxides by micro-Raman spectroscopy
The need for rapid, fast and nondestructive determination of the epoxy equivalent weight (EEW) of the resins was the underlying motivation to develop...
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Sample illumination device facilitates in situ light-coupled NMR spectroscopy without fibre optics
In situ illumination of liquid-state nuclear magnetic resonance (NMR) samples makes it possible for a wide range of light-dependent chemical and...
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Pd-Doped SSZ-13 for Low-T NOx Adsorption: an Operando FT-IR Spectroscopy Study
In this study, mechanistic aspects of NO adsorption/desorption over a home-made Pd/SSZ-13 passive NOx adsorber (PNA) catalyst are investigated....
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Surface Ir-Ti Alloy Formed via Strong Metal − Support Interaction over Ir/TiO2
The strong metal-support interaction and its chemical nature was examined over a Ir/TiO 2 catalyst, constructed by dispersing 2 nm Ir colloids on the...
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Investigation of the chemical changes and mechanism of the epoxy-amine system by in situ infrared spectroscopy and two-dimensional correlation analysis
A simple and effective method based on in situ infrared spectroscopy and two-dimensional (2D) correlation analysis was applied to research the...
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In situ/operando characterization techniques for electrochemical CO2 reduction
Utilizing CO 2 as a carbon feedstock for producing fuels and useful chemicals is attractive due to the advantages of being abundant, nontoxic, and...
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In Situ Green Generation of Palladium Nanoparticles on Reduced Graphene Oxide and Its Catalytic Activity for Suzuki Coupling Reactions
AbstractA novel in-situ route was developed to load palladium nanoparticles on the graphene oxide in this paper. Palladium ions was immobilized on...
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Infrared Spectroscopy for Quality Control of Chinese Medicines
Infrared spectra of solid, liquid, and gas samples can be measured without separation or extraction. Most organic and inorganic molecules can... -
In Situ Hydrothermal Technique Assisted Synthesis of Nano-Rod Shaped Iron Vanadate, Characterization and Visible Light Active Behaviour against Toxicant
AbstractContamination of water from the textile mills and natural contaminants has increased in recent decades, prompting the design of...
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Modulation in the electronic structure of Ir-rich shell on AuIr solid solution as OER electrocatalyst for PEM electrolyzer
The design of low-cost and high-performance anodic electrocatalyst is essential in proton exchange membrane water electrolysis (PEMWE) application....
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Direct detection of photo-induced reactions by IR: from Brook rearrangement to photo-catalysis
In situ IR detection of photoreactions induced by the light of LEDs at appropriate wavelengths provides a simple, cost-effective, and versatile...
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A simplified methodology: pH sensing using an in situ fabricated Ir electrode under neutral conditions
Herein, a simplified fabrication method for the producing of a pH-sensitive iridium electrode is developed. The in situ electrochemical fabrication...
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Comparison of covalent and in situ immobilization of Candida antarctica lipase A on a flexible nanoporous material
In this study, Candida antarctica lipase A, which has a unique applicability for the conversion of highly branched and bulky substrates, was...