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  1. Development of Liquid Chromatography-Mass Spectrometry (LC-MS) Method for Quantification of Broccoli Sulforaphane

    Sulforaphane (SFN) is an isothiocyanate and the product of the hydrolysis of glucoraphanin (GRA) by myrosinase. Broccoli is one of the rich sources...

    Ali Ali Redha, Hung T. Hong, ... Daniel Cozzolino in Food Analytical Methods
    Article Open access 02 November 2023
  2. Detection of lard adulteration in 3 kinds of vegetable oils by liquid chromatography–mass spectrometry with porous graphite carbon column

    Liquid chromatography‒mass spectrometry employing porous graphite carbon columns and an n-octane-isopropanol mobile phase was utilized for the...

    Can Gong, **ang-Ting Lu, ... Xu Xu in Analytical Sciences
    Article 06 April 2024
  3. Analysis of milk with liquid chromatography–mass spectrometry: a review

    As a widely consumed foodstuff, milk and dairy products are increasingly studied over the years. At the present time, milk profiling is used as a...

    Sebastian Imperiale, Ksenia Morozova, ... Matteo Scampicchio in European Food Research and Technology
    Article Open access 07 February 2023
  4. Quantification of Gabapentin, Lacosamide, Perampanel, Pregabalin, Rufinamide, and Vigabatrin in Serum Using Liquid Chromatography-Tandem Mass Spectrometry

    Antiepileptic drugs (AEDs) have been used to control epilepsy. More than 17 new AEDs, including gabapentin (GPN), lacosamide (LCM), perampanel (PER),...
    Eunbin Chong, Hyeonju Oh, ... Soo-Youn Lee in Clinical Applications of Mass Spectrometry in Drug Analysis
    Protocol 2024
  5. Determination of Methylphosphonic Acid and Alkyl Methylphosphonic Acid Esters in Soils by Liquid Chromatography–High-Resolution Mass Spectrometry

    Abstract

    A method has been optimized for simultaneous extraction of ethyl methylphosphonic acid ester (EMPA), isopropyl methylphosphonic acid ester...

    M. F. Vokuev, A. V. Braun, ... I. A. Rodin in Inorganic Materials
    Article 01 December 2023
  6. Detection of 41 Drugs and Metabolites in Urine with Internal Hydrolysis Control by Liquid Chromatography-Tandem Mass Spectrometry

    Regular monitoring of pain management and substance use disorder patients through urine drug screening is important for assessing patient compliance...
    Stephen D. Merrigan, Yifei K. Yang, ... Jessica M. Boyd in Clinical Applications of Mass Spectrometry in Drug Analysis
    Protocol 2024
  7. Determination of Hydrolytic Transformation Products of Sesquimustards in Water by High Resolution Liquid Chromatography/Mass Spectrometry

    Abstract

    An approach to the determination of five sesquimustard markers, namely, bis(2-hydroxyethylthio)methane (BHETM),...

    M. F. Vokuev, A. V. Braun, ... I. A. Rodin in Journal of Analytical Chemistry
    Article 01 December 2023
  8. Photoionization Features of Mobile Phase Components in Supercritical Fluid Chromatography–Mass Spectrometry

    Abstract

    Supercritical fluid chromatography with mass spectrometric detection (SFC–MS) represents a rapidly evolving analytical method that offers an...

    D. V. Ovchinnikov, S. A. Vakhrameev, ... D. S. Kosyakov in Journal of Analytical Chemistry
    Article 01 December 2023
  9. Analysis of Serum Estrogens Using High-Performance Liquid Chromatography–Tandem Mass Spectrometry Coupled to Differential Ion Mobility Spectrometry

    Abstract

    A new quantification method is proposed for the determination of serum estrone (E1), estradiol (E2), and estriol (E3) based on...

    V. A. Ioutsi, Yu. M. Panov, ... N. G. Mokrysheva in Journal of Analytical Chemistry
    Article 01 December 2022
  10. Mass spectrometry coupling of chip-based supercritical fluid chromatography enabled by make-up flow-assisted backpressure regulation

    This work introduces a novel microfluidic backpressure pressure control developed for chip-based supercritical fluid chromatography (chipSFC). The...

    Chris Weise, Johannes Fischer, Detlev Belder in Analytical and Bioanalytical Chemistry
    Article Open access 22 June 2024
  11. Improving predictions of compound amenability for liquid chromatography–mass spectrometry to enhance non-targeted analysis

    Mass-spectrometry-based non-targeted analysis (NTA), in which mass spectrometric signals are assigned chemical identities based on a systematic...

    Nathaniel Charest, Charles N. Lowe, ... Antony J. Williams in Analytical and Bioanalytical Chemistry
    Article 26 March 2024
  12. Determination of Treosulfan and Fludarabine in Plasma by Turbulent Flow Liquid Chromatography-Tandem Mass Spectrometry (TFLC-MS/MS)

    Treosulfan is a structural analog of the alkylating agent busulfan which has been shown in clinical trials to exhibit comparable myeloablative...
    Shelby M. Hutcherson, Ryan C. Schofield, Dean C. Carlow in Clinical Applications of Mass Spectrometry in Drug Analysis
    Protocol 2024
  13. Screening anabolic androgenic steroids in human urine: an application of the state-of-the-art gas chromatography-Orbitrap high-resolution mass spectrometry

    Over the past few decades, anabolic androgenic steroids (AASs) have been abused in and out of competition for their performance-enhancing and...

    Ziyi Ji, Lei Liao, ... **aojun Deng in Analytical and Bioanalytical Chemistry
    Article 04 April 2024
  14. Nitrogen stable isotope analysis of sulfonamides by derivatization-gas chromatography-isotope ratio mass spectrometry

    The continuous introduction of micropollutants into the environment through livestock farming, agricultural practices, and wastewater treatment is a...

    Qingyuan Dou, Aoife Canavan, ... Martin Elsner in Analytical and Bioanalytical Chemistry
    Article Open access 07 June 2024
  15. Determination of Volatile Metabolites in Vinegar by Stir Bar Sorptive Extraction–Gas Chromatography–Mass Spectrometry (SBSE–GC–MS)

    Stir bar sorptive extraction (SBSE) is a rapid, sensitive, precise, and environmentally friendly extraction technique that, coupled to gas...
    Enrique Durán-Guerrero, Remedios Castro in Mass Spectrometry for Metabolomics
    Protocol 2023
  16. Advances and key considerations of liquid chromatography–mass spectrometry for porcine authentication in halal analysis

    The halal food industries are rapidly expanding to fulfill global halal demands. Non-halal substances such as porcine proteins are often added...

    Kifayati Rosiyanti Dewi, Maya Ismayati, ... Sunghwan Kim in Journal of Analytical Science and Technology
    Article Open access 20 February 2023
  17. Sample Screening and Determination of 214 Veterinary Drug Residues in Food Using Chromatography–High-Resolution Mass Spectrometry

    Abstract

    A combination of sample screening and subsequent confirmatory detection of contaminants represents an optimal strategy for routine analysis...

    V. G. Amelin, O. I. Lavrukhina, ... L. K. Kish in Journal of Analytical Chemistry
    Article 27 February 2024
  18. Application of Bubbling Extraction Coupled to Gas Chromatography Mass Spectrometry in Food Analysis

    In recent years, occurrence of selective enrichment of organic matter and partial concentration of inorganic components by gaseous microbubbles in...
    Yuanji Gao, Lei He, ... Quan He in Mass Spectrometry for Food Analysis
    Chapter 2022
  19. Comprehensive Analysis of Pistachio (Pistacia vera L.) Hull Phenolics by High-Performance Liquid Chromatography-Diode Array Detection-Tandem Mass Spectrometry

    Pistachio hull, the by-product of pistachio processing, is a plant source rich in phenolic compounds with diverse biological activities that may...
    Chapter 2024
  20. Anthocyanin Identification and Quantitation by High Performance Liquid Chromatography Coupled with Mass Spectrometry (HPLC-MSn)

    Anthocyanins are considered the principal agent for wine’s intense color response for the first sensory sight assessed by the consumers, the...
    Maurício Bonatto Machado de Castilhos, Sergio Gómez-Alonso, Esteban García-Romero in Basic Protocols in Enology and Winemaking
    Chapter 2023
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