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Article
Battery-type NiMoO4@NiMoS4 composite electrodes for high-performance supercapacitors
A novel NiMoO4@NiMoS4/NF nanocomposite is facilely grown on nickel foam (NF) via hydrothermal reaction and high-temperature calcination methods. The NiMoO4@NiMoS4/NF possesses a specific nanorods@nanosheets core–...
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Article
Crosslinked polyaniline nanorods coupled with molybdenum disulfide on functionalized carbon cloth for excellent electrochemical performance
In this work, the binary nanocomposite of crosslinked polyaniline nanorods (CPANINRs) and molybdenum disulfide (MoS2) is first synthesized by in situ polymerization, and CPANINRs/MoS2 on functionalized carbon clo...
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Article
Fast and Sensitive Detection of Bisphenol A and 4-n-Octylphenol in Foods Based on a 2D Graphitic Carbon Nitride (g-C3N4)/Gold Nano-Composite Film
In this paper, graphite phase carbon nitride (g-C3N4) was prepared by one-step high temperature thermal decomposition method, and layered g-C3N4 was prepared by protonation with concentrated hydrochloric acid. Th...
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Article
Electrochemical Reaction Mechanism of Nitrofurazone at Poly-ACBK/GCE and Its Analytic Application
In this paper, an electrochemical sensor based on depositing acid chrome blue K on the surface of glassy carbon electrode was developed for detection of nitrofurazone. The obtained poly-ACBK film was character...
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Article
Electrochemical determination of 2,4,6-trinitrophenol using a hybrid film composed of a copper-based metal organic framework and electroreduced graphene oxide
A metal organic framework (MOF) of the type copper(II)-1,3,5-benzenetricarboxylic acid (Cu-BTC) was electrodeposited on electroreduced graphene oxide (ERGO) placed on a glassy carbon electrode (GCE). The modif...
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Article
Preparation of protonated, two-dimensional graphitic carbon nitride nanosheets by exfoliation, and their application as a fluorescent probe for trace analysis of copper(II)
Bulk graphitic carbon nitride (g-C3N4) was obtained by pyrolysis of urea at 600 °C. The material was then subjected to protonation and exfoliation to obtain strongly fluorescent g-C3N4 nanosheets. These nanosheet...
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Article
Electrochemical hydrogen peroxide sensor based on a glassy carbon electrode modified with nanosheets of copper-doped copper(II) oxide
A new electrochemical sensor for H2O2 was constructed by depositing copper doped CuO nanosheets on a glassy carbon electrode (GCE). The morphology and composition of the modified electrode were characterized via ...
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Article
A glassy carbon electrode modified with poly(anthranilic acid), poly(diphenylamine sulfonate) and CuO nano-particles for the sensitive determination of hydrogen peroxide
We report on a modified glassy carbon electrode (GCE) for sensing hydrogen peroxide (H2O2). It was constructed by consecutive electrochemical deposition of poly(anthranilic acid) and poly(diphenylamine sulfonate)...
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Article
Simultaneous analysis of three catecholamines by a kinetic procedure: comparison of prediction performance of several different multivariate calibrations
A rapid kinetic method for the simultaneous determination of levodopa, dopamine, and dobutamine was examined and developed. It was based on a consecutive reaction of a reduction of Cu(II) to Cu(I) by catechola...
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Article
Investigation of the pharmacokinetics and determination of certain cephalosporins in rabbit plasma by a kinetic spectrophotometric method with the aid of chemometrics
This paper describes a kinetic spectrophotometric method for simultaneous determination of three cephalosporin antibiotics, cephradine, cefaclor and cefixime, with the aid of chemometrics. The method relies on...
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Article
Discrimination of Chinese traditional soy sauces based on their physico-chemical properties
This work aimed to classify the categories (produced by different processes) and brands (obtained from different geographical origins) of Chinese soy sauces. Nine variables of physico-chemical properties (dens...
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Article
Simultaneous kinetic spectrophotometric determination of norfloxacin and rifampicin in pharmaceutical formulation and human urine samples by use of chemometrics approaches
A kinetic spectrophotometric method with aid of chemometrics is proposed for the simultaneous determination of norfloxacin and rifampicin in mixtures. The proposed method was applied for the simultaneous deter...
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Article
Fingerprint Analysis of Eucommia Bark by LC-DAD and LC-MS with the Aid of Chemometrics
Chromatographic fingerprints of 46 Eucommia Bark samples were obtained by liquid chromatography-diode array detector (LC-DAD). These samples were collected from eight provinces in China, with different geographic...
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Article
Spectrophotometric Determination of Europium, Terbium and Yttrium in a Perchloric Acid Solution by the Kalman Filter Approach
In the presence of perchloric acid, rare-earth elements of europium, terbium and yttrium at large concentrations have well-shaped absorption spectra in the ultraviolet region even without the addition of a chr...