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Article
Determination of trace amounts of vanadium: A ternary extraction and photometric method using N-salicylhydroxamic acid and thiocyanate
A new extractive photometric method has been developed for a binary complex of vanadium(V) with salicylhydroxamic acid, a bluish-violet complex at pH 3.0 and a violet ternary complex system with ammonium thioc...
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Article
Spectrophotometric determination of vanadium with disodium maleonitrile dithiolate
Vanadium(IV) forms a deep green complex with disodium maleonitrile dithiolate, in 0.05N sulphuric acid in 50 % acetonitrile solution, having maximum absorption at 580 nm. The colour system obeys Beer's law from 0...
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Article
Spectrophotometric determination of iron with chelidamic acid
Chelidamic acid forms with iron a complex at pH 5.8 to 8.5 having the maximum absorption at 460 nm. The metal to reagent ratio is 1∶3 and the instability constant is about 8.21 · 10−15. The complex obeys Beer's l...
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Article
Spectrophotometric determination of iron with β-aminopicolinic acid
β-Amino-picolinsäure bildet mit FeIII-Ionen einen Komplex, der bei 420 nm dem Beerschen Gesetz gehorcht, ein Verhältnis Metall: Reagens =1∶2 aufweist und eine Instabilitätskonstante von 3,764 · 10−8 besitzt. Mit...
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Article
Gravimetric determination of palladium with quinolinimide as a reagent
Quinolinimide which is found to be a selective reagent for palladium forms a complex of the composition Pd(C7H3O2N2)2. The reagent quantitatively precipitates palladium from solutions of pH 0.5 to 2.5 in presence...
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Article
Quinolinic acid as a reagent for the gravimetric and volumetric estimation of palladium
Like Β-amino-picolinic acid, quinolinic acid behaves as a highly selective reagent for palladium with which it forms a complex of composition Pd(C7H4O4N)2. The complex being very stable is precipitated from solut...
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Article
β-Aminopicolinic acid as a reagent for the gravimetric and volumetric estimation of palladium
β-Aminopicolinic acid has been used successfully as a very selective reagent for the precipitation of palladium as Pd(C6H5O2N2)2 from solutions 1.0 normal with respect to hydrochloric acid as well from solutions...