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Beneficiation of rock phosphate fertilisers by mechano-milling
Mechano-milling is a process where materials are ball-milled at high energy to induce chemical and physical reactions. This study investigated the effect of milling on the properties and agronomic effectivenes...
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Article
Mechanochemical Synthesis and Characterization of GaN Nanocrystals
A solid-state displacement reaction of Ga2O3 with Mg3N2 has been used to synthesize GaN nanocrystals by mechanochemical processing. X-ray diffraction, transmission electron microscopy (TEM) and selected area elec...
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Article
Investigation of a synthetic aluminosilicate inorganic polymer
A melt-quenched of mixture of alumina and silica (46 wt% Al2O3 or Al2O3(SiO2)2) was found to react with an alkaline silicate solution (Na2O)(SiO2)1.2(H2O)9.5) at low-temperatures to form a synthetic aluminosilica...
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Article
The ferromagnetic transition in MnAs synthesised by mechanical alloying and powder blending techniques
A study of the structure and properties of MnAs synthesized by mechanical alloying and powder blending techniques has been carried out. Mechanical alloying resulted in the formation of MnAs during milling. Fol...
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Article
Magnetization Reversal in Melt-Ouenched NdFeB
Melt-quenched NdFeB is an important modem permanent magnet material. However there still remains doubt as to the magnetization reversal mechanism which controls coercivity in material prepared by this processi...
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Microstructural evolution of Ni-NaCl mixtures during mechanochemical reaction and mechanical milling
The evolution of microstructure of Ni and NaCl mixtures formed by mechanochemical reaction and mechanical milling has been studied using X-ray diffraction, electron microscopy and magnetic measurements. Separa...
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Article
The fundamentals of mechanochemical processing
It has been demonstrated that the activation of chemical reactions by mechanical energy can lead to many interesting applications, ranging from waste processing to the production of advanced materials with nov...
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Article
Mechanically activated reduction of nickel oxide with graphite
The reduction of nickel oxide with graphite during ball milling at both ambient and elevated temperatures was investigated using X-ray diffraction (XRD), simultaneous thermogravimetry and differential thermal ...
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Article
Synthesis of CdS quantum dots by mechanochemical reaction
+ Na2S → CdS + 2NaCl induced by mechanical milling resulted in the formation of CdS particles with an average diameter of < 8 nm. The average particle size was controlled within the range of 4 to 8 nm by varying...
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Article
Effect of low temperature ageing on the transformation behaviour of near-equiatomic NiTi
A unique three-stage transformation behaviour on cooling has been observed in a Ti-50.2 at% Ni alloy after a low temperature ageing treatment. The cooling transformation in the aged alloy occurred as a three-s...
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Article
Destruction of toxic materials
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Article
Synthesis of titanium oxynitride by mechanical milling
The synthesis of a titanium oxynitride phase by mechanically milling elemental titanium powder in air at ambient temperature has been studied. X-ray powder diffraction, transmission electron microscopy and che...
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Reduction of tantalum chloride by magnesium during reaction milling
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Article
On the kinetics of mechanical alloying
The kinetics of solid-state displacement reactions during mechanical alloying have been investigated. The effects of charge ratio and ball size on the progress of the reaction between CuO and Fe have been eval...
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Synthesis of NdFeO3 by mechanical alloying
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Anomalous combustion effects during mechanical alloying
Combustion in solid-state displacement reactions during mechanical alloying has been investigated. It was found that mechanical alloying decreases the critical reaction temperature at which unstable combustion...
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Displacement reactions during mechanical alloying
The occurrence of simple solid-state displacement reactions during mechanical alloying has been investigated. The reduction of cupric oxide to pure copper metal by a variety of metallic reducing agents was stu...
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Combustion and resultant powder temperatures during mechanical alloying
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Cloud-reflected radiation
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Hydrostatic extrusion behaviour of high density polyethylene
The solid state processing of a high density polyethylene by hydrostatic extrusion at room temperature has been investigated. The extrusion pressure for a given extrusion ratio is found to depend on the pressu...