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Article
Heterometallic (Nickel, Titanium)-Containing Dimethylglyoximates as Precursors for Nickel Titanate Coating
Heterometallic (nickel, titanium) dimethylglyoximate (II) with a nickel : titanium ratio of 1 was synthesized from nickel(I) dimethylglyoximate and titanium tetrachloride TiCl4 in chloroform. Resulting complex II...
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Article
Behavior of Dopant Ions in the Solution Synthesis of Substituted Calcium Phosphates
The dependence of (Zn, Cu, Co, Ni, Mn)-substituted calcium phosphates on the synthesis method was studied. The phosphates were synthesized by precipitation from aqueous solution and by mechanoactivation-assist...
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Article
Composition and Structure of Mn/Sr-Cosubstituted Tricalcium Phosphate Prepared by Solid-State Synthesis
Unsubstituted tricalcium phosphate (TCP) and Mn/Sr-cosubstituted TCP have been prepared by solid-state synthesis at 1200°C. The synthesized compounds have been characterized by X-ray diffraction, IR spectrosco...
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Article
Composite Mineral–Polymer Materials with Cation-Substituted Calcium Phosphates
Powders of copper-, zinc-, manganese-substituted tricalcium phosphates (TCP) are synthesized; the composition and structure of the obtained compounds are studied. It is shown how copper, zinc, and manganese io...
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Article
Development of Methods for Determination of the Ag, Cu, Fe, and Zn Contents in Materials Based on Calcium Phosphate for Medical Purposes
Using inductively coupled plasma atomic emission spectrometry (ICP-AES) and atomic absorption spectroscopy (AAS), we developed methods that allow express determination of impurity elements (Ag, Cu, Fe, and Zn)...
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Article
Barium-Substituted Tricalcium Phosphate Ceramics
Barium-substituted tricalcium phosphates containing 0.43 and 4.28 wt % barium have been prepared via mechanochemical activation and precipitation from aqueous solutions, followed by calcination. We have determ...
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Article
Porous matrixes based on polyvinylpyrrolidone containing calcium phosphates for medical application
A number of materials based on biocompatible polymers (polyvinylpyrrolidone and sodium alginate) with hydroxyapatite and dicalcium phosphate dihydrate were developed. The properties of prepared materials were ...
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Article
Plasma-Sprayed Manganese-Containing Tricalcium Phosphate Coatings on Titanium
Manganese-substituted tricalcium phosphates (TCPs), Ca3(PO4)2, containing 0–1.49 wt % manganese have been prepared by heterophase synthesis using mechanical activation. The percentage of manganese has been determ...
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Article
Composite Materials Based on Polyvinylpyrrolidone and Calcium Phosphates for Medicine
Mineral-polymer composites based on PVP and hydroxyapatite (HA) are obtained by in situ deposition in solutions of polyvinylpyrrolidone (PVP). The composites are presented in the form of films of hydrogels. Du...
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Article
Synthesis and Properties of Manganese-Containing Calcium Phosphate Materials
We have studied manganese-containing calcium phosphates differing in manganese content and phase composition. At a manganese content of 0.15 wt %, the whitlockite content is ~90 wt % and the calcium pyrophosph...
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Article
Polymer Materials Containing Calсium Phosphates for Medicine: Part I. Methylcellulose and Starch Containing Calcium Phosphates (Review)
This review is devoted to methylcellulose and starch also to its composite materials with calcium phosphates for application in medicine. The techniques of manufacturing the composite materials from methylcell...
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Article
Polymer Materials Containing Calсium Phosphates for Medicine: Part II. Chitosan and Polyvinylpyrrolidone Containing Calcium Phosphates (Review)
The review deals with chitosan and polyvinylpyrrolidone and its composite materials with calcium phosphates for medical application. The approaches to obtain the composite materials from chitosan and polyvinyl...
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Article
Methylcellulose Films Partially Crosslinked by Iron Compounds
An original method is proposed for the production of methylcellulose-based film materials. The method is based on obtaining a homogeneous MC mixture with sodium alginate in an aqueous solution and subsequently...
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Article
Mineral–Polymer Composites Based on Hydroxyapatite and Polyvinylpyrrolidone for Medical Applications
Hydroxyapatite (HA)–polyvinylpyrrolidone (PVP) nanocomposites with the HA/PVP ratio of 3.6–14.5 were synthesized by chemical precipitation from solutions of calcium nitrate and ammonium hydrogen phosphate in a...
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Article
Porous Ceramics Based on Substituted Tricalcium Phosphates for Bone Tissue Recovery
The results of studies concerning ceramics made of substituted (silver, zinc, copper, iron) tricalcium phosphate (TCP) powders are presented. It is shown that the pores in the obtained ceramics are interrelate...
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Article
Porous Carbonated Hydroxyapatite Ceramics Obtained by the Original Method of “Ceramic Biscuit” for Medicine
Carbonated hydroxyapatite (CHA) owing to its chemical and phase composition that is similar to that of the inorganic component of native bone tissue is a promising material for reconstructive surgery to heal b...
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Article
Reinforcement of Brushite Cement Based on α-TCP by Rigid Polylactide Framework
Brushite cement obtained from α-Ca3(PO4)2 and orthophosphoric acid in the presence of Mg(H2PO4)2 with compressive strength of 18 MPa was armored with a framework with the Kelvin architecture made of polylactide b...
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Article
Tricalcium Phosphate Ceramics Doped with Silver, Copper, Zinc, and Iron (III) Ions in Concentrations of Less Than 0.5 wt.% for Bone Tissue Regeneration
Novel materials with a variety of properties, such as biocompatibility, antibacterial activity, interconnected porosity, and functionalities combined in one, are required for regenerative medicine. Porous β-tr...
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Article
Microstructure and properties of α-tricalcium phosphate-based bone cement
This paper examines the physicochemical properties and microstructure of brushite calcium phosphate cements possessing strength acceptable for application in surgery (15–20 MPa) and ensuring an optimal acidity...
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Article
Brushite cement based on β-TCP for orthopedics
The phase composition of brushite cement that is based on β-tricalcium phosphate (β-TCP) and monocalcium phosphate monohydrate (MCPM) is optimized. It is shown that an increase in the β-TCP/MCPM ratio from 1.0...