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Article
The defect evolution in 1-D shocked tantalum single crystals
Tantalum single crystals were impacted along [001], [011] and [111] using 1-D planar shock waves with pressures of 6.4 GPa, 15.4 GPa and 21.7 GPa. The defect structures generated have been characterised using ...
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Article
Three-dimensional analysis of dendrites via automated serial sectioning using a Robo-Met.3D
The dendrite morphologies of the cast nickel-based superalloy CMSX-4® (CMSX-4® is registered trademarks of the Cannon-Muskegon Corporation) and the austenitic stainless steel HP microalloy have been obtained via ...
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Article
The Effects of Prior Cold Work on the Shock Response of Copper
A series of experiments have been performed to probe the effects of dislocation density on the shock response of copper. The shear strength immediately behind the shock front has been measured using embedded m...
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Article
Anatomical explanations for the changes in properties of western red cedar (Thuja plicata) wood during heat treatment
Thermal treatment is an alternative to the chemical treatment in wood preservation, which has been used to some extent in improving timber quality. Despite the enormous works done so far on the effects of heat...
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Article
The Effects of a New Grain Boundary Phase in Ni-Al Alloy
In a ψ/ψ’ nickel-aluminum alloy, a new phase has been identified along grain boundaries by conventional transmission electron microscopy. This phase is identified to be of the C6Cr23 type structure with lattice p...
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Article
Nanoscale defects and microwave properties of (BaSr)TiO3 ferroelectric thin films
Thin film ferroelectrics may have important applications in microwave devices but in general have significantly worse properties than bulk material. This is principally because of secondary and point defects. ...
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Article
Microwave Phase Shifters: Epitaxial Growth by Pulsed Laser Deposition of Dielectric Ba0.5Sr0.5TiO3 Thin Films on MgO
Ba0.5Sr0.5TiO3 (BSTO) thin films were grown on (001) MgO using pulsed-laser deposition (PLD). The microstructures of in-situ and ex-situ annealed BSTO films were studied by X-ray diffraction and transmission elec...
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Article
Effect of carbon on microstructure and mechanical properties of a eutectoid β titanium alloy
The influence of carbon addition on the aging response of quenched Ti-13wt. % Cr has been investigated using hardness tests, tensile tests, optical microscopy, scanning electron microscopy, and transmission el...
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Article
Suzuki Segregation to Stacking Faults in a Cu-Si alloy
Field Emission Gun Transmission Electron Microscopy (FEG TEM) is used to measure solute atom segregation to stacking faults in a Cu- 7.15 at% Si alloy annealed at temperatures of 275oC, 400oC and 550oC. A highly ...
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Article
TEM characterisation of fatigue tested lamellar Ti-44Al-8Nb-1B
Detailed microstructural examination by TEM of fine-grained polycrystalline lamellar Ti-44Al-8Nb-1B after fatigue testing (R=0.1) at room temperature has been carried out. The operative slip systems were ident...
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Article
The Oxidation of NdFeB Magnets
The oxidation kinetics in air of a commercial NdFeB magnet have been investigated over the temperature range 335–500°C. The oxide microstructure has been characterized by SEM, XRD and cross-sectional TEM. The ...
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Article
Oxygen-stabilised partial amorphisation in a Zr50Cu50 alloy
Structural transitions on heating a ZrCu martensite prepared by induction melting and subsequent rapid cooling have been investigated by means of differential scanning calorimetry (DSC), electrical resistivity...
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Article
Microstructural characteristics of the eutectoid mixture Zr2Cu and Zr7Cu10
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Article
Incommensurate Structure in Al-rich TiAl Alloys
The microstructures of Ti-Al alloys in the range 56–62 at.% Al have been studied. These compounds consist of a basic L10 structure on which is superimposed an irrational modulation (Ti3Al5 related). This is incom...
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Article
Creep in Single Crystal Ni3AI
Single crystals of Ni3AI (1 at%Ta) with a compression axis of [123] were subject to creep at a stress of 550 MPa and a temperature of 520 °C. Slip trace and TEM microstructural observations reveal that primary oc...
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Article
Creep Deformation of a Fully Lamellar Gamma Based Titanium Aluminide Alloy
A complex two phase γ-TiAl alloy, Ti-47Al-lCr-1Mn-2Ta-0.2Si (at.%) in a fully lamellar condition, has been creep tested at a stress of 200MPa and a temperature of 700°C. This simulates the in-service operating...
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Article
Influence of Substrate Preparation on the Two-Stage MOCVD of CdTe on (001)GaAs
A TEM study of the initial nucleation layers for the two-step growth of CdTe on 2°-off (001) GaAs substrates by MOCVD is presented. When the substrates are degreased and etched in the usual manner, the initial...
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Article
Site Occupation of Excess Al Atoms in Off-Stoichiometric γ-Tial: Measurement of Debye-Waller Factors
In recent years, the determination of x-ray structure factors and hence the electron charge density distribution in TiAl has received considerable attention. Experimental assessment of electron charge densitie...
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Article
Defect Anisotropy in Movpe CdTe/GaAs
A cross-sectional TEM study of the defect structure in CdTe buffer layers grown on 2° off (001) GaAs substrates by MOVPE is presented. The nature and distribution of defects in the buffer layers are shown to b...
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Article
Antiphase Boundary Tubes in Ordered Intermetallic Compounds
TEM observations suggest the presence of edge-type strain fields around antiphase boundary tubes in deformed L12 compounds such as Ni3Al and Fe3Ge. The present paper aims at discussing the origin of these strain ...