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Article
Mesoporous Silica Gel Doped with Dysprosium, Lanthanum and Modified with Silver as a Catalyst for Selective Hydrogenation of a 1-Heptyne/1-Heptene Mixture
Mesoporous silica gel doped with dysprosium, lanthanum and modified with silver (Dy-Ag/MPS, La-Ag/MPS) was obtained by the template method. The physicochemical characteristics of the obtained catalyst were stu...
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Article
Subcritical Water Extracts of Japanese Kelp as a Potential Base for Functional Nutrition
The efficiency of extracting iodine and alginic acids from dry thalli of Japanese kelp (Saccharina japonica) with subcritical water at 130, 150, and 170°C in the dynamic extraction mode is determined. It is found...
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Article
Distribution and Structure of the Ice Complex of the Lena Delta Area
The study of distribution and cryogenic structure of the Ice Complex is necessary for identification of its genesis. The intermediate results of the Ice Complex exposures surveys in the Lena Delta area are pre...
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Article
The Formation of Dispersed Systems from Aqueous Extracts from Milk Thistle Fruits
The regularities of the formation of dispersed systems (DSs) from the extracts from milk thistle after extraction with water at 150, 200, and 250°C and 5 MPa in the dynamic mode are studied. The sizes of the p...
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Article
Catalytic Activity of the Autoclave Thermolysis Products of [Co(NH3)5Cl][PtCl4] in the Complete Oxidation of Propane and Their Morphology and Phase Composition
The catalytic phases containing highly dispersed platinum metal particles on large particles of mixed cobalt oxide were obtained from the binary complex [Co(NH3)5Cl][PtCl4] under hydrothermal conditions. The chem...
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Article
Investigation of Sorption Microsystems as Reference Samples of Volatile Organic Compounds
The technology of obtaining reference samples of volatile organic compounds using sorption microsystems is described. The most effective are 0.147–0.178 mm (80–100 mesh) polymer sorbents fractions, which provi...
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Article
Hydrothermal Synthesis of Platinum–Chromium Oxidation Catalysts on Metal Supports
Catalysts containing highly dispersed platinum metal particles in a matrix of chromium oxides with different degrees of oxidation on metallic supports were obtained using the hydrothermal decomposition reactio...
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Article
Evaluation of the Extraction Efficiency of Biologically Active Compounds from Chamomile Flowers (Chamomilla recutita R.) Grown in the Samara Region by Extractants in the Subcritical State
Extracts of biologically active compounds (BACs) from chamomile flowers grown in the Samara region produced by extraction with subcritical water, as well as aqueous ethanol solutions of various concentrations ...
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Article
Methods and Devices for the Preparation of Standard Gas Mixtures
A review of methods for the preparation of standard gas mixtures (SGMs) with the known concentrations of organic and inorganic gases and vapors is presented. The classification of methods is proposed and their...
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Article
Extraction of Biologically Active Compounds from Eucalyptus (Eucalypti viminalis Labill) Leaves by Subcritical Water and Water-Ethanol Mixtures
Extraction of biologically active compounds (BAC) from eucalyptus viminalis (Eucalypti viminalis Labill) leaves with subcritical water was conducted using a dynamic regime at temperatures of 120–200°C and pressur...
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Article
Preparation of Calibration Gas Mixtures by the Chromato-Desorption Method for Increasing the Accuracy of Quantitative Determination of Biogenic Pentane in Expired Air
The possibility of increasing the accuracy of preparing n-pentane calibration gas mixtures by using injection-type chromato-desorption microsystems is investigated. The possibility of obtaining calibration gas...
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Article
Determination of Arbutin in Vaccinium vitis-idaea L. Leaves
A reversed-phase HPLC method for quantitative determination of arbutin in leaves of cowberry (Vaccinium vitis-idaea L.) was developed. The optimal conditions for extracting arbutin from the plant raw material wer...
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Article
Chromatographic-Desorption Method for Preparing Calibration Gas Mixtures of Volatile Organic Compounds
This is a study of the feasibility of using chromatographic-desorption systems for preparing calibration gas mixtures containing microscopic amounts of volatile impurities of saturated, aromatic, and halogenco...
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Article
Planar microchromatographic columns for gas chromatography
The adsorption and selective properties of aluminum-based planar microcolumns filled with the Carbopack B adsorbent are studied. The effect of geometrical parameters of the columns on their chromatographic pro...
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Article
Evaluation of the efficiency of volatile organic compounds extraction from eucalyptus viminalis (Eucalypti viminalis Labill) using subcritical extractants
Bioactive compounds were extracted from Eucalyptus viminalis with subcritical water in the temperature range of 120–200°C under a pressure of 5 MPa, as well as with aqueous solutions of ethanol with different con...
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Article
Stationary phases deposition on the planar columns capillaries
One of the modern trends of chromatography is the miniaturization of the analytical equipment. A successful way to carry out miniaturization is to use planar technologies based on methods developed for the cre...
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Article
A gas chromatograph based on planar systems
A chromatographic system consisting of a microinjector with the volume of sampling loop 10 µL, a microchromatographic column with nanodisperse silica particles on a planar aluminum plate, and a catalytic combu...
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Article
The Dynamic Characteristics of a Thermal Conductivity Microdetector for Gas Analyzers
The dynamic characteristics of micro- and standard thermal conductivity detectors and flame-ionization detectors are compared. The dynamic characteristics are estimated from the time constant. It is shown that...
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Article
Improved approach towards synthesis of adamantane-1,3,5-triol
1-Adamantanol can be converted into adamantane-1,3,5-triol in the presence of N-hydroxylphthtalimide, cobalt(II) acetylacetonate, and manganese dioxide under oxygen atmosphere in glacial acetic acid.
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Article
Extraction of biologically active compounds from medicinal plant raw material by extractants in subcritical state
Extraction of biologically active compounds (BACs) from the medicinal-plant raw material “leaves of eucalyptus viminalis” (Eucalypti viminalis Labill) was performed by traditional methods, by sub-critical water a...