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Hydrothermal Synthesis and Characterization of Two New Phosphatomolybdates(V) Containing Sandwich-Shaped [M(Mo6P4)2] Clusters (M = Co, Ni)
A new hybrid material, (H2dien)2(Hamimi)2[Co3Mo12O24(OH)6(HPO4)6(PO4)2]2 · nH2O (1) (n = 5.26), was hydrothermally synthesized via a simultaneous in situ cyclization of acetic acid and diethylenetriamine to 1-(2-...