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Biosynthesis and Characterization of Monodisperse Gold Nanoparticles using Mulberry Leaf Extract at Room Temperature

  • CHEMICAL PHYSICS OF NANOMATERIALS
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Russian Journal of Physical Chemistry B Aims and scope Submit manuscript

Abstract

In this research, spherical and small size gold nanoparticles were successfully prepared by a cost-effective, eco-friendly green approach using mulberry leaf extract as both reducing and stabilizing agent. The reducing potential of mulberry leaf extract was studied for the synthesis of gold nanoparticles without adding any external reducing agents. The formation of gold nanoparticles was confirmed by the change of color. The prepared gold nanoparticles were characterized by UV-visible absorption spectroscopy, dynamic light scattering, scanning electron microscope, transmission electron microscopy, fourier transform infrared and powder X-ray diffraction. The absorbance peak which found at 560 nm in UV-vis spectroscopy demonstrated the generation of gold nanoparticles. The fourier transform infrared elucidated that the gold nanoparticles were capped with various functional groups from extracts, kee** them from agglomeration and oxidation. The X-ray diffraction results illustrated that the particles were highly crystalline in nature. The transmission electron microscopy and scanning electron microscope showed the particles were small and spherical. The effect of reaction temperature, amount of chloroauric acid solution and extracts was also investigated. The results demonstrated that these parameters play vital roles in the production of gold nanoparticles.

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Funding

This work was supported by the Hubei Provincial Natural Science Foundation of China (2022CFD053), the Science and Technology Research Project of Hubei Provincial Department of Education (nos. D20194502 and B2019226), Hubei Polytechnic University scientific research project (19XJK02Z and 19XJK02Y), Science and Technology Foundation of Jiangxi Educational Committee (no. GJJ180701), and State Key Laboratory of Materials Processing and Die & Mould Technology in Huazhong University of Science and Technology (no. P2018-015). We also gratefully acknowledge the financial support of the Open Foundation of Hubei Key Laboratory of Mine Environmental Pollution Control and Remediation (2019102).

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Authors and Affiliations

  1. School of Mechanical and Electrical Engineering, Hubei Polytechnic University, 435003, Huangshi, P. R. China

    C. Dong, R. Fu & W. Chen

  2. School of Mechanical and Electrical Engineering, **gdezhen Ceramic Institute, 333403, **gdezhen, P. R. China

    S. Yu & W. Chen

  3. School of Mathematics and Physics, Hubei Polytechnic University, 435003, Huangshi, P. R. China

    X. Guo

  4. Hubei Key Laboratory of Intelligent Convey Technology and Device, Hubei Polytechnic University, 435003, Huangshi, P. R. China

    C. Dong & W. Chen

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  1. C. Dong
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  3. S. Yu
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Correspondence to C. Dong.

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Dong, C., Fu, R., Yu, S. et al. Biosynthesis and Characterization of Monodisperse Gold Nanoparticles using Mulberry Leaf Extract at Room Temperature. Russ. J. Phys. Chem. B 18, 599–606 (2024). https://doi.org/10.1134/S1990793124020064

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