Abstract
Solid phase extraction technique is a widely used sample preparation technique for the extraction of components from complex food matrices. However, there are several parameters in SPE that leads to low recovery, and reproducibility, insufficiently clean extracts and evaporation of volatile compounds. These drawbacks can be addressed through the use of innovative techniques and instrumentation that offers improved efficiency and accuracy for isolation of active constituents from food and beverage samples. Here a solid phase extraction methodology and extraction assembly has been developed for extracting compounds from orange fruit juice, followed by analysis using a LC-HRMS system. The methodology and assembly eliminate the evaporation step, thus facilitating the analysis of wide range of volatile and non-volatile compounds without the risk of their evaporation, making it particularly suitable for thermo-sensitive compounds. Also, the elute can be used for further analysis using LC-HRMS. The effectiveness of the designed extraction assembly and technique was demonstrated by comparing the procedure with the available conventional extraction assemblies, highlighting the advantages of the developed method.
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The data sets generated and analyzed during the study are available from the corresponding author upon reasonable request.
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Funding
The authors are thankful to the Director, CSIR-Indian Institute of Toxicology Research, Lucknow for providing necessary facilities. This work was supported by the Council of Scientific and Industrial Research, India (HCP-031).
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Pawankumar Rai: Conceptualization, Methodology, Experimentation, Writing—original draft, Formal analysis; Srishti Mehrotra: Methodology, Experimentation, Writing—original draft, Formal analysis; Vaibhavi Lahane: Part of the analysis, writing, and experiment; Akhilesh K. Yadav: Part of the analysis and writing; Sandeep K Sharma: Conceptualization, Methodology, Resources, Supervision, Writing—review & editing.
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The work was approved by scientific ethical committee of CSIR-IITR with a communication number: IITR/SEC/MS/2023/47.
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Rai, P., Mehrotra, S., Lahane, V. et al. Development of a positive pressure-based instrumentation for efficient solid phase extraction. J Food Sci Technol (2024). https://doi.org/10.1007/s13197-024-06010-3
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DOI: https://doi.org/10.1007/s13197-024-06010-3