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    Detection of a thermally unstable intermediate in the Wittig reaction using low-temperature liquid secondary ion and atmospheric pressure ionization mass spectrometry

    The signal of an extremely air sensitive and thermally unstable intermediate, four-membered ring oxaphosphetane in the Wittig reaction was detected for the first time at subambient temperature using liquid sec...

    Chin-Hsiung Wang, Min-Wen Huang… in Journal of the American Society for Mass S… (1998)