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Article
Reaction of 4-iminothiazolidin-2-one with acetylacetone
By the reaction of acetylacetone and arylazoacetylacetones with 4-iminothiazolidin-2-one thiazolo[4,5-b]pyridines were obtained in good yields. Optimum reaction conditions were chosen and some properties of compo...
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Article
Reaction of 4-iminothiazolidinone-2 with acetoacetic ester
The reaction of 4-iminothiazolidinone-2 with acetoacetic ester and its alkyl and aralkyl derivatives gives derivatives of thiazolo-[4,5-b]pyridine, which form salts with alkalis and are acylated.
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Article
Azolidine-4-thiones, their derivatives and analogs
4-Thioxothiazolid-2-one (isorhodanine) is distinguished from the initial thiazolidine-2,4-dione, and also from rhodanine and other azolid-4-ones, by the highly active C=S group in position 4. When isorhodanine...
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Article
A study of azolidones and their derivatives
A study was made of the reaction of 5-alkylthiazolidindiones-2, 4 (I) with P2S5 in a medium of dioxane. 4-Thioxo-derivatives of compound I were obtained which readily react with ammonia and amines with the format...
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Article
Studies on azolidones and their derivatives
The action of a concentrated aqueous solution of ammonia on 4-thioxothiazolid-2-one has given an isomer of pseudothiohydantoin, 4-iminothiazolid-2-one (I). 5-Substituted derivatives of I have been obtained by ...
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Article
Investigation of methylene group hydrogen atom reactivity in some azolidines
UV specttoscopy is used to investigate the kinetics of formation of arylidenerhodanines from rhodanine and various aromatic aldehydes whose benzene ring substitutents differ in nature and position. Hammett's e...
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Article
4-Thiazolidines, derivatives and analogs
In order to prepare isomers of 5-arylidene derivatives of rhodanine, 4-thione-1, 3-thiazolid-2-one (isorhodanine) is condensed with aromatic aldehydes and furfural. The reaction takes place when the reactants ...
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Article
4-Thionazolidones, derivatives and analogs
A hitherto unknown isomer of rhodanine, 4-thiothiazolid-2-one (isorhodanine), is prepared by boiling thiazolidine-2, 4-dione with P2S5 in anhydrous dioxane for 3 hr. Isorhodanine I is characterized by great react...
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Article
Study of the reactivity of the methylene hydrogen atoms of some azolidines. III. Kinetics of the reaction of azolidones-4 with benzaldehyde
UV spectroscopy is used to study the kinetics of formation of 5-benzylideneazolidones-4. The reaction is shown to be irreversible and follows a second-order equation. The effect of various hetero atoms (sulfur...