-
Article
Structural characterization of dicyanidobis-(N,N′-dimethylthiourea-κS)cadmium(II)
A cadmium(II) complex dicyanidobis(N,N′-dimethylthiourea-S) cadmium(II) [Cd(Dmtu)2(CN)2] (1) is prepared and its structure in the solid state is determined by single crystal X-ray structural analysis. The cadmium...
-
Article
Synthesis, spectral and thermal studies of zinc(II) and mercury(II) complexes with bidentate Schiff-base ligand (234-MeO-Ba)2En: the crystal structure of Zn(234-MeO-Ba)2En)I2
New Symmetric bidentate Schiff-base ligands N,N′-bis(2,3,4-trimethoxybenzylidene)-1,2-di-aminoethane, (234-MeO-Ba)2En, and its corresponding zinc(II) and mercury(II) complexes, Zn((234-MeO-Ba)2En)I2 (I), Hg((234-...
-
Article
Synthesis and crystal structure of new one-dimensional copper(II) complex [Cu4(En)2(μ1,1-N3)4(μ1,1,1-N3)2(μ1,3-N3)2] n
A new polymer azido-bridged copper(II) complex [Cu4(En)2(μ1,1-N3)4(μ1,1,1-N3)2(μ1,3-N3)2] n (I) (En = ethylenediamine) has been synthesized and crystallography characterized. Co...
-
Article
Structural characterization of a cadmium(II)-sulfato complex, [Cd(N,N′-diethyl thiourea)4(SO4)]
A cadmium(II) complex, tetrakis(N,N′-diethylthiourea)sulfatocadmium(II), [Cd(Detu)4SO4] (1) is prepared and its crystal structure is determined by X-ray crystallography. The crystal structure of the complex consi...
-
Article
Crystal structure of dinuclear azide-bridged copper(II) complex [Cu2((3,4-MeO-Ba)2En)2(μ1,1-N3)2(N3)2]{(3,4-MeO-Ba)2En=N,N′-Bis(3,4-dimethoxybenzylidene)-1,2-ethanediamine}
New dinuclear copper(II)-azido complex [Cu2((3,4-MeO-Ba)2En)2(μ1,1-N3)2(N3)2] (I) ((3,4-MeO-Ba)2En = N,N′-bis(3,4-dimethoxybenzylidene)-1,2-diaminoethane) has been synthesized and characterized by elemental analy...
-
Article
Crystal structures of three complexes structurally similar to KTbW(CN)8 · 7H2O
Three complexes that crystallize into structures like KTbW(CN)8 · 7H2O (triclinic crystal system, space group P $$ \ba...
-
Article
Crystal structure of a silver(I) complex {[Ag(N-methylthiourea)2]NO3} n exhibiting infinite chains of AgS4 tetrahedra
A polymeric silver(I) complex, bis(N-methylthiourea)silver(I) nitrate, {[Ag(Metu)2]NO3} n is prepared and its crystal structure is determined. The compound crystallizes in the m...
-
Article
Crystal structure of lanthanum potassium octacyanomolybdate(IV) nonahydrate
The crystal structure of KLaMo(CN)8 · 9H2O was determined from X-ray diffraction data. The crystals are monoclinic, space group P21/c, a = 8.7451(4), b = 25.2761(13), c = 10.6744(5) Å, β = 117.059(3)°, V = 2101.2...
-
Article
Synthesis, structural elucidation and X-ray analysis of triphenyltin(IV) [2-(2,3-dimethylanilino)nicotinate]
Triphenyltin(IV) [2-(2,3-dimethylanilino)nicotinate] was prepared by the interaction of triphenyltin(IV) hydroxide and 2-(2,3-dimethylanilino)nicotinic acid in 1:1 ratio. This compound was characterized by ele...
-
Article
Crystal structure of rubidium cobalticyanide
The crystal structure of Rb3[Co(CN)6] was determined by X-ray diffraction analysis. The crystals are monoclinic, space group P21/c, a = 7.163(2), b = 10.601(3), c = 8.675(3) Å, β = 107.83(2)°, V = 627.1(3) Å3, Z ...
-
Article
X-ray diffraction investigation of siloxanes. III. Structure and configuration of cyclic tetra-and pentasiloxanes bearing different organic substituents at silicon atoms
Single crystal X-ray diffraction is applied to elucidate the structures of six tetra-and one penta-siloxane compounds differing in the nature and position of silicon-sitting organic substituents (Me — methyl, ...
-
Article
X-ray diffraction investigation of siloxanes. I. Effects of organic substituents at the silicon atoms on the structure of acyclic trisiloxane-1,5-diols and on formation of different hydrogen bond systems
The molecular and crystal structure of four acyclic trisiloxane compounds, which differ in substituents at the silicon atoms (Ph-phenyl, mPh-methoxyphenyl, 2mPh-dimethoxyphenyl), was investigated by X-ray diff...
-
Article
X-ray diffraction investigation of siloxanes. II. Dependence of the structure of cyclic trisiloxanes on the nature of organic substituents at the silicon atom
The structure of six cyclic trisiloxane compounds with various combinations of carbon and oxygen-containing organic radicals Me, Ph, 2mPh, and 3mPh attached to the silicon atoms and lying in different position...
-
Article
Abstracts of short lectures