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Article
Synthesis and crystal structure of 3,10-dimethyl-10H-dibenzo[b,e]iodinium tetrafluoroborate
The crystal and molecular structures of a chiral cyclic iodonium salt, namely, 3,10-dimethyl-10H-dibenzo[b,e]iodinium tetrafluoroborate, is solved by the direct method (a = 20.678(5) Å, b = 20.738(5) Å, c = 8.408...
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Article
Structure of a new crystalline modification of 4-amino-5-ethoxymethyl-1,2-dimethylpyrimidinium iodide
The structure of a new crystalline modification (II) of 4-amino-5-ethoxymethyl-1,2-dimethylpyrimidinium iodide, C9H16IN3O, the major product of methylation of 4-amino-5-ethoxymethyl-2-methylpyrimidine has been de...
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Article
Crystal and molecular structure of the membrane-active antibiotic enniatin C
The crystal structure of the cyclic hexadepsipeptide antibiotic enniatin C c[-(L-MeLeu-D-Hyi)3-], C34H59N3O9, was established by X-ray structure analysis (sp. gr. P21, a = 20.205(5) Å, b = 8.702(2) Å, c = 25.587(...
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Article
Stereoisomerism of the matrine alkaloids
The stereoisomerism of compounds of the matrine series is considered on the basis of the authors' own x-ray structural studies of these alkaloids. A corrected series of eight stereoisomers has been drawn up. I...
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Article
Molecular and crystal structure of tetrahydroneosophoramine
The structure of tetrahydroneosophoramine has been studied by x-ray structural analysis. Rings A, B, and C have the chair conformation, and ring D the half-chair conformation. On the basis of a semiquantitativ...
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Article
Molecular and crystal structure of sophoridine N-oxide
The spatial structure of natural sophoridine N-oxide has been studied by x-ray structural analysis. It has been shown that when sophoridine is oxidized, rings B and C, which have the boat form, are deformed in...
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Article
Structure of isosophoridine
A complete x-ray study of the structure of a stereoisomer of the alkaloid matrine -isosophoridine - has been made. Rings A and B have the cis type of linkage. Rings A, B, and C have the chair form and D the ha...
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Article
Structure of tetrahydroneosophoramine
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Article
X-ray structural investigation of allomatrine and its N-oxide
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Article
Molecular and crystal structure of sophoridine
The three-dimensional structure of the alkaloid sophoridine C15H24ON2 has been studied by x-ray structural analysis; the parameters of the elementary cell are: a=5.458, b=10.640, c=11.989 Å; γ=99.7°; z=2; space g...
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Article
Dispersion of the optical rotation of derivatives of gramicidin S
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The dispersion of the optical rotation and UV absorption spectra of derivatives of gramicidin S with heavy at...
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Article
The crystal structure of the isomorphous dihalogeno-dipyridineates of cobalt and zinc