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Irreversible thermal transformation kinetics of halloysite to metahalloysite using XRD analysis
Dehydration of halloysite (Hly) to metahalloysite (m-Hly) was examined by X-ray diffraction (XRD). The Hly samples heated in temperature range of...
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Tracking Structural Deactivation of H-Ferrierite Zeolite Catalyst During MTH with XRD
We used the methanol-to-hydrocarbon (MTH) reaction as a shape-selective model reaction to investigate coke formation in zeolite H-Ferrierite. Despite...
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A Research into Chiral Thiosemicarbazide Compound: XRD Analysis, Hirshfeld Surface Analysis, and Energy Framework
AbstractThe present work combined single-crystal XRD analysis, Hisrhfeld Analysis, and energy framework analysis to interpret and comprehend the...
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Temperature Dependence of Electrical Conductivity and XRD Studies of Hydroquinone Modified Amberlite XAD-4 Resin
AbstractCommercial amberlite XAD-4 resin was modified with hydroquinone moiety through the azo spacer (–N=N–) technique and abbreviated as...
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Preparation and Characterization of Fe-Containing Aluminosilicate Phosphate Ceramic-Glass from a Geopolymer Precursor: Insights from XRD, Raman Spectroscopy, and Optical Properties
In this study, Fe-Al 2 O 3 -SiO 2 -P 2 O 5 (FASP) glass–ceramic was prepared by heating Fe-acid-based geopolymer at 1050 °C. The Fe-geopolymer was obtained by...
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XRD Characterization of Active Material β-Ni(OH)2 and AB5 Alloy
This chapter introduces the principle and method of X-ray diffraction characterization of positive and negative active material β-Ni(OH)2 and...
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Kinetics and Rietveld XRD structural study of Cs+ sorption on natural and synthetic mordenites in the first 12 h
Kinetics of Cs + uptake by natural and synthetic mordenites was studied. The experimental data is best fitted to the pseudo-second-order rate model...
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Preparation and XRD Analysis of Carbon Materials Used for Li-Ion Batteries
The preparation method of related carbon materials for lithium-ion battery was introduced, and the process of preparing carbon nanospheres with...
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Various crystalline phases of N-(2-hydroxy-4-methoxybenzylidene)-4′-n-butylaniline (OHMBBA) identified by a simultaneous measurement of DSC-XRD and DSC-Raman spectroscopy
The effect of precooling treatments on phase behaviors of N -(2-hydroxy-4-methoxybenzylidene)-4′- n -butylaniline (OHMBBA) was investigated by...
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Synthesis, Spectral, and Single Crystal XRD Studies of Novel Terpyridine Derivatives of Benzofuran-2-carbaldehyde and their Cu(II) Complex
AbstractA series of novel terpyridine derivatives of benzofuran (NP1–NP3) were synthesised by simple multicomponent one pot reaction among...
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Novel oxo–peroxo W(VI) Schiff base complex: synthesis, SC-XRD, spectral characterization, supporting on chloromethylated polystyrene, and catalytic oxidation of sulfides
A novel oxo–peroxo tungsten(VI) Schiff base complex, [WO(O 2 )L(CH 3 OH)], as a homogeneous catalyst for sulfoxidation was synthesized by treating WO 3 in...
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Synthesis of a Novel Dinuclear Ruthenium(III) Ono Pincer Complex Containing a M–M Bond: an XRD Study
AbstractA novel dinuclear ruthenium(III) ONO pincer complex was synthesized from RuCl 3 ·H 2 O and 2,6-pyridinedicarboxylic acid (H 2 pydc) in methanol by...
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TG, DSC, XRD, and SEM studies of the substituted lithium ferrite formation from milled Sm2O3/Fe2O3/Li2CO3 precursors
Formation of substituted lithium ferrite Li 0.5 Sm x Fe 2.5–x O 4 (where x = 0.06 and 0.2) from Sm 2 O 3 /Fe 2 O 3 /Li 2 CO 2 precursors was studied by X-ray...
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STRUCTURE OF THE IMMEDIATE ENVIRONMENT OF IONS IN ZINC CHLORIDE AQUEOUS SOLUTIONS ACCORDING TO XRD DATA
AbstractQuantitative characteristics of the immediate environment of ions in aqueous ZnCl 2 solutions are determined by XRD in a wide range of...
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Cu(II)(PhOMe-Salophen) Complex: Greener Pasture Biological Study, XRD/HAS Interactions, and MEP
AbstractPhOMe-salophen ( 1b ) (salophen is N , N -bis(salycilidene)-1,2-phenylenediamine with two tert- butyl on each ring) and Cu(II) complex with...
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Effects of crystallization temperature on the characteristics of sugar crystals in date fruit syrup as measured by differential scanning calorimetry (DSC), polarized microscopy (PLM), and X-ray diffraction (XRD)
Characteristics of sugar crystals are important for develo** set-syrup due to their contribution to the desired mouth feel when consumed. Two types...
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Effects of urea and glycerol mixture on morphology and molecular mobility in thermoplastic starch/montmorillonite-type nanofiller composites studied using XRD and NMR
Starch-based polymer systems have attracted a great deal of interest as a potential alternative to conventional plastics for packaging applications....
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XRD, PDF, AND EXAFS STUDY OF THE PHASE COMPOSITION AND LOCAL STRUCTURE OF SUPPORTED RUTHENIUM-CESIUM CATALYSTS
AbstractSupported catalysts Ru/MgO, Ru–Cs + /MgO, Ru/γ-Al 2 O 3 , and Ru–Cs + /γ-Al 2 O 3 are prepared by the impregnation method using RuOHCl 3 and Cs 2 CO 3 as...
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Ultrasound irradiation synthesis of novel copper(II) complex with the 2-thiophenimidazoline ligand: SC-XRD, HSA, and DFT study
A novel coordination CuCl 2 (L) 2 complex was synthesized by complexation of the 2-thiophenimidazoline ligand with CuCl 2 .2H 2 O in less than 10 min. The...
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Morpho/Opto-structural Characterizations and XRD-Assisted Estimation of Crystallite Size and Strain in MgO Nanoparticles by Applying Williamson–Hall and Size–Strain Techniques
Magnesium oxide (MgO) nanoparticles were fabricated at the ambient temperature by a chemical precipitation method. The as-synthesized nanoparticles...
