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NOAH
This final chapter describes my work on NOAH (NMR by Ordered Acquisition using...
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Identification of compounds using HPLC-QTOF-MS online antioxidant activity map** from aerial parts of Ligularia stenocephala
Inflammation, diabetes, and even malignancies are pharmacological effects connected by antioxidant capacity and free radicals. Many antioxidants...
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A New Anhydride of Alpinia officinarum
One new anhydride, alpinofficinol ( 1 ) was isolated from the rhizomes of Alpinia officinarum Hance (Zingiberaceae). The structure was determined by...
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Xylarianolide, A New Lignanoid from Xylaria sp.
A new lignanoid, named xylarianolide ( 1 ), was isolated from the fungal strain Xylaria sp. Its structure was elucidated by spectroscopic analyses,...
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Smart IM-MS and NMR study of natural diastereomers: the study case of the essential oil from Senecio transiens
Unambiguous identification of the components of a natural mixture remains a challenging and meticulous issue. Usually, different analytical...
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Using surface plasmon resonance, capillary electrophoresis and diffusion-ordered NMR spectroscopy to study drug release kinetics
Nanomedicines, including polymer nanocarriers with controlled drug release, are considered next-generation therapeutics with advanced therapeutic...
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An Integrated Approach Based on NMR and HPLC–UV-ESI–MS/MS to Characterize Apple Juices and Their Nanofiltration (NF) Bioactive Extracts
In the present work, Calabrian apple juices belonging to four different cultivars, Royal Gala, Pink Lady, Golden Delicious, and Fuji, were studied....
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Aggreganoid G, a New Methylene-Bridged Sesquiterpenoid Dimer from Lindera aggregata
Aggreganoid G ( 1 ), a new methylene-bridged lindenane sesquiterpenoid dimer was isolated and identified from the roots of Lindera aggregata. The...
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Lanthanide complexes with polyaminopolycarboxylates as prospective NMR/MRI diagnostic probes: peculiarities of molecular structure, dynamics and paramagnetic properties
The paramagnetic lanthanide complexes with polyaminopolycarboxylate (PAPC) ligands attract considerable attention from the standpoint of potential...
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Exploring the enantiomeric 13C position-specific isotope fractionation: challenges and anisotropic NMR-based analytical strategy
Trying to answer the intriguing and fundamental question related to chiral induction/amplification at the origin of homochirality in Nature: “Is...
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Mechanism of moisture adsorption in plant fibers surface-modified with glycerol evaluated by LF-NMR relaxation technique
Surface modification by humectants is an important technology to improve product quality in textile field, healthcare, tobacco processing and...
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Hop** dynamics and diffusion of atoms, molecules, and ions in nanoporous solids by exchange NMR spectroscopy
Molecular diffusion in nanoporous materials can be understood as series of dynamic hop** or exchange motions of molecules between different...
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Talaromycone A, a New 2-Benzopyran-1,3-Dione from Talaromyces wortmannii LGT-4
A new 2-benzopyran-1,3-dione, talaromycone A ( 1 ), was isolated from Talaromyces wortmannii LGT-4, an endophytic fungus of Tripterygium wilfordii . The...
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The anatomy of unfolding of Yfh1 is revealed by site-specific fold stability analysis measured by 2D NMR spectroscopy
Most techniques allow detection of protein unfolding either by following the behaviour of single reporters or as an averaged all-or-none process. We...
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A pipeline for making 31P NMR accessible for small- and large-scale lipidomics studies
Detailed molecular analysis is of increasing importance in research into the regulation of biochemical pathways, organismal growth and disease....
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Xylariaone, A New Cyclohexanone from Xylaria sp. 12F0758
A new cyclohexan-1-one, named xylariaone ( 1 ), was isolated from the fungal strain Xylaria sp. 12F0758. Its structure was elucidated by spectroscopic...
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Chemical Constituents from Gentiana urnula
A new compound, named 7-O-(4- β -glucopyranosyloxy-3-hydroxybenzoyl)secologanol ( 1 ), together with twelve known compounds ( 2–13 ), were isolated from...
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A New Isocoumarin Glucoside from the Aerial Parts of Aruncus sylvester
A new isocoumarin glucoside, 3S-6-methoxy-8-hydroxy 3-(4-hydroxyphenylethyl)-3,4-dihydroisocoumarin- 8-O- β -D-glucopyranoside ( 1 ), along with seven...
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Characterization, α-Amylase Inhibition and In Silico Docking Study of Polysaccharides Extracted from Rosy Garlic (Allium roseum) Bulbs
This work aimed to extract polysaccharides from Allium roseum bulbs, study and discuss, via in silico analysis, their in vitro inhibitory effects...
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Development of a novel indirubin derivative with enhanced anticancer properties: synthesis, in Vitro, and in Vivo evaluation
The indirubin ( 2 ) derivative undergoes condensation with hydroxylamine hydrochloride, resulting in the formation of a novel indirubin derivative ( 3 )...
