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  1. No Access

    Article

    Application of High Temperature LC to the Separation of AZD5438 (4-(1-Isopropyl-2-methyl-1H-imidazol-5-yl)-N-[4-(methylsulfonyl)phenyl]pyrimidin-2-amine) and Its Metabolites: Comparison of LC, UPLC and HTLC

    A comparison is made of the separation and analysis of a test probe, AZD5438 (4-(1-isopropyl-2-methyl-1H-imidazol-5-yl)-N-[4-(methylsulfonyl)phenyl]pyrimidin-2-amine), and its metabolites using conventional LC, U...

    Stefanie Shillingford, Laurence Bishop, Christopher J. Smith… in Chromatographia (2009)

  2. No Access

    Article

    Quantification of the In Vitro and In Vivo Metabolic Fates of 2-, 3- and 4-Bromobenzoic Acids Using High Temperature LC Coupled to ICP-MS and Linear Ion Trap MS

    High temperature liquid chromatography (HTLC), with water as the mobile phase, combined with ICP-MS tuned to the detection of Br, for quantification, and a linear ion trap MS, for structural identification, we...

    Christopher J. Smith, Stefanie Shillingford, Anthony M. Edge… in Chromatographia (2008)

  3. No Access

    Article

    Quantification of monohydroxy-PAH metabolites in urine by solid-phase extraction with isotope dilution-GC–MS

    For measurement of biomarkers from polycyclic aromatic hydrocarbon (PAH) exposure, an analytical method is described quantifying hydroxylated PAH (OH-PAH) in urine samples. This method determined monohydroxy ...

    Christopher J. Smith, Wenlin Huang… in Analytical and Bioanalytical Chemistry (2002)