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Article
Electrochemical Properties of Superionic Conductors CsAg4Br3 – хI2 + х
Solid solutions CsAg4Br3 – хI2 + х (x = 0.38; 0.50; 0.68) are prepared by solid-state synthesis; the single phase of the products is confirmed using the methods of X-ray diffraction and differential scanning calo...
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Article
Synthesis and Comparative Investigation of the Electrochemical Characteristics of CsAg4Br2.5I2.5 and RbAg4I5 Solid Electrolytes
A new method for the solid-phase synthesis of the superionic conductor CsAg4Br2.5I2.5 is proposed, which facilitates the preparation of a single-phase product. The thermal behavior of CsAg4Br2.5I2.5 in the temper...
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Article
Reaction of 1-aryl-2,2-dibromoalkan-1-ones with zinc and 4-aroyl-1H-benzo[c]oxepin-3-ones
Zinc enolates formed from the substituted 1-aryl-2,2-dibromoalkan-1-ones and zinc react with 4-aroyl-1H-benzo[c]oxepin-3-ones to form 1-alkyl-1-aroyl-1a -aroyl-1,1a,4,8b-tetrahydro-3-oxabenzo[a]cyclopropa c]cyclo...
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Article
Synthesis of alkyl-1,3-dihydro-3-oxobenzo[c]oxepine-4-carboxylates
Alkyl-1,3-dihydro-3-oxobenzo[c]oxepine-4-carboxylates were obtained by bromination of dialkyl-2-(2-methylbenzylidene)malonates with N-bromosuccinimide followed by the cyclization of dialkyl-2-(2-bromomethylbenzyl...
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Article
Interaction of zinc enolates prepared from 1-aryl-2,2-dibromoalkanones and zinc with alkyl 3-oxo-1,3-dihydrobenzo[c]oxepine-4-carboxylates
Zinc enolates obtained from substituted 1-aryl-2,2-dibromoalkanones and zinc react with alkyl 3-oxo-1,3-dihydrobenzo[c]oxepine-4-carboxylate to give the alkyl 1-alkyl-1-aroyl-2-oxo-4,8b-dihydro-1H-3-oxabenzo[a]cy...