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Preparation and functional properties of soy hull pectin

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Journal of the American Oil Chemists' Society

Abstract

Soy hulls (400 g), a co-product of the soybean processing industry, were used as a source of pectin which was extracted by0.05 N hydrochloric acid and precipitated with alcohol. The effect of various ratios of hull to extraction solvent (1∶10, 1∶15, 1∶20, and 1∶25) on the yield and purity of soy hull pectin was measured. The soy hull pectin extracts contained 63.07 to 68.72% galacturonic acid at various hull/solvent ratios. The pectin yield increased from 7.68 to 13.73% as the hull/solvent ratio increased from 1∶10 to 1∶15. Changes in pectin yield for higher hull/solvent ratio were insignificant (16.31–13.28% for 1∶20–1∶25 ratio, respectively). The hull/extraction solvent ratio did not significantly affect the pectin content and degree of esterification. Diffuse reflectance Fourier transform infrared spectroscopy of soy hull pectin revealed a similar surface structure to commercial-and analytical-grade pectins. The solubility of soy hull pectins was independent of solvent extraction ratios and pH. Rheology studies showed that pectin solution viscosity increased as the ratio of extraction solvent to hull decreased.

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References

  1. Thakur, B.R., R.K. Singh, and A.K. Handa, Chemistry and Uses of Pectin—A Review, Cirt. Rev. Food Nutr. 37:47–73 (1997).

    Article  CAS  Google Scholar 

  2. Whistler, R.L., and J.N. BeMiller, Pectins, in Carbohydrate Chemistry for Food Scientists, Eagan Press, St. Paul, Minnesota, 1997, pp. 203–210.

    Google Scholar 

  3. Fernadez, M.L., D.M. Sun, M.A. Tosca, and D.J. McNamara, Citrus Pectin and Cholesterol Interact to Regulate Hepatic Cholesterol Homeostasis and Lipoprotein Metabolism: A Dose Response Study in Guinea Pigs, Am. J. Clin. Nutr. 59:869–872 (1994).

    Google Scholar 

  4. Voragen, A.G.J., W. Pilnik, J.F. Thibault, M.A.V. Axelos, and C.M.G.C. Renard, Pectins, in Food Polysaccharides and Their Applications, edited by A.M. Stephan, Academic Press New York, 1995, pp. 287–339.

    Google Scholar 

  5. Walter, R.H., The Chemistry and Technology of Pectin, Academic Press, New York, 1991, pp. 24, 197.

    Google Scholar 

  6. May, C.D., Industrial Pectins: Sources, Production, and Application, Carbohydr. Polym. 12:79–84 (1986).

    Article  Google Scholar 

  7. Michael, F., J.F. Thibault, C. Mereier, F. Heitz, and F. Pouolladue, Extraction and Characterization of Pectin from Sugar Beet Pulp, J. Food Sci. 50:1499–1503 (1985).

    Article  Google Scholar 

  8. Miyamoto, A., and K.C. Chang, Extraction and Physicochemical Characterization of Pectins from Sunflower Head Residue, Can. Inst. Food Technol. 57:1439–1445 (1992).

    CAS  Google Scholar 

  9. Eriksson, I., R. Andersson, and P. Amen, Extraction of Pectic Substances from Dehulled Rapeseed, Carbohydr. Res. 301:177–185 (1997).

    Article  CAS  Google Scholar 

  10. Snyder, H.E., and T.W. Kown, Soybean Utilization, Van Nostrand Reinhold, New York, 1987, p. 60.

    Google Scholar 

  11. Gnanasambandam, R., and A. Proctor, Preparation of Soy Hull Pectin, Food Chem. 65:461–467 (1999).

    Article  CAS  Google Scholar 

  12. Kalapathy, U., and A. Proctor, Effect of Acid Extraction and Alcohol Precipitation Conditions on the Yield and Purity of Soy Hull Pectin, Food Chem. 73:393–396 (2001).

    Article  CAS  Google Scholar 

  13. Kinter, P.K., and J.P. Van Buren, Carbohydrate Interference and Its Correction in Pectin Analysis Using m-Hydroxydiphenyl Method, J. Food Sci. 47:756–759 (1982).

    Article  Google Scholar 

  14. Vazquez-Blanko, M.E., M.L. Vazquez-Oderiz, J. Lopez-Hernandez, J. Simal-Lozano, and M.A. Romero-Rodriguez, HPLC Determination of Pectins in Raspberries as Galacturonic Acid and Optimizing Using Forward Optical Scanning, J. Chromatogr. Sci. 31:477–479 (1993).

    Google Scholar 

  15. Gnanasambandam, R., and A. Proctor, Determination of Pectin Degree of Esterification by Diffuse Reflectance Fourier Transform Infrared Spectroscopy, Food Chem. 68:327–332 (2000).

    Article  CAS  Google Scholar 

  16. FCC III Food Chemical Codex (3rd edn.), National Academy of Science, Washington, DC 1981, p. 518.

  17. Harbers, L.H., Ash Analysis, in Chemical Analysis of Foods, edited by S.S. Nielsen, Jones and Bartlett Publishers, Inc., London, 1994, pp. 113–121.

    Google Scholar 

  18. SAS Institute Inc., SAS/STAT User's Guide, Statistical Analysis System Institute, Cary, NC (1994).

    Google Scholar 

  19. Kravtchenko, T.P., A.G.J. Vorgan, and W. Pilnik, Analytical Composition in Three Industrial Pectin Preparations, Carbohydr. Polym. 18:17–22 (1992).

    Article  CAS  Google Scholar 

  20. Wellner, N., M. Kacurakova, A. Malovikaova, R. Wilson, and P.S. Belton, FTIR Study of Pectate and Pectinate Gels Formed by Divalent Cations, Carbohydr. Res. 308:123–131 (1998).

    Article  CAS  Google Scholar 

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Correspondence to A. Proctor.

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Monsoor, M.A., Proctor, A. Preparation and functional properties of soy hull pectin. J Amer Oil Chem Soc 78, 709–713 (2001). https://doi.org/10.1007/s11746-001-0330-z

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  • DOI: https://doi.org/10.1007/s11746-001-0330-z

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