Abstract
Niobium is known to segregate strongly to grain boundaries in steel. The strong interaction of Nb with grain boundaries results in an important reduction of the grain boundary mobility and strong retardation of recrystallization and grain growth. In this study, the effect of Nb on the mobility of grain boundaries in a second-generation Fe-30 pct Mn TWIP steel is investigated. Grain growth kinetics was measured in a series of Nb-containing Fe-30 pct Mn model alloys. An estimate of the grain boundary mobility was obtained for various temperatures and niobium contents. It was found that Nb slows down the mobility of random high-angle grain boundary segments that are not twin related. The effect of solute Nb on grain growth, in the presence of annealing twins, was modeled using Cahn’s theory of solute drag coupled with a recently formulated twin-inhibited grain growth model. The results are shown to be in very good agreement with the experimentally determined growth kinetics.
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References
G. W. Yang, X. J. Sun, Q. L. Yong, Z. D. Li & X. X. Li: Journal of Iron and Steel Research, International, 2014, vol. 21, pp. 757-64.
J. G. Speer, A. L. Araujo, D. K. Matlock & E. de Moor: Materials Science Forum, 2017, vol. 879, pp. 1834 - 40.
T. N. Baker: Ironmaking & Steelmaking, 2016, vol. 43, pp. 264 -07.
J. Villalobos, A. Del-Pozo, B. Campillo, J. Mayen & S. Serna: Metals, 2018, vol. 8, pp. 351.
M. Maalekian, R. Radis, M. Militzer, A. Moreau & W. Poole: Acta materialia, 2012, vol. 60, pp. 1015-26.
H. L. Yang, G. Xu, L. Wang, Q. Yuan & B. He: Metal Science and Heat Treatment, 2017, vol. 59, pp. 8-13.
L. Zhang & T. Kannengiesser: Materials Science and Engineering: A, 2014, vol. 613, pp. 326-35.
L.C. Zhang, X. L. Wen & Y. Z Liu: Materials Science Forum, 2017, vol. 898, pp. 783-90.
S. Yamamoto, C. Ouchi, T. Osuka: Thermomechanical Process. Microalloyed Austenite, TMS-AIME, New York, 1981, pp. 613–39.
L. Bäcke: ISIJ Int., 2010, vol. 50, pp. 239–47.
J. Takahashi, K. Kawakami, J. I. Hamada & K. Kimura: Acta Materialia, 2016, vol. 107, pp. 415-22.
H.S. Zurob, Y. Brechet, G. Purdy: Acta Mater., 2001, vol. 49, pp. 4183–90.
S. Medina, J. Mancilla: ISIJ Int., 1996, vol. 36, pp. 1070-76.
S.F. Medina: Scr. Metall. Mater. States, 1995, vol. 32, p. 43.
M. Suehiro, Z.-K. Liu, J. Ågren: Acta Mater., 1996, vol. 44, pp. 4241-51.
T. Jia & M. Militzer: Metallurgical and Materials Transactions A, 2015, vol. 46, pp. 614-21.
M. Militzer, J. J. Hoyt, N. Provatas, J. Rottler, C. Sinclair & H. S. Zurob: JOM, 2014, vol. 66, pp. 740-46.
L.M. Fu, H.R. Wang, W. Wang, A.D. Shan: Mater. Sci. Technol., 2011, vol. 44, pp. 996-01.
K. Banerjee, M. Militzer, M. Perez, X. Wang: Metall. Mater. Trans. A, 2010, vol. 41, pp. 3161-72.
A.H. Seikh, M.S. Soliman, A. Almajid, K. Alhajeri, W. Alshalfan: Adv. Mater. Sci. Eng., 2014, vol. 2014, p. 1-8.
Q. Yu, Y.Sun: Mater. Sci. Eng. A, 2006, vol. 420, pp. 34-38.
C. Shang & C. Miao, Advanced Steels, Springer, Berlin, 2011, pp. 341-56.
M. Militzer, Comprehensive Materials Processing, vol. 1, Elsevier, Amsterdam, 2014, pp. 191-216.
K. A. Annan, C. W. Siyasiya & W. E. Stumpf: Journal of the Southern African Institute of Mining and Metallurgy, 2015, vol. 115, pp. 973-80.
Z. Cui, J. Patel & E. J. Palmiere, HSLA Steels 2015, Microalloying 2015 & Offshore Engineering Steels 2015, Springer, Cham, 2015, pp. 281-87.
P. Lejcek, Grain Boundary Segregation in Metals, vol. 136, Springer, Berlin, 2010, pp. 25-43.
G. Gottstein, L.S. Shvindlerman, Grain Boundary Migration in Metals: Thermodynamics, Kinetics, Applications, 2nd ed., CRC Press, Boca Raton, 2009, pp. 509-577.
B. C. De Cooman, O. Kwon & K. G. Chin: Materials Science and Technology, 2012, vol. 28, pp. 513-27.
L. Chen, Y. Zhao & X. Qin: Acta Metallurgica Sinica (English Letters), 2013, vol. 26, pp. 1-15.
L. Llanos, B. Pereda & B. Lopez: Metallurgical and Materials Transactions A, 2015, vol. 46, pp. 5248-65.
A. Hamada, A. Khosravifard, D. Porter & L. P. Karjalainen: Materials Science and Engineering: A, 2017, vol. 703, pp. 85-96.
C. Haase, M. Kühbach, L. A. Barrales-Mora, S. L. Wong, F. Roters, D. A. Molodov & G. Gottsstein: Acta Materialia, 2015, vol. 100, pp. 155-68.
L. Llanos, B. Pereda, D. Jorge-Badiola, J. M. Rodriguez-Ibabe, B. López: Mater. Sci. Forum, 2013, vol. 753, pp. 443-48.
M. Bhattacharyya, B. Langelier, G. Purdy, H.S. Zurob: Metallurgical and Materials Transactions A., 2019, vol. 50, pp. 905-14.
M. Bhattacharyya, Y. Brechet, G.R. Purdy, and H.S. Zurob: Met Trans. A (under review).
J.W. Cahn: Acta Metall., 1962, vol. 10, pp. 789–98.
K. Furumai, H. Zurob, A. Phillion: ISIJ Int. (accepted).
F. J. Humphreys, M. Hatherly, Recrystallization and Related Annealing Phenomena, 2nd ed., Elsevier Ltd., Amsterdam, 2012, pp. 159-60.
M.K Rehman, H.S. Zurob: Metall. Mater. Trans. A, 2013, vol. 44, pp. 1862-71.
N. Maruyama, G.D.W. Smith, A. Cerezo: Mater. Sci. Eng. A, 2003, vol. 353, pp. 126–32.
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Manuscript submitted May 22, 2018.
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Bhattacharyya, M., Langelier, B. & Zurob, H.S. Effect of Solute Nb on Grain Growth in Fe-30 Pct Mn Steel. Metall Mater Trans A 50, 3674–3682 (2019). https://doi.org/10.1007/s11661-019-05273-2
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DOI: https://doi.org/10.1007/s11661-019-05273-2