Abstract
In-situ transmission electron microscopy (TEM) is used to directly observe twin evolution in Mg under tension and compression. Twins grow during tensile loading. Upon load reversal, the first-generation twin detwins by nucleation and growth of a second-generation twin within its volume. This mechanism for detwinning is different from the more traditional mechanism of detwinning by reverse motion of a twin boundary. Reloading in tension causes the second-generation twin to recede, leaving behind residual features. In compression, the second-generation twin re-nucleates in the area of this debris, and grows. Interactions between dislocations and twin boundaries change the character of the observed dislocations. Direct observation of such behavior aids in clearer understanding of the observed microstructures from post-mortem TEM.
![](http://media.springernature.com/m312/springer-static/image/art%3A10.1007%2Fs11661-013-1765-0/MediaObjects/11661_2013_1765_Fig1_HTML.gif)
![](http://media.springernature.com/m312/springer-static/image/art%3A10.1007%2Fs11661-013-1765-0/MediaObjects/11661_2013_1765_Fig2_HTML.jpg)
![](http://media.springernature.com/m312/springer-static/image/art%3A10.1007%2Fs11661-013-1765-0/MediaObjects/11661_2013_1765_Fig3_HTML.jpg)
![](http://media.springernature.com/m312/springer-static/image/art%3A10.1007%2Fs11661-013-1765-0/MediaObjects/11661_2013_1765_Fig4_HTML.jpg)
Similar content being viewed by others
References
G Proust, C N Tomé, A Jain, and S R Agnew: Int. J. Plast., 2009, vol. 25, pp. 861–80.
I J Beyerlein, R J McCabe, and C N Tomé: J. Mech. Phys. Solids, 2011, vol. 59, pp. 988–1003.
C N Tomé, I J Beyerlein, J Wang, and R J McCabe: JOM, 2011, vol. 63, pp. 19–23.
P G Partridge and R W Gardiner: Acta Metall., 1967, vol. 15, pp. 387–89.
Q Yu, J Zhang, and Y Jiang: Philos. Mag. Lett., 2011, vol. 91, pp. 75765.
J Wang, N Li, O Anderoglu, X Zhang, A Misra, J Y Huang, and J P Hirth: Acta Mater., 2010, vol. 58, pp. 2262–70.
S R Agnew, J A Horton, and M H Yoo: Metall. Mater. Trans. A, 2002, vol. 33A, pp. 851–58.
G.S. Kim, S. Yi, Y. Huang, and E. Lilleodden: MRS Symp. Proc., 2010, vol. 1224.
T Obara, H Yoshinga, and S Morozumi: Acta Metall., 1973, vol. 21, pp. 845–53.
S R Agnew and Ö Duygulu: Int. J. Plast., 2005, vol. 21, pp. 1161–93.
Q Yu, L Qi, K Chen, R K Mishra, J Li, and A M Minor: Nano Lett., 2012, vol. 12, pp. 887–92.
J Ye, R K Mishra, A K Sachdev, and A M Minor: Scripta Mater., 2011, vol. 64, pp. 292–95.
E Lilleodden: Scripta Mater., 2010, vol. 62, pp. 532–35.
L Wu, A Jain, D W Brown, G M Stoica, S R Agnew, B Clausen, D E Fielden, and P K Liaw: Acta Mater., 2008, vol. 56, pp. 688–95.
D W Brown, A Jain, S R Agnew, and B Clausen: Mater. Sci. Forum, 2007, vol. 539–543, pp. 3407–13.
R D Field and P A Papin: Ultramicroscopy, 2004, vol. 102, pp. 23–26.
S.G. Song and G.T. Gray, III: Acta Metall. Mater., 1995, vol. 43, pp. 2339–50.
D Bhattacharyya, EK Cerreta, R McCabe, M Niewczas, GT Gray, A Misra, and CN Tomé (2009) Acta Mater. 57:305–15.
G Proust, G C Kaschner, I J Beyerlein, B Clausen, D W Brown, R J McCabe, and C N Tomé: Experimental Mechanics, 2010, vol. 50, pp. 125–33.
L Wu, S R Agnew, D W Brown, G M Stoica, B Clausen, A Jain, D E Fielden, and P K Liaw: Acta Mater., 2008, vol. 56, pp. 3699–3707.
A. Jain and S.R. Agnew: Magnesium Technology 2006, 2006, pp. 219–24.
T Uota, T Suzu, S Fukumoto, and A Yamamoto: Mater. Trans. Jpn. Inst. Met., 2009, vol. 50, pp. 2118–20.
X Y Lou, M Li, R K Boger, S R Agnew, and R H Wagoner: Int. J. Plast., 2007, vol. 23, pp. 44–86.
T Yasutomi and M Enoki: Mater. Trans. Jpn. Inst. Met., 2012, vol. 53, pp. 1611–16.
H. Wang, P.D. Wu, J. Wang, and C.N. Tomé: Int. J. Plast., 2013 (in press).
E Roberts and P G Partridge: Acta Metall., 1966, vol. 14, pp. 513–27.
P.B. Hirsch, A. Howie, R.B. Nicholson, D.W. Pashley, and M.J. Whelan (1977) Electron Microscopy of Thin Crystals, 2nd edn. Krieger Publishing Co., Malabar, FL.
Acknowledgment
The current study was fully funded by the Department of Energy, Basic Energy Science Project FWP06SCPE401.
Author information
Authors and Affiliations
Corresponding author
Additional information
Manuscript submitted March 14, 2013.
Electronic supplementary material
Below is the link to the electronic supplementary material.
Rights and permissions
About this article
Cite this article
Morrow, B.M., McCabe, R.J., Cerreta, E.K. et al. In-Situ TEM Observation of Twinning and Detwinning During Cyclic Loading in Mg. Metall Mater Trans A 45, 36–40 (2014). https://doi.org/10.1007/s11661-013-1765-0
Published:
Issue Date:
DOI: https://doi.org/10.1007/s11661-013-1765-0