Abstract
A modular automated radionuclide separator for 89/90Sr (MARS Sr-90) has been developed for the rapid and reproducible isolation of radiostrontium. The automated radiochemical method for separation and purification of 89/90Sr in milk was developed and applied to the determination of radiostrontium in spiked milk powders supplied for IAEA inter-laboratory testing. The activities of 89/90Sr in milk samples could be measured within 1 day with less than 5 % relative bias using MARS Sr-90 and a liquid scintillation counter.
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References
Maxwell SL, Culligan BK (2009) Rapid method for determination of radiostrontium in emergency milk samples. J Radioanal Nucl Chem 279(3):757–760
Tait D, Haase G, Wiechen A (1997) Rapid and efficient separation of strontium from liquid milk with a cation resin Dowex 50WX8 treated with cryptand 222. J Radioanal Nucl Chem 226(1–2):225–228
Brun S, Bessac S, Uridat D, Boursier B (2002) Rapid method for the determination of radiostrontium in milk. J Radioanal Nucl Chem 253(2):191–197
Gunther K, Lange S, Veit M (2009) A rapid method for determining 89Sr and 90Sr by Cerenkov counting. Appl Radiat Isot 67:781–785
Kim CK, Al-Hamwi A, Torvenyi A, Kis-Benedek G, Sansone U (2009) Validation of rapid methods for the determination of radiostrontium in milk. Appl Radiat Isot 67:786–793
International Atomic Energy Agency (2013) Rapid simultaneous determination of 89Sr and 90Sr in milk: A procedure using Cerenkov and scintillation counting. IAEA/AQ/27, International Atomic Energy Agency, Vienna, Austria
Brun S, Kergadallan Y, Boursier B, Fremy J-M, Janin F (2003) Methodology for determination of radiostrontium in milk: a review. Lait 83:1–15
Vajda N, Kim CK (2010) Determination of radiostrontium isotopes: A review of analytical methodology. Appl Radiat Isot 68:2306–2326
Heckel A, Vogl K (2009) Rapid method for determination of the activity concentrations of 89Sr and 90Sr. Appl Radiat Isot 67:794–796
Maxwell SL III (2006) Rapid column extraction method for actinides and 89/90Sr in water samples. J Radioanal Nucl Chem 267(3):537–543
Lamb JD, Nordmeyer FR, Drake PA, Elder MP, Miles RW, Lash RP (1989) Ion chromatographic separation for analysis of radiostrontium in nuclear reprocessing solutions of high ionic strength. J Radioanal Nucl Chem 134(2):317–331
Mateos JI, Gomez E, Garcias F, Gasas M, Cerda V (2000) Rapid 90Sr/90Y determination in water samples using a sequential injection method. Appl Radiat Isot 67:79–794
O’Hara MJ, Burge SR, Grate JW (2009) Automated radioanalytical system for the determination of 90Sr in environmental water samples by 90Y Cerenkov radiation counting. Anal Chem 81:1228–1237
HASL-300, Sr-02-RC (1997) In: Chieco NA (ed) The procedures manual of the environmental measurements laboratory, 28th edn. U.S. Department of Energy, New York
Chung KH, Choi SD, Choi GS, Kang MJ (2013) Design and performance of an automated radionuclide separator: its application on the determination of 99Tc in groundwater. Appl Radiat Isot 81:57–61
Acknowledgments
This work was performed under the auspices of the Ministry of Science, ICT and Future Planning (MSIP) of Korea, NRF contract No. 2012M2A8A4025915.
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Chung, K.H., Kim, H., Lim, J.M. et al. Rapid determination of radiostrontium in milk using automated radionuclides separator and liquid scintillation counter. J Radioanal Nucl Chem 304, 293–300 (2015). https://doi.org/10.1007/s10967-014-3594-z
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DOI: https://doi.org/10.1007/s10967-014-3594-z