Log in

Microwave curing for applying polymeric nanocapsules containing essential oils on cotton fabric to produce antimicrobial and fragrant textiles

  • Original Paper
  • Published:
Cellulose Aims and scope Submit manuscript

Abstract

Application of encapsulated essential oils in the chemical finishing of textiles is rapidly develo** because of their versatility and flexibility. In this work, alginate nanocapsules containing peppermint oil were prepared by the microemulsion method and applied on cotton fabric by a microwave curing process. Effective parameters on antimicrobial activity of finished cotton fabric were optimized to obtain a good antimicrobial and fragrant textile. FT-IR spectroscopy and TGA were used to quantify the presence of nanocapsules on the cotton fabric. Also, the surface distribution, attendance and preferred position of the nanocapsules on the textile fibers were investigated by SEM images. The releasing behavior of peppermint oil from the finished cotton fabric in different washing cycles measured by GC-MS analysis indicated that the percent of peppermint oil reached 16 % after 25 washing cycles. Antimicrobial activity of the finished fabric showed 100 % bacterial reduction for both E. coli and S. aureus bacteria in optimum conditions.

This is a preview of subscription content, log in via an institution to check access.

Access this article

Subscribe and save

Springer+ Basic
EUR 32.99 /Month
  • Get 10 units per month
  • Download Article/Chapter or Ebook
  • 1 Unit = 1 Article or 1 Chapter
  • Cancel anytime
Subscribe now

Buy Now

Price includes VAT (France)

Instant access to the full article PDF.

Fig. 1
Fig. 2
Fig. 3
Fig. 4
Fig. 5
Fig. 6
Fig. 7

Similar content being viewed by others

References

  • AATCC test method 100–2004 (2005) Antibacterial finishes on textile materials: assessment of AATCC technical manual. American Association of textile chemists and colorists, Research Triangle Park

    Google Scholar 

  • ASTM D-1388-64 (1975) Method A: standard test method for stiffness of fabrics. ASTM, New York

    Google Scholar 

  • Bakkali F, Averbeck S, Averbeck D, Idaomar M (2008) Biological effects of essential oils—a review. Food Chem Toxicol 46:446–475. doi:10.1016/j.fct.2007.09.106

    Article  CAS  Google Scholar 

  • Beristain CI, García HS, Vernon-Carter EJ (2001) Spray-dried encapsulation of cardamom (Elettaria cardamomum) essential oil with mesquite (Prosopis juliflora) gum. LWT Food Sci Technol 34:398–401. doi:10.1006/fstl.2001.0779

    Article  CAS  Google Scholar 

  • Bischof Vukušić S, Flinčec Grgac S, Budimir A, Kalenić S (2011) Cotton textiles modified with citric acid as efficient antibacterial agent for prevention of nosocomial infections. Croat Med J 52:68–75. doi:10.3325/cmj.2011.52.68

    Article  Google Scholar 

  • Bonet Aracil MÁ, Monllor P, Capablanca L, Gisbert J, Díaz P, Montava I (2015) A comparison between padding and bath exhaustion to apply microcapsules onto cotton. Cellulose 22:2117–2127. doi:10.1007/s10570-015-0600-8

    Article  CAS  Google Scholar 

  • Budimir A, Bischof Vukusic S, Grgac Flincec S (2012) Study of antimicrobial properties of cotton medical textiles treated with citric acid and dried/cured by microwaves. Cellulose 19:289–296. doi:10.1007/s10570-011-9614-z

    Article  CAS  Google Scholar 

  • Chen X, Yu J, Zhang Z, Lu C (2011) Study on structure and thermal stability properties of cellulose fibers from rice straw. Carbohydr Polym 85:245–250. doi:10.1016/j.carbpol.2011.02.022

    Article  CAS  Google Scholar 

  • Cristina ED (2004) Understanding true aromatherapy: understanding essential oils. Home Health Care Manag Pract 16:474–479. doi:10.1177/1084822304265851

    Article  Google Scholar 

  • El-Molla MM, Haggag K, El-Shall FN, Shaker NO, Alian NA (2013) Use of novel synthesized aqueous binders for pigment printing of polyester fabrics. Indian J Fibre Text Res 38:57–65

    Google Scholar 

  • Ghayempour S, Mortazavi SM (2013) Fabrication of micro–nanocapsules by a new electrospraying method using coaxial jets and examination of effective parameters on their production. J Electrostat 71:717–727. doi:10.1016/j.elstat.2013.04.001

    Article  Google Scholar 

  • Ghayempour S, Mortazavi SM (2014) Antibacterial activity of peppermint fragrance micro–nanocapsules prepared with a new electrospraying method. J Essent Oil Res 26:492–498. doi:10.1080/10412905.2014.949882

    Article  CAS  Google Scholar 

  • Ghayempour S, Mortazavi SM (2015) Preparation and investigation of sodium alginate nanocapsules by different microemulsification devices. J Appl Polym Sci. doi:10.1002/app.41904

    Google Scholar 

  • Heywood D (2003) Textile finishing. Society of Dyers and Colourists, Bradford

    Google Scholar 

  • Hong K, Park S (1999) Melamine resin microcapsules containing fragrant oil: synthesis and characterization. Mater Chem Phys 58:128–131. doi:10.1016/S0254-0584(98)00263-6

    Article  CAS  Google Scholar 

  • Hong K, Park S (2000) Preparation of poly(l-lactide) microcapsules for fragrant fiber and their characteristics. Polymer 41:4567–4572. doi:10.1016/S0032-3861(99)00677-1

    Article  CAS  Google Scholar 

  • International Standard, ISO 105-C10 (2006) Textiles-Tests for colour fastness: Colour fastness to washing with soap or soap and soda. ISO, Geneva

    Google Scholar 

  • International Standard, ISO 105-X12 (2001) Textiles-Tests for colour fastness: Colour fastness to rubbing. ISO, Geneva

    Google Scholar 

  • Jantas R, Górna K (2006) Antibacterial finishing of cotton fabrics. Fibres Text East Eur 14:88–91

    CAS  Google Scholar 

  • Javid A, Raza ZA, Hussain T, Rehman A (2014) Chitosan microencapsulation of various essential oils to enhance the functional properties of cotton fabric. J Microencapsul 31:461–468

    Article  CAS  Google Scholar 

  • Lee A, Han C, Yi E (2014) Preparation and characterization of melamine-formaldehyde microcapsules containing Citrus unshiu essential oil. Fibers Polym 15:35–40. doi:10.1007/s12221-014-0035-0

    Article  CAS  Google Scholar 

  • Li S, Boyter H, Qian L (2005) UV curing for encapsulated aroma finish on cotton. J Text Inst 96:407–411. doi:10.1533/joti.2005.0116

    Article  CAS  Google Scholar 

  • Li S, Lewis JE, Stewart NM, Qian L, Boyter H (2008) Effect of finishing methods on washing durability of microencapsulated aroma finishing. J Text Inst 99:177–183. doi:10.1080/00405000701489701

    Article  CAS  Google Scholar 

  • Monllor P, Bonet MA, Cases F (2007) Characterization of the behaviour of flavour microcapsules in cotton fabrics. Eur Polym J 43:2481–2490. doi:10.1016/j.eurpolymj.2007.04.004

    Article  CAS  Google Scholar 

  • Rajendran R, Radhai R, Kotresh TM, Csiszar E (2013) Development of antimicrobial cotton fabrics using herb loaded nanoparticles. Carbohydr Polym 91:613–617. doi:10.1016/j.carbpol.2012.08.064

    Article  CAS  Google Scholar 

  • Rodrigues SN, Martins IM, Fernandes IP, Gomes PB, Mata VG, Barreiro MF, Rodrigues AE (2009) Scentfashion®: microencapsulated perfumes for textile application. Chem Eng J 149:463–472. doi:10.1016/j.cej.2009.02.021

    Article  CAS  Google Scholar 

  • SIST-EN 12127 (1999) Determination of mass per unit area using small samples. CEN, Brussels

    Google Scholar 

  • SIST-EN ISO 5084:1999 (1996) Determination of thickness of textiles and textile products. CEN, Brussels

    Google Scholar 

  • Teixeira CSNR, Martins IMD, Mata VLG, Filipe Barreiro MF, Rodrigues AE (2011) Characterization and evaluation of commercial fragrance microcapsules for textile application. J Text Inst 103:269–282. doi:10.1080/00405000.2011.566312

    Google Scholar 

  • Thilagavathi G, Krishna Bala S, Kannaian T (2007) Microencapsulation of herbal extracts for microbial resistance in healthcare textiles. Indian J Fibre Text Res 32:351–354

    CAS  Google Scholar 

  • Wang CX, Chen SL (2005) Aromachology and its application in the textile field. Fibres Text East Eur 13:41–44

    CAS  Google Scholar 

  • Zhao X, Min J, Jx He (2011) Effect of microwave curing on antimicrobial activity of chitosan biguanidine hydrochloride treated wool fabrics. J Text Inst 102:801–807. doi:10.1080/00405000.2010.522047

    Article  CAS  Google Scholar 

Download references

Author information

Authors and Affiliations

Authors

Corresponding author

Correspondence to Soraya Ghayempour.

Rights and permissions

Reprints and permissions

About this article

Check for updates. Verify currency and authenticity via CrossMark

Cite this article

Ghayempour, S., Mortazavi, S.M. Microwave curing for applying polymeric nanocapsules containing essential oils on cotton fabric to produce antimicrobial and fragrant textiles. Cellulose 22, 4065–4075 (2015). https://doi.org/10.1007/s10570-015-0765-1

Download citation

  • Received:

  • Accepted:

  • Published:

  • Issue Date:

  • DOI: https://doi.org/10.1007/s10570-015-0765-1

Keywords

Navigation