Abstract
A microwave assisted solvothermal method is described for rapid preparation of nano-oxides. This method is based on exploiting differential dielectric constants to induce preferred heating and decomposition of the oxide precursors in the presence of suitable cap** agents. This strategic approach has been used to prepare nanopowders of MgO, NiO, ZnO, Al2O3, Fe2O3 and ZrO2.
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Agrafiotis C, Tsetsekou A, Stournaras C J, Julbe A, Dalmazio L and Guizard C 2000Solid State Ionics 136 1301
Anderson Kris, Fernández Silvia Cortiñas, Hardacre Christopher and Marr Patricia C 2004Inorg. Chem. Commun. 7 73
Ding Tao, Zhang Jian-Rong, Long Su and Zhu Jun-Jie 2003Microelectronic Eng. 66 46
Edelstein A S and Cammarata R C 1998Nanomaterials: Synthesis, properties and application (Washington DC: Naval Research Laboratory)
Esaki Leo 1999Nanostructured Mater. 121
He Rong, Qian Xue-feng, Yin Jie, ** Hong-an, Bian Li-juan and Zhu Zi-kang 2003Colloids and Surfaces A: Phys. Eng. Aspects 220 151
Kaskel Stefan, Schlichte Klaus and Kratzke Tobias 2004J. Mol. Catal. A: Chem. 208 291
Komarneni S 2003Curr. Sci. 85 30
Lee D W and Kim B K 2004Mater. Lett. 58 378
Lee **-Seok and Choi Sung-Churl 2004Mater. Lett. 58 390
Pang Qi, Shi Jianxin, Liu Yu, **ng Desong, Gong Menglian and Xu Ningsheng 2003Mater. Sci. Eng. B103 57
Panneerselvam M 2002Microwave synthesis and consolidation of advanced ceramics and ceramic composites, PhD thesis, Indian Institute of Science, Bangalore
Piticescu R R, Barbara Malic, Marija Kosec, Motoc A, Monty C, Iulia Soare, Kosmac T and Daskobler A 2004J. Euro. Ceram. Soc. 24 1941
Rao K J, Vaidhyanathan B, Ganguli M and Ramakrishnan P A 1998Chem. Mater. 882 11
Sankaranarayanan V K and Sreekumar C 2003Appl. Phys. 3 205
Savchuk A I, Paranchych S, Yu, Kurganetski M V, Stolyarchuk I D, Tanasyuk Yu, Perrone V A and DeGiorgi M L 2003Mater. Sci. Eng. C23 259
Shen Cheng-min, Zhang **ao-gang, Zhou Ying-ke and Li Hu-lin 2003Mater. Chem. Phys. 78 437
Yin Hengbo, Yamamoto Tetsushi, Wada Yuji and Yanagida Shozo 2004Mater. Chem. Phys. 83 66
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Under graduate Summer Research Fellow of the Indian Academy of Sciences from IIT Madras.
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Rao, K.J., Mahesh, K. & Kumar, S. A strategic approach for preparation of oxide nanomaterials. Bull Mater Sci 28, 19–24 (2005). https://doi.org/10.1007/BF02711166
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DOI: https://doi.org/10.1007/BF02711166