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Gas Chromatography and Mass Spectrometry: The Technique

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Emerging Food Authentication Methodologies Using GC/MS

Abstract

Combining the techniques of gas chromatography and mass spectrometry provides conjunction with a confirmatory character, which has a great power of detection, identification, and quantification of a wide range of chemical compounds. This chapter serves as a brief description of gas chromatography-mass spectrometry (GC/MS) instruments and their components, variations, and suitability for specific applications. Various gas chromatography techniques, such as standard GC or multidimensional GC, but also different types of mass spectrometers, ranging from classic quadrupole systems to high-resolution mass spectrometers, will be presented. The chapter encompasses corresponding merits and drawbacks, as well as references to subsequent chapters.

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Abbreviations

CI:

Chemical ionization

GC:

Gas chromatography

GC×GC:

Two-dimensional gas chromatography

EI:

Electron ionization

IR:

Isotope-ratio

IT:

Ion-trap

IUPAC:

The International Union of Pure and Applied Chemistry

LC:

Liquid chromatography

M:

Magnetic sector mass analyzer

MS:

Mass spectrometry

MS/MS:

Tandem or hybrid mass spectrometry

m/z :

Mass-to-charge ratio

NCI:

Negative chemical ionization

PCI:

Positive chemical ionization

PTV:

Programmed temperature vaporizing

SFC:

Supercritical fluid chromatography

TOF:

Time-of-flight

Q:

Quadrupole

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Acknowledgment

The authors would like to acknowledge the support from the Ministry of Education, Science and Technological Development of the Republic of Serbia (Program No. 451-03-68/2022-14/200134).

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Authors and Affiliations

  1. Department of Applied and Engineering Chemistry, Faculty of Technology Novi Sad, University of Novi Sad, Novi Sad, Serbia

    Kristian Pastor, Marko Ilić, Djura Vujić, Marijana Ačanski, Snežana Kravić, Zorica Stojanović & Ana Đurović

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  1. Kristian Pastor
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  2. Marko Ilić
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  3. Djura Vujić
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Correspondence to Kristian Pastor .

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  1. Department of Applied and Engineering Chemistry, Faculty of Technology Novi Sad, University of Novi Sad, Novi Sad, Serbia

    Kristian Pastor

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Pastor, K. et al. (2023). Gas Chromatography and Mass Spectrometry: The Technique. In: Pastor, K. (eds) Emerging Food Authentication Methodologies Using GC/MS. Springer, Cham. https://doi.org/10.1007/978-3-031-30288-6_1

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