Effect of Size and Preconditioning of Concrete Cores Against Sulfate Attack (Test)

  • Conference paper
  • First Online:
Proceedings of the 75th RILEM Annual Week 2021 (RW 2021)

Abstract

Some of the proposed accelerated tests for evaluating the sulfate resistance of concrete address only the Portland cement, as the hydrated cement paste contains unstable compounds that may react with sulfate ions, while others are based on concrete performance. In search of comprehensive and practical assessments, some researchers proposed the evaluation of core samples as performance tests. The kinetics of attack is accelerated by further exposing the inner matrix of the concrete to the aggressive solution. Another accelerating strategy reported in the literature is to precondition the samples by vacuum saturation with sulfate solution, which speeds up the penetration of sulfate ions into concrete at the start of the test.

In this work, both strategies were applied to develop an accelerated performance test for concrete. Core specimens of two sizes were drilled off from two concrete types and exposed to a highly concentrated sulfate solution. Two preconditioning procedures were applied to the samples prior to exposure. The results show a large reduction in failure time when a vacuum step is used as preconditioning (one-sixth). This methodology could be useful in recycled concrete production to evaluate the potential reactivity of source concrete against sulfates.

This is a preview of subscription content, log in via an institution to check access.

Access this chapter

Subscribe and save

Springer+ Basic
EUR 32.99 /Month
  • Get 10 units per month
  • Download Article/Chapter or Ebook
  • 1 Unit = 1 Article or 1 Chapter
  • Cancel anytime
Subscribe now

Buy Now

Chapter
GBP 19.95
Price includes VAT (United Kingdom)
  • Available as PDF
  • Read on any device
  • Instant download
  • Own it forever
eBook
GBP 199.50
Price includes VAT (United Kingdom)
  • Available as EPUB and PDF
  • Read on any device
  • Instant download
  • Own it forever
Softcover Book
GBP 249.99
Price includes VAT (United Kingdom)
  • Compact, lightweight edition
  • Dispatched in 3 to 5 business days
  • Free ship** worldwide - see info
Hardcover Book
GBP 249.99
Price includes VAT (United Kingdom)
  • Durable hardcover edition
  • Dispatched in 3 to 5 business days
  • Free ship** worldwide - see info

Tax calculation will be finalised at checkout

Purchases are for personal use only

Institutional subscriptions

Similar content being viewed by others

References

  1. Girardi, F., Vaona, W., Di Maggio, R.: Resistance of different types of concretes to cyclic sulfuric acid and sodium sulfate attack. Cem. Concr. Compos. 8, 595–602 (2010). https://doi.org/10.1016/j.cemconcomp.2010.07.002

    Article  Google Scholar 

  2. Brunetaud, X., Khelifa, M.R., Al-Mukhtar, M.: Size effect of concrete samples on the kinetics of external sulfate attack. Cem. Concr. Compos. 34(3), 370–376 (2012). https://doi.org/10.1016/j.cemconcomp.2011.08.014

    Article  Google Scholar 

  3. Loser, R., Leemann, A.: An accelerated sulfate resistance test for concrete. Mater. Struct. 49(8), 3445–3457 (2015). https://doi.org/10.1617/s11527-015-0731-2

    Article  Google Scholar 

  4. Menéndez, E., García-Rovés, R., Aldea, B., Ruíz, S., Baroghel-Bouny, V.: Combination of immersion and semi-immersion tests to evaluate concretes manufactured with sulfate-resisting cements. J. Sustain. Cem. Mater. 8(6), 337–352 (2019). https://doi.org/10.1080/21650373.2019.1624659

  5. Achour, R., Zentar, R., Abriak, N.E., Rivard, P., Gregoire, P.: Durability study of concrete incorporating dredged sediments. Case Stud. Constr. Mater. 11, e00244 (2019). https://doi.org/10.1016/j.cscm.2019.e00244

    Article  Google Scholar 

  6. Standard S. SIA 262/1, Appendix D

    Google Scholar 

  7. Alexander, M., Bertron, A., De Belie, N. (eds.): Performance of cement-based materials in aggressive aqueous environments. RSR, vol. 10. Springer, Dordrecht (2013). https://doi.org/10.1007/978-94-007-5413-3

    Book  Google Scholar 

  8. Whittaker, M., Black, L.: Current knowledge of external sulfate attack. Adv. Cem. Res. 27(9), 532–545 (2015). https://doi.org/10.1680/adcr.14.00089

    Article  Google Scholar 

  9. Suma, M.F., Santhanam, M.: Influence of specimen size on the expansion of portland cement mortars immersed in sodium sulphate solution. In: Menéndez, E., Baroghel-Bouny, V. (eds.) External Sulphate Attack – Field Aspects and Lab Tests, RILEM Final Workshop of TC 251-SRT (Madrid - SPAIN, 2018), RILEM Bookseries, RB 21, p. 81. Springer, Cham (2020). https://doi.org/10.1007/978-3-030-20331-3_7

  10. Messad, S., Carcasses, M., Linger, L.: Design of an accelerated test method for external sulfate attack. In: Alexander, M.G., Bertron, B. (eds.) Concrete in aggressive aqueous environments – Perform., Testing and Modeling, RILEM Book, pp. 307–317. Springer (2009)

    Google Scholar 

  11. Aguayo, F.M.: External sulfate attack of concrete : an accelerated test method. mechanisms and mitigation techniques. Dissertation, The University of Texas at Austin (2016). https://repositories.lib.utexas.edu/handle/2152/39727

  12. Irassar, E.F., González, M., Rahhal, V.: Sulphate resistance of type V cements with limestone filler and natural pozzolana. Cem. Concr. Compos. 22(5), 361–368 (2000). https://doi.org/10.1016/S0958-9465(00)00019-6

    Article  Google Scholar 

  13. ASTM International C143-03: Standard test method for slump of hydraulic-cement concrete (2004)

    Google Scholar 

  14. Alderete, N.M., Villagrán-Zaccardi, Y.A., De Belie, N.: Physical evidence of swelling as the cause of anomalous capillary water uptake by cementitious materials. Cem. Concr. Res. 120, 256–266 (2019). https://doi.org/10.1016/j.cemconres.2019.04.001

    Article  Google Scholar 

Download references

Acknowledgment

Financial support from FONCyT through PICT 2015–3339 and PICT 2017–0091 Prest BID for this research is greatly appreciated.

Author information

Authors and Affiliations

Authors

Corresponding author

Correspondence to Lautaro R. Santillán .

Editor information

Editors and Affiliations

Rights and permissions

Reprints and permissions

Copyright information

© 2023 The Author(s), under exclusive license to Springer Nature Switzerland AG

About this paper

Check for updates. Verify currency and authenticity via CrossMark

Cite this paper

Santillán, L.R., Villagrán-Zaccardi, Y.A., Irassar, E.F., Zega, C.J. (2023). Effect of Size and Preconditioning of Concrete Cores Against Sulfate Attack (Test). In: Escalante-Garcia, J.I., Castro Borges, P., Duran-Herrera, A. (eds) Proceedings of the 75th RILEM Annual Week 2021. RW 2021. RILEM Bookseries, vol 40. Springer, Cham. https://doi.org/10.1007/978-3-031-21735-7_33

Download citation

  • DOI: https://doi.org/10.1007/978-3-031-21735-7_33

  • Published:

  • Publisher Name: Springer, Cham

  • Print ISBN: 978-3-031-21734-0

  • Online ISBN: 978-3-031-21735-7

  • eBook Packages: EngineeringEngineering (R0)

Publish with us

Policies and ethics

Navigation