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Estimation of Uncertainty Budgets in Analysis of Nickel by ICP-MS and High-Resolution Mass Spectrometry with a Glow Discharge

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Moscow University Chemistry Bulletin Aims and scope

Abstract

This paper estimates uncertainty budgets in determining the content of impurities of 15 elements (P, Mn, Fe, Cu, Zn, As, Se, Ag, Cd, Sn, Sb, Te, Tl, Pb, Bi) in nickel samples by inductively coupled plasma mass spectrometry (ICP-MS) and high-resolution glow discharge mass spectrometry (GDMS). It is validated by analyzing a certified standard nickel sample (assessed using Student’s simple t test). The main sources of uncertainty in the results of analysis by two methods, including sample preparation and calibration graph, are presented. The total and expanded uncertainties for the two methods are compared. A nickel alloy of the ZhS6U type is analyzed by the ICP-MS and GDMS methods of industrial melting of and the results are compared with a modified Student’s test.

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REFERENCES

  1. Kablov, E.N., Aviats. Mater. Tekhnol., 2015, no. 1(34), p. 3. https://doi.org/10.18577/2071-9140-2015-0-1-3-33

  2. Petrushin, N.V., Ospennikova, O.G., and Svetlov, I.L., Aviats. Mater. Tekhnol., 2017, no. 1 (suppl.), p. 72. https://doi.org/10.18577/2071-9140-2017-0-S-72-103

  3. Kablov, E.N., Sidorov, V.V., Kablov, D.E., and Min, P.G., Aviats. Mater. Tekhnol., 2017, no. 1 (suppl.), p. 55. https://doi.org/10.18577/2071-9140-2017-0-S-55-71

  4. Kablov, E.N., Ospennikova, O.G., and Svetlov, I.L., Aviats. Mater. Tekhnol., 2017, no. 2(47), p. 3.https://doi.org/10.18577/2071-9140-2017-0-2-3-14

  5. Kablov, E.N., Chabina, E.B., Morozov, G.A., and Muravskaya, N.P., Kompetentnost’, 2017, no. 2, p. 40.

  6. Hu, J. and Wang, H., Microchim. Acta, 2001, vol. 137, p. 149.

    Article  CAS  Google Scholar 

  7. Alekseev, A.V., Yakimovich, P.V., and Kvachenok, I.K., Tr, VIAM, 2020, no. 2, 11. http://www.viam-works.ru. Accessed October 21, 2020.

  8. Leikin, A.Yu., Karandashev, V.K., Lisovskii, S.V., and Volkov, I.A., Inorg. Mater., 2015, vol. 51, p. 1389. https://doi.org/10.1134/S0020168515140095

    Article  CAS  Google Scholar 

  9. Yakimovich, P.V., Alekseev, A.V., and Min, P.G., Tr, VIAM, 2014, no. 10, 02. http://www.viam-works.ru. Accessed October 21, 2018.

  10. Karandashev, V.K., Zhernokleeva, K.V., and Karpov, Yu.A., Inorg. Mater., 2013, vol. 49, p. 1303. https://doi.org/10.1134/S0020168513140069

    Article  CAS  Google Scholar 

  11. Pupyshev, A.A. and Epova, E.N., Anal. Kontrol’, 2001, vol. 5, no. 4, p. 335.

    Google Scholar 

  12. Garmash, A.V. and Sorokina, N.M., Metrologicheskie osnovy analiticheskoi khimii (Metrological Foundations of Analytical Chemistry), Moscow: Mosk. Gos. Univ., 2017.

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Funding

This study was supported by the All-Russian Institute of Aviation Materials (VIAM).

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Authors and Affiliations

  1. All-Russian Research Institute of Aviation Materials, 105275, Moscow, Russia

    A. V. Alekseev & P. V. Yakimovich

Authors
  1. A. V. Alekseev
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  2. P. V. Yakimovich
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All authors contributed equally to the preparation of the paper.

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Correspondence to A. V. Alekseev or P. V. Yakimovich.

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The authors declare that they have no conflicts of interest.

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Translated by A. Muravev

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Alekseev, A.V., Yakimovich, P.V. Estimation of Uncertainty Budgets in Analysis of Nickel by ICP-MS and High-Resolution Mass Spectrometry with a Glow Discharge. Moscow Univ. Chem. Bull. 77, 206–213 (2022). https://doi.org/10.3103/S0027131422040022

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  • DOI: https://doi.org/10.3103/S0027131422040022

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