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An Improved Reflection Colorimeter Integrated with a Coaxial Optical-fiber Cable for Highly Sensitive Solid-phase Colorimetry Using a Membrane Filter

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Abstract

Highly sensitive solid-phase colorimetry for nickel ion was demonstrated using an improved reflection colorimeter equipped with a coaxial optical-fiber cable. The nickel complex with α-furil dioxime was collected on a small-size membrane filter embedded in a disposable syringe filter unit. The leading edge of the optical-fiber cable was connected to the syringe filter unit via a Luer-lock fitting, and the color intensity of the sample on the filter was evaluated accurately. The detection limit was 0.8 ng in 2.5 mL of the complex solution (0.3 μg L−1). This improved configuration is applicable to highly sensitive on-site analysis without expensive instruments nor high laboratory skills.

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Authors and Affiliations

  1. Department of Applied Chemistry, Graduate School of Science and Technology, Tokushima, 770-8506, Japan

    Hitoshi Mizuguchi, Yusuke Taniguchi & Toshio Takayanagi

  2. Department of Chemistry, Faculty of Mathematics and Natural Sciences, Universitas Gadjah Mada, Yogyakarta, 55281, Indonesia

    Suherman Suherman

  3. Ushio Inc., 1-6-5 Marunouchi, Chiyoda, Tokyo, 100-8150, Japan

    Kinichi Morita

  4. College of Bioscience and Chemistry, Kanazawa Institute of Technology, 3-1 Yatsukaho, Hakusan, Ishikawa, 924-0838, Japan

    Yasutada Suzuki

Authors
  1. Hitoshi Mizuguchi
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  2. Yusuke Taniguchi
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  3. Suherman Suherman
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  4. Kinichi Morita
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  5. Toshio Takayanagi
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  6. Yasutada Suzuki
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Correspondence to Hitoshi Mizuguchi.

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Mizuguchi, H., Taniguchi, Y., Suherman, S. et al. An Improved Reflection Colorimeter Integrated with a Coaxial Optical-fiber Cable for Highly Sensitive Solid-phase Colorimetry Using a Membrane Filter. ANAL. SCI. 37, 1045–1048 (2021). https://doi.org/10.2116/analsci.20N033

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  • DOI: https://doi.org/10.2116/analsci.20N033

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