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Synthesis and crystal structures of 1,2-diaminobenzene-Ni complexes

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Abstract

Treatment in different proportions of 1,2-diaminobenzene with Ni(OAc)2 · 4H2O in methanol results in the formation of two 1,2-diaminobenzene-Ni complexes I (C92H134N24Ni9O28) and II (C16H22N4NiO4). Their structures were determined by X-ray diffraction analysis. The complexes are also characterized by elemental analysis and IR.

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Authors and Affiliations

  1. Hefei University of Technology, Hefei, 230009, P.R. China

    L. Mei & L. S. Tai

  2. University of Science and Technology of China, Hefei, 230009, P.R. China

    Z. S. Ming & L. Q. Rong

  3. Shanghai Institute of Organic Chemistry, Shanghai, 200032, P.R. China

    S. Jie

Authors
  1. L. Mei
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  2. L. S. Tai
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  3. Z. S. Ming
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  4. S. Jie
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  5. L. Q. Rong
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Correspondence to L. Mei.

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Mei, L., Tai, L.S., Ming, Z.S. et al. Synthesis and crystal structures of 1,2-diaminobenzene-Ni complexes. Russ J Coord Chem 38, 337–341 (2012). https://doi.org/10.1134/S1070328412050077

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  • DOI: https://doi.org/10.1134/S1070328412050077

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