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Synthesis of ceramics based on zirconium and hafnium borides by spark plasma sintering and study of its thermal oxidative stability

  • Synthesis and Properties of Inorganic Compounds
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Abstract

Ultra-high-temperature ceramic materials based on zirconium and hafnium borides were obtained by spark plasma sintering. The samples were thermal-shock tested on a gas-dynamic setup in an oxidizing atmosphere; the temperature on the surface of the samples was 2100°C. The microstructure of the samples after sintering and gas-dynamic tests was studied by electron microscopy, X-ray tomography, and elemental analysis.

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Authors and Affiliations

  1. JSC Ural Research Institute of Composite Materials, ul. Novozvyaginskaya 57, Perm, 614014, Russia

    Yu. B. Lyamin & E. N. Pryamilova

  2. Perm National Research Polytechnic University, Komsomol’skii pr. 29, Perm, 614990, Russia

    V. Z. Poilov, E. N. Pryamilova & A. A. Efimov

  3. Lavrent’ev Institute of Hydrodynamics, Russian Academy of Sciences, Siberian Branch, pr. Lavrent’eva 15, Novosibirsk, 630090, Russia

    V. I. Mali & A. G. Anisimov

Authors
  1. Yu. B. Lyamin
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  2. V. Z. Poilov
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  3. E. N. Pryamilova
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  4. A. A. Efimov
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  5. V. I. Mali
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  6. A. G. Anisimov
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Corresponding author

Correspondence to E. N. Pryamilova.

Additional information

Original Russian Text © Yu.B. Lyamin, V.Z. Poilov, E.N. Pryamilova, A.A. Efimov, V.I. Mali, A.G. Anisimov, 2016, published in Zhurnal Neorganicheskoi Khimii, 2016, Vol. 61, No. 2, pp. 160–166.

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Lyamin, Y.B., Poilov, V.Z., Pryamilova, E.N. et al. Synthesis of ceramics based on zirconium and hafnium borides by spark plasma sintering and study of its thermal oxidative stability. Russ. J. Inorg. Chem. 61, 149–155 (2016). https://doi.org/10.1134/S0036023616020133

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  • DOI: https://doi.org/10.1134/S0036023616020133

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