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Synthesis, Crystal Structure, and Properties of [Dy(p-ABA)3Phen · H2O] · 1.5H2O1

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Abstract

(1.10-Phenanthroline)-tris(4-amidobenzoate)dysprosium, [Dy(p-ABA)3Phen · H2O] · 1.5H2O (where p-ABA = p-amidobenzoate and Phen = 1.10-phenanthroline) has been synthesized. The complex was characterized by elemental analysis, UV, IR spectroscopy, and molar conductance. The crystal structure was determined by X-ray crystallography. The coordination number of the mononuclear complex is nine. The crystals are triclinic, space group P1 with a = 10.4484(13) Å, b = 12.2015(15) Å, c = 14.0170(17) Å; α = 92.800(2)°, β = 102.7220(10)°, γ = 108.880(2)°. Z = 2, d c = 1.617 mg m−3, F(000) = 786. R1 = 0.0327, and wR2 = 0.0911.

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Authors and Affiliations

  1. Experimental Center, Hebei Normal University, Shijiazhuang, 050016, P R China

    Jian-Jun Zhang, Su-Ling Xu, Ning Ren & Hai-Yan Zhang

  2. College of Chemistry and Material Science, Hebei Normal University, Shijiazhuang, 050016, P R China

    Su-Ling Xu, Ning Ren & Hai-Yan Zhang

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  1. Jian-Jun Zhang
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  2. Su-Ling Xu
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  3. Ning Ren
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  4. Hai-Yan Zhang
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Zhang, JJ., Xu, SL., Ren, N. et al. Synthesis, Crystal Structure, and Properties of [Dy(p-ABA)3Phen · H2O] · 1.5H2O1 . Russ. J. Inorg. Chem. 53, 397–401 (2008). https://doi.org/10.1134/S0036023608030108

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  • DOI: https://doi.org/10.1134/S0036023608030108

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