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Study on wear and corrosion properties of functionally graded nickel–cobalt–\((\hbox {Al}_{2}\hbox {O}_{3})\) coatings produced by pulse electrodeposition

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Abstract

Functionally graded nickel–cobalt coatings with/without alumina nanoparticles were pulse electrodeposited on a carbon steel substrate by a continuous decrease in duty cycle from 95 to 10% at different frequencies of 100, 500 and 1000 Hz. The effect of pulse parameters on the nanoparticle content, chemical composition, microstructure, corrosion properties and tribological behaviour of coatings was studied. Energy-dispersive X-ray spectroscopy analysis showed that the amount of cobalt is gradually reduced and the content of alumina nanoparticles is increased from the substrate/coating interface to the surface. Based on the electrochemical studies in 3.5 wt% NaCl, the nanocomposite coatings gain the highest corrosion resistance at the lowest frequency. Also, the hardness of coatings gradually increased. Evaluation of the tribological behaviour of coatings by a pin-on-disk wear test showed that the nanoparticles have a positive effect on wear resistance and improve it by increasing frequency.

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Authors and Affiliations

  1. Department of Materials Engineering, Faculty of Engineering, Tarbiat Modares University, Tehran, 1411713116, Iran

    A Karimzadeh, M Aliofkhazraei & A S Rouhaghdam

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  1. A Karimzadeh
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  2. M Aliofkhazraei
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  3. A S Rouhaghdam
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Correspondence to M Aliofkhazraei.

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Karimzadeh, A., Aliofkhazraei, M. & Rouhaghdam, A.S. Study on wear and corrosion properties of functionally graded nickel–cobalt–\((\hbox {Al}_{2}\hbox {O}_{3})\) coatings produced by pulse electrodeposition. Bull Mater Sci 42, 53 (2019). https://doi.org/10.1007/s12034-018-1715-y

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