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Effect of Normalizing Treatment on Microstructure and Mechanical Properties of Non-oriented Fe-3.0% Si Steel

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Abstract

This study focuses on the microstructure evolution of non-oriented silicon steel for the drive motor iron core of new energy vehicles. The Fe-3.0% Si non-oriented silicon steel hot-rolled bands were taken as the research objects and were normalized at 700, 800 and 900 °C for 3 and 10 min. The influence of low-temperature normalization process on the microstructure, texture and mechanical properties was studied. The results show that the bands normalized at 700 and 800 °C inherit the gradient microstructure and texture characteristics of the initial hot-rolled band. The surface layer consists of homogeneous and fine recrystallized grains, the central layer consists of elongated deformed grains with γ-fiber and α-fiber textures and the subsurface layer has mixed grain structure with strong Goss texture. When the normalizing temperature is increased to 900 °C, the normalized band is completely recrystallized, and the gradient structure and texture are significantly weakened. During the normalizing process, the θ-fiber oriented grains in the subsurface mainly nucleate at the grain boundaries of the α*-fiber and <110> //ND matrix grains, and the <110> //ND oriented grains mainly nucleate at the grain boundaries of Goss and {110} <115> deformed matrix grains. The θ-fiber oriented grains in the central layer mainly nucleate at the grain boundaries of {001} <110>, γ-fiber and {114} <481> matrix grains, the α-fiber oriented grains nucleate in the {111} <110> and α-fiber deformed matrix grains, the nucleation of α*-fiber grains is related to the α-fiber deformed matrix grains. After normalizing at 900 °C, θ-fiber and α*-fiber grains have growth advantages, resulting in strong θ-fiber and α*-fiber textures. As the normalizing temperature increases, the gradient structure of the normalized microstructure is gradually weakened, thus leading to the decrease in plastic deformation ability.

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Data Availability

Data will be made available on request.

References

  1. C.X. Zhou, H.J. Jiang, C.M. Liu, B. Yan, and P.F. Yan, Microstructure Features of High Performance Soft Magnetic Alloy Fe-3 wt.% Si Prepared by Metal Injection Molding, Mater. Chem. Phys., 2021, 273, p 125068.

    Article  CAS  Google Scholar 

  2. Q.S. Liu, Z.H. Zhang, Y.H. Pei, L.F. Shi, and X. Qi, Study on High Temperature Ductility of Fe-3.0 % Si Non-oriented Electrical Steel, Electrical Steel, 2019, 1(2), p 42-44+53.

    Google Scholar 

  3. B. Zhong, Z. Cheng, M. Wendler, O. Volkova, and J. Liu, Optimized Rolling Processes to Balance Magnetic and Mechanical Properties of High-Strength Non-oriented Silicon Steels, Mater. Des., 2023, 232, 112096.

    Article  CAS  Google Scholar 

  4. X. Li, X. Hu, Q. Guo, X. Wu, H. Sui, L. **ang, and H. Luo, Characterizing Changes in Microstructures, Mechanical and Magnetic Properties of Non-oriented Silicon Steel Due to Pulsed Current, Mater Charact, 2024, 211, 113904.

    Article  CAS  Google Scholar 

  5. H. Wang, K. Shao, J. Qiao, H. Pan, B. Fu, and S. Qiu. Influence Mechanism of Sn on 2.7% Si-0.5% Al Non-oriented Silicon Steel. JOM, 1-11 (2024)

  6. X.D. Zhang, Y. Wang, C. Liu et al., Development and Application Research Status on Non-oriented Silicon Steel for Driving Motor of New Energy Vehicles, Automob. Technol. Mater., 2022, 9, p 9–14.

    Google Scholar 

  7. C.Y. Zhu, Y.K. Bao, Y. Wang, J.H. Ma, and G.Q. Li, Research Progress on Application Status and Property Control of Non-oriented Silicon Steel for Traction Motor of New Energy Vehicles, Mater. Rep., 2021, 35(23), p 23089–23096.

    Google Scholar 

  8. L.F. Fan, M.M. Qin, E.B. Yue, L.J. **ao, and J.Z. He, Technological Challenges of New Energy Vehicle to Non-oriented Silicon Steel, Mater. Rep., 2021, 35(15), p 15183–15188.

    Google Scholar 

  9. D.M. Chen, G.D. Wang, and H.T. Liu, The Significance of Hot Rolled Microstructure Controlled by Fine-Tuning Al Content to Texture Evolution and Magnetic Properties of Low Silicon Non-oriented Electrical Steels, J. Magn. Magn. Mater., 2021, 528, 167740.

    Article  CAS  Google Scholar 

  10. J. Hunady, M. Cernik, E.J. Hilinski, M. Predmersky, and A. Magurova, Influence of Chemistry and Hot Rolling Conditions on High Permeability Non-grain Oriented Silicon Steel, J. Magn. Magn. Mater., 2006, 304, p 620–623.

    Article  Google Scholar 

  11. S.B.C. Paolinelli, M.A.D. Cunha, and A.B. Cota, Effect of Hot Band Grain Size on the Texture Evolution of 2%Si Non-oriented Steel During Final Annealing, IEEE Trans. Magn., 2015, 51, p 1–4.

    Article  CAS  Google Scholar 

  12. H. Yashiki and T. Kaneko, Effect of Hot-band Annealing on Anisotropy of Magnetic Properties in Low-Si Semi-Processed Electrical Steels, J. Magn. Magn. Mater., 1992, 112, p 200–202.

    Article  CAS  Google Scholar 

  13. K.M. Lee, M.Y. Huh, H.J. Lee, J.T. Park, J.S. Kim, E.J. Shin, and O. Engler, Effect of Hot Band Grain Size on Development of Textures and Magnetic Properties in 2.0% Si Non-oriented Electrical Steel Sheet, J. Magn. Magn. Mater., 2015, 396, p 53–64.

    Article  CAS  Google Scholar 

  14. T. Ye, Z.Y. Gao, Z.W. Lu, Z.G. Zhong, and C.H. Ma, Effect of Normalized Temperature on Microstructure, Texture Transformation and Magnetic Properties of Hot Rolled Band of Electrical Steel 50W300, Special Steel, 2022, 43(4), p 82–87.

    Google Scholar 

  15. X.D. Zhang, J.B. Qi, Z.L. **, and Z.W. Wu, Effect of Normalizing Process on Hot Rolling Microstructure and Precipitates of Non-oriented Silicon Steel, Shaxi Metall., 2022, 45(4), p 4–5.

    Google Scholar 

  16. H.D. Yao, G.T. Liu, Z.Y. Hu, D.Y. An, B.L. Zhang, and L. Cheng, Influence of Normalizing Temperature on Microstructure and Properties of Non-oriented Electrical Steel Bands, Electrical Steel, 2021, 3(6), p 19–25.

    Google Scholar 

  17. X.L. Wang, L. Luo, and W.Z. Li, Origin of Fine Equiaxed Grains in Industrial Low-Temperature Grain-Oriented Silicon Steel Normalized Band and Their Influence on Magnetic Properties, J. Magn. Magn. Mater., 2022, 552, p 169210.

    Article  CAS  Google Scholar 

  18. J.B. Qi, X.D. Zhang, and Z.L. **, Effects of Normalized Annealing on Hot Rolled Microstructure and Texture of 50W400 Non-oriented Silicon Steel, Hot Work. Technol., 2023, 10, p 118–122.

    Google Scholar 

  19. C.X. He, F.Y. Yang, G.C. Yan, L. Meng, G. Ma, X. Chen, and W.M. Mao, Effect of Normalizing on Textures of Thin-Gauge Grain-Oriented Silicon Steel, Acta Metall. Sin., 2016, 52(9), p 1063–1069.

    CAS  Google Scholar 

  20. Y. Li, Research Progress on Gradient Metallic Materials, Mater. China, 2016, 35(9), p 658-665+700-701.

    Google Scholar 

  21. H. Li, Y.L. Feng, M. Song, J.L. Liang, and D.Q. Cang, Effect of Normalizing Cooling Process on Microstructure and Precipitates in Low-Temperature Silicon Steel, Trans. Nonferrous Metals Soc. China, 2014, 24(3), p 770–776.

    Article  CAS  Google Scholar 

  22. E.J. Gutiérrez-Castañeda and A. Salinas-Rodríguez, Effect of Annealing Prior to Cold Rolling on Magnetic and Mechanical Properties of Low Carbon Non-Oriented Electrical Steels, J. Magn. Magn. Mater., 2011, 323(20), p 2524–2530.

    Article  Google Scholar 

  23. H.J. Xu, Y.B. Xu, H.T. Jiao, S.F. Cheng, R.D.K. Misra, and J.P. Li, Influence of Grain Size and Texture Prior to Warm Rolling on Microstructure, Texture and Magnetic Properties of Fe-6.5 wt.% Si Steel, J. Magn. Magn. Mater., 2018, 453, p 236–245.

    Article  CAS  Google Scholar 

  24. Y.F. Wang, G.Q. Zu, S.C. Sun, Y. Han, W.W. Zhu, H. Wu, Y. Zhao, and X. Ran. Role of Texture Before Rolling: A Research Based on Texture and Magnetic Properties of 4.5 wt.% Si Non-oriented Electrical Steel. J. Iron Steel Res. Int. 1-14 (2024)

  25. S. Takajo, C.C. Merriman, S.C. Vogel, and D.P. Field, In-situ EBSD Study on the Cube Texture Evolution in 3 wt% Si Steel Complemented by Ex-Situ EBSD Experiment-From Nucleation to Grain Growth, Acta Mater., 2019, 166, p 100–112.

    Article  CAS  Google Scholar 

  26. P. Gobernado, R.H. Petrov, and L.A. Kestens, Recrystallized {311}<136> Orientation in Ferrite Steels, Scripta Mater., 2012, 66(9), p 623–626.

    Article  CAS  Google Scholar 

  27. N. Zhang, P. Yang, and W. Mao, 001}<120>-{113}<361> Recrystallization Textures Induced by Initial {001 Grains and Related Microstructure Evolution in Heavily Rolled Electrical Steel, Mater Charact, 2016, 119, p 225–232.

    Article  CAS  Google Scholar 

  28. J.L. Liu, Y.H. Sha, K. Hu, F. Zhang, and L. Zuo, Formation of Cube and Goss Texture After Primary Recrystallization in Electrical Steels, Metall. and Mater. Trans. A., 2014, 45(1), p 134–138.

    Article  Google Scholar 

  29. T. Nguyen-Minh, J.J. Sidor, R.H. Petrov, and L.A.I. Kestens, Occurrence of Shear Bands in Rotated GOSS ({110}<110>) Orientations of Metals with bcc Crystal Structure, Scripta Mater., 2012, 67(12), p 935–938.

    Article  CAS  Google Scholar 

  30. Y. Wang, Numerical Investigations on Strengthening-Toughening and Failuremechanisms of Metallic Materials with Gradient Structure, Bei**g Jiaotong University, 2019.

    Google Scholar 

  31. K. Lu, Gradient Nanosr tured Materials, Acta Metall. Sin., 2015, 51(1), p 1–10.

    Article  Google Scholar 

Download references

Acknowledgments

This paper is financially supported by the National Natural Science Foundation of China (52205385 and 52205403), the Open Research Fund from the State Key Laboratory of Rolling and Automation, Northeastern University (2021RALKFKT002), Zhejiang Provincial Natural Science Foundation of China (LQ23E050008), Ningbo Science and Technology Major Project (2022Z009 and 2023Z011) and Ningbo Yongjiang Talent Introduction Program (2023A-157-G).

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Cheng Xu helped in preliminary investigation, method proposed, data collation and writing—original draft. Haijie Xu helped in concept proposed, resource provided and writing—review. Xuedao Shu worked in supervision and guidance, and writing—editing. Xubeng Lu worked in software simulation. Lulan Jiang helped in part of the ideas. Zixuan Li helped in data validation. Yuanxiang Zhang contributed to experimental help.

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Correspondence to Haijie Xu.

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Xu, C., Xu, H., Shu, X. et al. Effect of Normalizing Treatment on Microstructure and Mechanical Properties of Non-oriented Fe-3.0% Si Steel. J. of Materi Eng and Perform (2024). https://doi.org/10.1007/s11665-024-09777-w

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