Abstract
Mechanically robust Fe3O4/porous carbon/diatomite composite monolith was prepared from waste corrugated cardboard box and diatomite via slurrying in FeCl3 solution, dewatering, molding, and carbonization at 600 °C. The products were characterized by X-ray diffraction (XRD), field emission scanning electron microscope (SEM), N2-adsorption/desorption, Raman spectroscopy, and ultraviolet-visible-near-infrared (UV-Vis-NIR) spectroscopy. The water wettability, photothermal conversion property, and solar steam generation performance of the products were also evaluated. Results showed that the presence of FeCl3 led to the formation of more pores and magnetic Fe3O4 crystallites, while diatomite provided good hydrophilicity for the composite. The product exhibited light absorption above 65% within the wavelength ranging from 200 to1974 nm, and its surface temperature eventually increased by 30 °C under 0.25 sun irradiation due to photothermal effect. Moreover, solar steam yield under 0.25 sun irradiation for 3600 s was improved by 67% with the presence of the monolithic composite because of the occurrence of interfacial solar steam generation and heat transfer from the composite acted as a heat island.
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References
Baek J, Lee H-M, Roh J-S, Lee H-S, Kang HS, Kim B-J (2016) Studies on preparation and applications of polymeric precursor-based activated hard carbons: I. Activation mechanism and microstructure analyses. Microporous Mesoporous Mater 219:258–264
Bagheripour E, Moghadassi AR, Hosseini SM, Ray MB, Parvizian F, Van der Bruggen B (2018) Highly hydrophilic and antifouling nanofiltration membrane incorporated with water-dispersible composite activated carbon/chitosan nanoparticles. Chem Eng Res Des 132:812–821
Bedia J, Belver C, Ponce S, Rodriguez J, Rodriguez JJ (2018) Adsorption of antipyrine by activated carbons from FeCl3-activation of Tara gum. Chem Eng J 333:58–65
Chang J, Zhang J, Tan B, Wang Q, Liu N, Xue Q (2020) New insight into the removal of Cd(II) from aqueous solution by diatomite. Environ Sci Pollut R 27:9882–9890
Chen Y, Sha C, Wang W, Yang F (2020) Solar-driven steam generation on nitrogen-doped graphene in a 2D water path isolation system. Mater Res Express 7:015507
Di Fidio N, Antonetti C, Raspolli Galletti AM (2019) Microwave-assisted cascade exploitation of giant reed (Arundo donax L.) to xylose and levulinic acid catalysed by ferric chloride. Bioresour Technol 293:122050
Ding Z, Xu X, Phan T, Hu X (2018) Carbonized waste corrugated paper packaging boxes as low-cost adsorbent for removing aqueous Pb(II), Cd(II), Zn(II), and Methylene Blue. Pol J Environ Stud 27:2483–2491
Ebrahimi M, Van der Bruggen B, Hosseini SM, Askari M, Nemati M (2018) Improving electrochemical properties of cation exchange membranes by using activated carbon-co-chitosan composite nanoparticles in water deionization. Ionics 25:1199–1214
Fang J, Liu J, Gu J, Liu Q, Zhang W, Su H, Zhang D (2018) Hierarchical porous carbonized lotus seedpods for highly efficient solar steam generation. Chem Mater 30:6217–6221
Fang Q, Li T, Chen Z, Lin H, Wang P, Liu F (2019) Full biomass-derived solar stills for robust and stable evaporation to collect clean water from various water-bearing media. ACS Appl Mater Interfaces 11:10672–10679
Galzerano B, Capasso I, Verdolotti L, Lavorgna M, Vollaro P, Caputo D, Iannace S, Liguori B (2018) Design of sustainable porous materials based on 3D-structured silica exoskeletons, diatomite: chemico-physical and functional properties. Mater Des 145:196–204
Gao S, Dong X, Huang J, Dong J, Maggio FD, Wang S, Guo F, Zhu T, Chen Z, Lai Y (2019) Bioinspired soot-deposited janus fabrics for sustainable solar steam generation with salt-rejection. Global Chall 3:1800117
He J, Zhao G, Mu P, Wei H, Su Y, Sun H, Zhu Z, Liang W, Li A (2019) Scalable fabrication of monolithic porous foam based on cross-linked aromatic polymers for efficient solar steam generation. Sol Energ Mat Sol C 201:110111
Hu N, Xu Y, Liu Z, Liu M, Shao X, Wang J (2020) Double-layer cellulose hydrogel solar steam generation for high-efficiency desalination. Carbohydr Polym 243:116480
Jia J, Liang W, Sun H, Zhu Z, Wang C, Li A (2019) Fabrication of bilayered attapulgite for solar steam generation with high conversion efficiency. Chem Eng J 361:999–1006
Kashyap V, Ghasemi H (2020) Solar heat localization: concept and emerging applications. J Mater Chem A 8:7035–7065
Sotoudehnia F, Baba Rabiu A, Alayat A, McDonald AG (2020) Characterization of bio-oil and biochar from pyrolysis of waste corrugated cardboard. J Anal Appl Pyrolysis 145:104722
Sun W, Du A, Feng Y, Shen J, Huang S, Tang J, Zhou B (2016) Super black material from low-density carbon aerogels with subwavelength structures. ACS Nano 10:9123–9128
Sun L, Liu J, Zhao Y, Xu J, Li Y (2019) Highly efficient solar steam generation via mass-produced carbon nanosheet frameworks. Carbon 145:352–358
Sun P, Zhang W, Zada I, Zhang Y, Gu J, Liu Q, Su H, Pantelic D, Jelenkovic B, Zhang D (2020) 3D-structured carbonized sunflower heads for improved energy efficiency in solar steam generation. ACS Appl Mater Interfaces 12:2171–2179
Tahir Z, Kim S, Ullah F, Lee S, Lee JH, Park NW, Seong MJ, Lee SK, Ju TS, Park S, Bae JS, Jang JI, Kim YS (2020) Highly efficient solar steam generation by glassy carbon foam coated with two-dimensional metal chalcogenides. ACS Appl Mater Interfaces 12:2490–2496
Tao P, Ni G, Song C, Shang W, Wu J, Zhu J, Chen G, Deng T (2018) Solar-driven interfacial evaporation. Nat Energy 3:1031–1041
Theydan SK, Ahmed MJ (2012) Adsorption of methylene blue onto biomass-based activated carbon by FeCl3 activation: equilibrium, kinetics, and thermodynamic studies. J Anal Appl Pyrolysis 97:116–122
Tian D, Xu Z, Zhang D, Chen W, Cai J, Deng H, Sun Z, Zhou Y (2019) Micro–mesoporous carbon from cotton waste activated by FeCl3/ZnCl2: preparation, optimization, characterization and adsorption of methylene blue and eriochrome black T. J Solid State Chem 269:580–587
Tsai W-T, Jiang T-J (2018) Mesoporous activated carbon produced from coconut shell using a single-step physical activation process. Biomass Convers Bior 8:711–718
Unlu N, Ceylan S, Erzengin M, Odabasi M (2011) Investigation of protein adsorption performance of Ni2+-attached diatomite particles embedded in composite monolithic cryogels. J Sep Sci 34:2173–2180
Usevičiūtė L, Baltrėnaitė-Gedienė E (2020) Dependence of pyrolysis temperature and lignocellulosic physical-chemical properties of biochar on its wettability. Biomass Convers Bior. https://doi.org/10.1007/s13399-020-00711-3
Wang H, Du A, Ji X, Zhang C, Zhou B, Zhang Z, Shen J (2019) Enhanced photothermal conversion by hot-electron effect in ultrablack carbon aerogel for solar steam generation. ACS Appl Mater Interfaces 11:42057–42065
**a M, Shao X, Sun Z, Xu Z (2020) Conversion of cotton textile wastes into porous carbons by chemical activation with ZnCl2, H3PO4, and FeCl3. Environ Sci Pollut R 27:25186–25196
Xu S, Jiang Q (2018) Surface modification of carbon fiber support by ferrous oxalate for biofilm wastewater treatment system. J Clean Prod 194:416–424
Xu N, Hu X, Xu W, Li X, Zhou L, Zhu S, Zhu J (2017) Mushrooms as efficient solar steam-generation devices. Adv Mater 29:1606762
Xu Z, Sun Z, Zhou Y, Chen W, Zhang T, Huang Y, Zhang D (2019) Insights into the pyrolysis behavior and adsorption properties of activated carbon from waste cotton textiles by FeCl3-activation. Colloid Surface A 582:123934
Xu Z, Zhou Y, Sun Z, Zhang D, Huang Y, Gu S, Chen W (2020) Understanding reactions and pore-forming mechanisms between waste cotton woven and FeCl3 during the synthesis of magnetic activated carbon. Chemosphere 241:125120
Yang J, Zhao Y, Ma S, Zhu B, Zhang J, Zheng C (2016) Mercury removal by magnetic biochar derived from simultaneous activation and magnetization of sawdust. Environ Sci Technol 50:12040–12047
Yang L, Chen G, Zhang N, Xu Y, Xu X (2019) Sustainable biochar-based solar absorbers for high-performance solar-driven steam generation and water purification. ACS Sustain Chem Eng 7:19311–19320
Yuan S-J, Zhang J-J, Fan H-X, Dai X-H (2018) Facile and sustainable shear mixing/carbonization approach for upcycling of carton into superhydrophobic coating for efficient oil-water separation. J Clean Prod 196:644–652
Zhang S, Zang L, Dou T, Zou J, Zhang Y, Sun L (2020) Willow Catkins-derived porous carbon membrane with hydrophilic property for efficient solar steam generation. ACS Omega 5:2878–2885
Zhao F, Guo Y, Zhou X, Shi W, Yu G (2020) Materials for solar-powered water evaporation. Nat Rev Mater 5:388–401
Zheng R, Ren Z, Gao H, Zhang A, Bian Z (2018) Effects of calcination on silica phase transition in diatomite. J Alloys Compd 757:364–371
Zhu L, Gao M, Peh CKN, Ho GW (2019a) Recent progress in solar-driven interfacial water evaporation: advanced designs and applications. Nano Energy 57:507–518
Zhu M, Yu J, Ma C, Zhang C, Wu D, Zhu H (2019b) Carbonized daikon for high efficient solar steam generation. Sol Energ Mat Sol C 191:83–90
Zhu Z, Mu P, Fan Y, Bai W, Zhang Z, Sun H, Liang W, Li A (2020) Highly efficient solar steam generation of bilayered ultralight aerogels based on N-rich conjugated microporous polymers nanotubes. Eur Polym J 126:109560
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The authors wish to thank the anonymous reviewers for their comments.
Funding
This work was supported by the National Natural Science Foundation of China (51909292) and Fundamental Research Funds for Central Public Welfare Scientific Research Institution (K-JBYWF-2018-T02, K-JBYWF-2019-ZT02, Y-JBYWF-2019-16).
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Ma, Y., Cao, J. Preparation of mechanically robust Fe3O4/porous carbon/diatomite composite monolith for solar steam generation. Environ Sci Pollut Res 27, 45775–45786 (2020). https://doi.org/10.1007/s11356-020-10511-x
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DOI: https://doi.org/10.1007/s11356-020-10511-x