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Effect of Zn2+ substitution on DC electrical resistivity and magnetic properties of Mg0.5−xZnxCo0.5Fe2O4 nano ferrite

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Abstract

Mg0.5−xZnxCo0.5Fe2O4 with ferrites were substituted with Zn2+ with concentrations x = 0.0, 0.05, 0.1, 0.15, 0.2, and 0.25 prepared from a sol–gel auto-combustion method. The impact of Zn2+ ion substitution on morphological, structural, DC electrical resistivity, and magnetic characteristics was examined. The diffraction analysis with X-ray reveals that the prepared ferrites are spinel with a single-phase face-centred cubic structure. The cubic crystal structure samples’ values for the crystallite size (42 to 25 nm) and lattice constant (8.386 to 8.425 Å) increased as the concentration increased. Field-effect scanning electron microscopy revealed the ferrite samples’ polycrystalline structures and spherical morphologies. Using FESEM micrographs, the average grain size was between 56.4 and 85.7 nm. Fourier-transform infrared spectroscopy was used to identify two different peaks that emerged at around 585–592 cm−1 and 401–405 cm−1. These peaks revealed information on the functional groups of the sample chemicals. Temperature-dependent DC electrical resistivity shows the semiconductors’ nature samples. The vibrating sample magnetometer analysis shows that the ferrites are soft ferrimagnetic. The saturation magnetisation was increased (60.45 to 85.04 emu/g), and coercivity was decreased (356.46 to 620.59 Oe) when the concentration was increased. The study unveiled tuned values of the physical characteristics, thereby highlighting potential applications in recent technologies.

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Data can be obtained from the corresponding author on request.

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Authors and Affiliations

  1. Department of Physics, Government Degree College, Uppal, Medchal-Malkajgiri (Dt), Telangana, 500039, India

    V. Srinivasa Rao

  2. Department of Physics, K. R. K. Government Degree College, Addanki, Bapatla (Dt), Andhra Pradesh, 523201, India

    V. Prasad

  3. Department of Physics, R. V. Institute of Technology, Chebrolu, Guntur (Dt), Andhra Pradesh, 522212, India

    A. Raghavendra Rao

  4. Department of Physics, Tirumala Engineering College, Jonnalagadda, Planadu (Dt), Andhra Pradesh, 522 601, India

    K. Anil Kumar

  5. Department of Physics, Vasireddy Venkatadri Institute of Technology, Nambur, Guntur (Dt), Andhra Pradesh, 522508, India

    T. Madhu Mohan

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  3. A. Raghavendra Rao
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Contributions

V. Srinivasa Rao, V Prasad prepared the sample and wrote the manuscript, A. Raghavendra Rao helped to discuss the article framework and participated in the testing of materials, K. Anil Kumar developed the experimental formula and provided the measurements, and T. Madhu Mohan provided research ideas and guided experiments. All authors contributed to the discussions and preparation of the manuscript.

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Rao, V.S., Prasad, V., Rao, A.R. et al. Effect of Zn2+ substitution on DC electrical resistivity and magnetic properties of Mg0.5−xZnxCo0.5Fe2O4 nano ferrite. J Mater Sci: Mater Electron 35, 1398 (2024). https://doi.org/10.1007/s10854-024-13166-3

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