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Fe3O4 Nanoparticles Embedded in Polyvinylpyrrolidone Matrix: Effects of Synthesis Processes on the Structure and Magnetic Properties

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Abstract

In this work, the effects of the interaction between the polyvinylpyrrolidone (PVP) and iron ions on the structure and magnetic properties of the Fe3O4 nanoparticles have been investigated. For this purpose, four co-precipitation processes were considered. The spinel structure of the magnetic nanoparticles was confirmed by X-ray diffraction (XRD) and the surface morphology of nanocomposites was analyzed using Scanning Electron microscopy (SEM). The interaction between the polymer and surface of the particles was studied by Fourier Transform Infrared spectroscopy (FT–IR). Also magnetic properties of the nanoparticles were measured applying Vibrating Sample Magnetometer (VSM). Results present that the samples have different crystallite sizes and saturation magnetizations. Also four precipitation processes led to various amount of tensile strain in the structure of nanocomposites.

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Acknowledgements

This research was supported by the University of Mohaghegh Ardabili.

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The Funding was provided by University of Mohaghegh Ardabili

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Authors and Affiliations

  1. Department of Engineering Sciences, Faculty of Advanced Technologies, University of Mohaghegh Ardabili, Namin, Iran

    Sharareh Mirzaee

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  1. Sharareh Mirzaee
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All parts of this research include the initial idea, Synthesis processes, characterization of the samples, and discussions on the results have been made and written by Sharareh Mirzaee.

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Correspondence to Sharareh Mirzaee.

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Mirzaee, S. Fe3O4 Nanoparticles Embedded in Polyvinylpyrrolidone Matrix: Effects of Synthesis Processes on the Structure and Magnetic Properties. Trans Indian Inst Met (2024). https://doi.org/10.1007/s12666-024-03346-4

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